Ultraviolet Spectrophotometric Determination of Benzoic Acid in Refined Phthalic Anhydride.

1962 ◽  
Vol 34 (2) ◽  
pp. 197-199 ◽  
Author(s):  
Raita Murnieks ◽  
C. E. Gonter
1977 ◽  
Vol 60 (5) ◽  
pp. 1175-1179
Author(s):  
Abdel-Aziz M Wahbi ◽  
Hassan Abdine ◽  
Salah M Blaih

Abstract Benzoic acid, propyl p-hydroxybenzoate, and sorbic acid in milk have been determined by using the corresponding first derivative curves of absorption spectra of clarified milk samples. The ΔA/Δλ curves were computed and the concentration of each preservative was calculated using 1 point, 2 points, and/or 3 points. In all cases, the percentage error was within 2.4%.


2020 ◽  
Vol 2020 ◽  
pp. 1-8 ◽  
Author(s):  
Oleksandr S. Tymoshuk ◽  
Orest S. Fedyshyn ◽  
Lesia V. Oleksiv ◽  
Petro V. Rydchuk ◽  
Vasyl S. Matiychuk

The simple, rapid spectrophotometric method for palladium(II) ions determination using a new analytical reagent is described. The interaction of Pd(II) ions with a reagent, of the class of azolidones, 4-(N′-(4-imino-2-oxo-thiazolidine-5-ylidene)-hydrazino)-benzoic acid, in water medium results in the formation of a complex. The Pd(II)-p-ITYBA complex shows maximum absorbance at a wavelength of 450 nm. The molar absorptivity is 4.30 × 103 L·mol−1·cm−1. The optimal pH for complex formation is 7.0. The developed method has a wide linearity range of 0.64–10.64 µg·mL−1 for Pd(II). The detection limit is 0.23 µg·mL−1. It was found that Co(II), Ni(II), Zn(II), Fe(III), Cu(II), Al(III), and many anions do not interfere with the Pd(II) determination. The proposed method was tested in the analysis of model solutions and successfully applied for the determination of palladium in catalyst. The obtained results show that this method can be used for serial determinations of palladium in various objects.


The Analyst ◽  
1997 ◽  
Vol 122 (3) ◽  
pp. 259-262 ◽  
Author(s):  
Takashi Hamano ◽  
Yukimasa Mitsuhashi ◽  
Nobumi Aoki ◽  
Masanori Semma ◽  
Yoshio Ito

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