Vacuum gas chromatography using short glass capillary columns combined with mass spectrometry

1978 ◽  
Vol 50 (8) ◽  
pp. 1164-1168 ◽  
Author(s):  
Frank W. Hatch ◽  
Milton E. Parrish
Keyword(s):  
Mass Spectrometry ◽  
Gas Chromatography ◽  
Capillary Columns ◽  
Glass Capillary ◽  
Glass Capillary Columns ◽  
Short Glass

Short Glass Micro-Packed Columns for Gas Chromatography

1994 ◽  
Vol 59 (3) ◽  
pp. 589-594
Author(s):  
Karel Komárek
Keyword(s):  
Gas Chromatography ◽  
Carboxylic Acids ◽  
Solid Phase ◽  
Chlorinated Hydrocarbons ◽  
Capillary Columns ◽  
Packed Columns ◽  
Glass Capillary ◽  
Porous Sorbent ◽  
Glass Capillary Columns ◽  
Short Glass

For a quick analysis of simple mixtures of lower chlorinated hydrocarbons a possible application has been studied of short glass micro-packed columns packed with commercial sorbents for extraction by solid phase. For analyses of lower alcohols, carboxylic acids, and other oxygen-containing substances the columns were packed with the organic porous sorbent, a copolymer of divinylbenzene and 1,4-di(methacryloyloxymethyl)naphthalene. The chosen sorbents were placed into glass capillary columns of 0.4 - 0.7 m length and 0.7 mm i.d. As the sorbent amount in the column is small, the columns are cheap. Whenever necessary, they can be prepared in any laboratory. The analyses of simple mixtures of above-mentioned classes of compounds lasted from 90 to 270 s.

High-temperature gas chromatography–mass spectrometry with glass capillary columns for the screening of natural products

2002 ◽  
Vol 947 (2) ◽  
pp. 255-265 ◽  
Author(s):  
Alberto dos Santos Pereira ◽  
Silvia Albero Carbonell ◽  
Francisco Radler de Aquino Neto ◽  
Ana Claudia Fernandes do Amaral ◽  
Roderick A Barnes
Keyword(s):  
Mass Spectrometry ◽  
Gas Chromatography ◽  
Natural Products ◽  
High Temperature ◽  
Capillary Columns ◽  
Gas Chromatography Mass Spectrometry ◽  
Glass Capillary ◽  
Chromatography Mass Spectrometry ◽  
Glass Capillary Columns ◽  
High Temperature Gas

Use of High-Resolution Open Tubular Glass Capillary Columns to Separate Acidic Metabolites in Urine

1975 ◽  
Vol 21 (7) ◽  
pp. 888-891 ◽  
Author(s):  
Brian A Knights ◽  
Mary Legendre ◽  
John L Laseter ◽  
James S Storer
Keyword(s):  
Mass Spectrometry ◽  
High Resolution ◽  
Capillary Columns ◽  
General Purpose ◽  
Gas Chromatography Mass Spectrometry ◽  
Glass Capillary ◽  
Glass Capillary Columns ◽  
Trimethylsilyl Derivatives ◽  
Derivatives Of ◽  
Urine Specimens

Abstract We used high-resolution glass capillary columns to study the trimethylsilyl derivatives of some acidic metabolites found in pooled urine specimens from control and postpartum subjects. About 30 compounds were identified by gas chromatography—mass spectrometry—computer techniques. In general, open tubular capillary columns effect better resolution of trimethylsilyl derivatives of organic acids than do conventional packed columns. GE SE-30 proved to be a good general-purpose stationary phase, whereas OV-17 offered certain advantages in resolving aromatic acid components.

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