Determination of the implantation-dose in silicon wafers by x-ray fluorescence analysis

1990 ◽  
Vol 62 (15) ◽  
pp. 1674-1676 ◽  
Author(s):  
Reinhold. Klockenkaemper ◽  
Maria. Becker ◽  
Henning. Bubert ◽  
Peter. Burba ◽  
Leopold. Palmetshofer
2020 ◽  
Vol 86 (10) ◽  
pp. 5-9
Author(s):  
D. G. Filatova ◽  
A. A. Arkhipenko ◽  
M. A. Statkus ◽  
V. V. Es’kina ◽  
V. B. Baranovskaya ◽  
...  

An approach to sorptive separation of Se (IV) from solutions on a novel S,N-containing sorbent with subsequent determination of the analyte in the sorbent phase by micro-x-ray fluorescence method is presented. The sorbent copolymethylenesulfide-N-alkyl-methylenamine (CMA) was synthesized using «snake in the cage» procedure and proven to be stable in acid solutions. Conditions for quantitative extraction of Se (IV) were determined: sorption in 5 M HCl or 0.05 M HNO3 solutions when heated to 60°C, phase contact time being 1 h. The residual selenium content in the solution was determined by inductively coupled plasma mass spectrometry (ICP-MS) using 82Se isotope. The absence of selenium losses is proved and the mechanism of sorption interaction under specified conditions is proposed. The method of micro-x-ray fluorescence analysis (micro-RFA) with mapping revealed a uniform distribution of selenium on the sorbent surface. The possibility of determining selenium in the sorbent phase by micro-RFA is shown. When comparing the obtained results with the results of calculations by the method of fundamental parameters, it is shown the necessity of using standard samples of sorbates to obtain correct results of RFA determination of selenium in the sorbent phase.


2010 ◽  
Vol 44 (1) ◽  
pp. 24-27 ◽  
Author(s):  
G. A. Bordovsky ◽  
A. V. Marchenko ◽  
P. P. Seregin ◽  
N. N. Smirnova ◽  
E. I. Terukov

2008 ◽  
pp. 615-615-13
Author(s):  
T Shiraiwa ◽  
T Ochiai ◽  
M Sano ◽  
Y Tada ◽  
T Arai

1993 ◽  
Vol 37 ◽  
pp. 697-709 ◽  
Author(s):  
Krassimir N. Stoev ◽  
Joseph F. Dlouhy

Nowadays x-ray fluorescence analysis is one of the major techniques for determination of trace elements. Vacuum operated Si (Li) .energy-dispersive x-ray spectrometers can analyze simultaneously up to 50 elements from Na (Z=11) to U (Z = 92) . Proper interpretation of the accumulated spectra requires correct solution of x-ray line overlap problems. In many cases knowledge of x-ray intensity ratios can make the procedure for resolving the overlapped peaks more reliable and reproducible. Measurements of radiative transition rates can also provide fundamental tests of theoretical atomic structure calculations. There are many other useful applications of x-ray emission rates in theoretical and experimental physics. On the other hand, there are differences in the published data, which suggests that x-ray intensity ratios are still not known with the necessary accuracy, and new measurements are useful and necessary.


Sign in / Sign up

Export Citation Format

Share Document