A novel approach to explore organochalcogen chemistry of tellurium based receptor for selective determination of silver ions in aqueous medium

Polyhedron ◽  
2017 ◽  
Vol 125 ◽  
pp. 238-245 ◽  
Author(s):  
Aman K.K. Bhasin ◽  
Jasminder Singh ◽  
Harjit Singh ◽  
Pushap Raj ◽  
Narinder Singh ◽  
...  
2001 ◽  
Vol 84 (2) ◽  
pp. 368-375 ◽  
Author(s):  
Mohammed Rizk ◽  
Fathalla Belal ◽  
Fawiza Ibrahim ◽  
Soad Ahmed ◽  
Zeinab A Sheribah

Abstract A derivative UV-spectrophotometric analytical procedure was developed for determination of three 4-quinolone antibacterials: norfloxacin (NFX), ciprofloxacin (CFX), and sparfloxacin (SFX). The method depends on the complexation of Cu(II) with the studied compounds in aqueous medium. A third order, measurement was applied for their quantification. A linear correlation was established between the amplitude of the peak and concentration for all the studied drugs in the range of 15–80, 35–120, and 200–700 ng/mL, with minimum detectability (S/N = 2) of 1.0, 1.3, and 5.1 ng/mL for NFX, CFX, and SFX, respectively. The method was successfully applied for accurate, sensitive, and selective determination of the studied drugs in bulk and tablets formulation with average percentage recoveries of 99.22 ± 0.55 to 100.33 ± 1.60. The results obtained were favorably compared with those of the reference method. The method was also used to determine sparfloxacin in spiked human plasma and urine. The results obtained were satisfactory, accurate, and precise.


Talanta ◽  
2015 ◽  
Vol 144 ◽  
pp. 619-626 ◽  
Author(s):  
Maryam Ebrahimi ◽  
Jahan Bakhsh Raoof ◽  
Reza Ojani

2018 ◽  
Vol 3 (27) ◽  
pp. 7792-7799 ◽  
Author(s):  
Meenakshi Verma ◽  
Amanpreet Kaur ◽  
Harpreet Kaur ◽  
Navneet Kaur ◽  
Narinder Singh

2019 ◽  
Vol 35 (2) ◽  
pp. 147-152 ◽  
Author(s):  
Yan Jun JU ◽  
Na LI ◽  
Shi Gang LIU ◽  
Yu Zhu FAN ◽  
Yu LING ◽  
...  

2010 ◽  
Vol 58 (22) ◽  
pp. 11883-11887 ◽  
Author(s):  
Manuela Curcio ◽  
Francesco Puoci ◽  
Giuseppe Cirillo ◽  
Francesca Iemma ◽  
Umile Gianfranco Spizzirri ◽  
...  

Author(s):  
Mark Morris ◽  
James Mohr ◽  
Esteban Ortiz ◽  
Steven Englebretson

Abstract Determination of metal bridging failures on plastic encapsulated devices is difficult due to the metal etching effects that occur while removing many of the plastic mold compounds. Typically, the acids used to remove the encapsulation are corrosive to the metals that are found within the device. Thus, decapsulation can result in removal of the failure mechanism. Mechanical techniques are often not successful due to damage that results in destruction of the die and failure mechanism. This paper discusses a novel approach to these types of failures using a silicon etch and a backside evaluation. The desirable characteristics of the technique would be to remove the silicon and leave typical device metals unaffected. It would also be preferable that the device passivation and oxides not be etched so that the failure location is not disturbed. The use of Tetramethylammonium Hydroxide (TMAH), was found to fit these prerequisites. The technique was tested on clip attached Schottky diodes that exhibited resistive shorting. The use of the TMAH technique was successful at exposing thin solder bridges that extruded over the edge of the die resulting in failure.


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