Growth, surface treatment and characterization of polycrystalline lead iodide thick films prepared using close space deposition technique

2012 ◽  
Vol 691 ◽  
pp. 10-15 ◽  
Author(s):  
Xinghua Zhu ◽  
Hui Sun ◽  
Dingyu Yang ◽  
Xiaolin Zheng
Keyword(s):  
Surface Treatment ◽  
Thick Films ◽  
Growth Surface ◽  
Deposition Technique ◽  
Lead Iodide

scholarly journals Microstructure and Thermoelectric Properties of (Bi0.48Sb1.52)Te3 Thick Films Prepared with Tape Casting Method

Electronics ◽  
2021 ◽  
Vol 10 (2) ◽  
pp. 140
Author(s):  
Lichen Liu ◽  
Ziping Cao ◽  
Min Chen ◽  
Jun Jiang
Keyword(s):  
Thermoelectric Properties ◽  
Low Cost ◽  
Thick Films ◽  
Tape Casting ◽  
Casting Process ◽  
Casting Method ◽  
Glass Substrates ◽  
Conductive Films ◽  
Casting Technology

This paper reports the fabrication and characterization of (Bi0.48Sb1.52)Te3 thick films using a tape casting process on glass substrates. A slurry of thermoelectric (Bi0.48Sb1.52)Te3 was developed and cured thick films were annealed in a vacuum chamber at 500–600 °C. The microstructure of these films was analyzed, and the Seebeck coefficient and electric conductivity were tested. It was found that the subsequent annealing process must be carefully designed to achieve good thermoelectric properties of these samples. Conductive films were obtained after annealing and led to acceptable thermoelectric performance. While the properties of these initial materials are not at the level of bulk materials, this work demonstrates that the low-cost tape casting technology is promising for fabricating thermoelectric modules for energy conversion.

scholarly journals Common Phase and Structure Misidentifications in High-Resolution TEM Characterization of Perovskite Materials

2020 ◽  
Vol 6 (1) ◽  
pp. 1
Author(s):  
Yu-Hao Deng
Keyword(s):  
High Resolution ◽  
Research Field ◽  
Structure Characterization ◽  
Phase Identification ◽  
Lead Iodide ◽  
Perovskite Materials ◽  
High Resolution Tem ◽  
Methylammonium Lead Iodide ◽  
Dose Imaging

High-resolution TEM (HRTEM) is a powerful tool for structure characterization. However, methylammonium lead iodide (MAPbI3) perovskite is highly sensitive to electron beams and easily decomposes into lead iodide (PbI2). Misidentifications, such as PbI2 being incorrectly labeled as perovskite, are widely present in HRTEM characterization and would negatively affect the development of perovskite research field. Here misidentifications in MAPbI3 perovskite are summarized, classified, and corrected based on low-dose imaging and electron diffraction (ED) simulations. Corresponding crystallographic parameters of intrinsic tetragonal MAPbI3 and the confusable hexagonal PbI2 are presented unambiguously. Finally, the method of proper phase identification and some strategies to control the radiation damage in HRTEM are provided. This warning paves the way to avoid future misinterpretations in HRTEM characterization of perovskite and other electron beam-sensitive materials.

scholarly journals Compositional, structural, and surface characterization of heat-treated halloysite samples: Influence of surface treatment on photochemical activity

2021 ◽  
Vol 212 ◽  
pp. 106222
Author(s):  
Balázs Zsirka ◽  
Veronika Vágvölgyi ◽  
Katalin Győrfi ◽  
Erzsébet Horváth ◽  
Róbert K. Szilágyi ◽  
...  
Keyword(s):  
Surface Treatment ◽  
Surface Characterization ◽  
Photochemical Activity ◽  
Heat Treated

Electrochemical characterization of YSZ thick films deposited by dip-coating process

2007 ◽  
Vol 171 (2) ◽  
pp. 783-788 ◽  
Author(s):  
F. Mauvy ◽  
P. Lenormand ◽  
C. Lalanne ◽  
F. Ansart ◽  
J.M. Bassat ◽  
...  
Keyword(s):  
Thick Films ◽  
Dip Coating ◽  
Electrochemical Characterization ◽  
Coating Process

Sol-gel preparation and characterization of transparent GdTaO 4 : Eu3+thick films

2008 ◽  
Author(s):  
Kun Han ◽  
Mu Gu ◽  
Xiaolin Liu ◽  
Chen Ni ◽  
Shiming Huang ◽  
...  
Keyword(s):  
Thick Films ◽  
Sol Gel ◽  
Gel Preparation

Development of crack free BLT thick films by chemical solution deposition technique

2015 ◽  
Vol 589 ◽  
pp. 686-691 ◽  
Author(s):  
Subir Roy ◽  
Rajalaxmi Maharana ◽  
Veena M ◽  
Atul Kumar ◽  
Sandip Bysakh ◽  
...  
Keyword(s):  
Chemical Solution Deposition ◽  
Thick Films ◽  
Chemical Solution ◽  
Deposition Technique ◽  
Solution Deposition

Preparation and characterization of Bi2Ti2O7 thin films by chemical solution deposition technique

2000 ◽  
Vol 370 (1-2) ◽  
pp. 30-32 ◽  
Author(s):  
XianMing Wu ◽  
Sh.W. Wang ◽  
H. Wang ◽  
Z. Wang ◽  
S.X. Shang ◽  
...  
Keyword(s):  
Thin Films ◽  
Chemical Solution Deposition ◽  
Chemical Solution ◽  
Deposition Technique ◽  
Solution Deposition

Characterization of layers produced by a reactive deposition technique: An EDAX and ESCA study

1987 ◽  
Vol 329 (2-3) ◽  
pp. 400-402
Author(s):  
K. Bange ◽  
G. Weinberg ◽  
S. Krause ◽  
K. Horn
Keyword(s):  
Deposition Technique ◽  
Reactive Deposition
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