The microstructure and magnetic properties of FeCo alloys with different OH¯/(Co2+, Fe2+) ratio and annealing temperature

Author(s):  
Meiyuan Ke ◽  
Tianfa Liao ◽  
Yunjie Jia ◽  
Hongbo Chen ◽  
Fujun Yang
2018 ◽  
Vol 941 ◽  
pp. 1324-1329 ◽  
Author(s):  
Shintaro Matai ◽  
Hibiki Sakakura ◽  
Mahoto Takeda

Numerous studies have been conducted to develop next-generation recording technology in spintronics. Because ultrafine magneitc particles are vital components of the technology, the interplay between the microsturcture and magnetic properties has attracted attention extensively in recent years. We focused on the relationship between the microstructure and magnetic properties of Cu-Ni-X (X=Fe, Co, FeCo) alloys comprising nanogranular magnetic particles. In this work, we prepared Cu-20 at% Ni-5 at% (FeCo), Cu-20 at% Ni-5 at% Fe, Cu-20 at% Ni-5 at% Co and examined the changes of microstructure and magnetic properties associated with heat treatments and composition. To examaine microstructural evolution of the alloy specimens, we conducted transmission electron microscope observations (TEM) with the as-quenched specimens and those aged at at 773-1073 K. We also carried out magneto-thermo gravimetry (MTG) measurements, superconducting quantum interference device (SQUID) measurements, magnetoresistance (MR) measurements and first-principles calculations based on the Koster-Korringa-Rostker (KKR) method with the Coherent Potential Approximation (CPA), to investigate the magnetic properties. The present work confirmed that the microstructure significantly changed, depending on the composition and heat treatment conditions. The present work also revealed that the magnetic properties closely correlated with the microstructure of samples.


1996 ◽  
Vol 11 (10) ◽  
pp. 2506-2517 ◽  
Author(s):  
Y. Xu ◽  
X. Yan

We studied composition, structure, microstructure, and magnetic properties of percolating (Ni–Fe)x(SiO2)1−x granular thin films. We found that the magnetic susceptibility increases and the coercivity decreases when increasing x toward xt, the critical metallic volume fraction for the metal-insulator transition, and the susceptibility decreases and the coercivity increases when increasing annealing temperature for x just below xt. Comparison of the microstructure and the magnetic properties suggests that the enhanced magnetic susceptibility for x just below xt is probably associated with the labyrinthine structure of the granular magnetic particles where there is an enhanced surface-to-volume ratio of the magnetic particles.


2016 ◽  
Vol 29 (8) ◽  
pp. 2035-2039
Author(s):  
Weiming Cheng ◽  
Shize Jiang ◽  
Wenchao Xu ◽  
Yajuan Hui ◽  
Haiwei Wang ◽  
...  

2007 ◽  
Vol 534-536 ◽  
pp. 1349-1352 ◽  
Author(s):  
Lian Xi Hu ◽  
Erde Wang ◽  
Bin Guo ◽  
Gang Shi

Nd2Fe14B/α-Fe nanocomposite powders with a nominal composition of Nd12Fe82B6 were prepared by HDDR combined with mechanical milling. The microstructure of both the as-disproportionated and the subsequently desorption-recombination annealed alloy powders was studied by Mössbauer spectrometry and TEM. The magnetic properties were investigated by VSM using bonded magnet samples. The results showed that the annealing temperature had significant influence on both the recombination kinetics and the grain size of the Nd2Fe14B/α-Fe nanocomposite phases, and the bonded magnet samples presented the best magnetic properties when the nanocomposite powders were prepared by annealing at 760°C for 30 min.


Sign in / Sign up

Export Citation Format

Share Document