scholarly journals Three-dimensional Investigation of Ceramic/Metal Heterophase Interfaces by Atom-probe Microscopy

2000 ◽  
Vol 6 (5) ◽  
pp. 445-451 ◽  
Author(s):  
Järg Rüsing ◽  
Jason T. Sebastian ◽  
Olof C. Hellman ◽  
David N. Seidman

AbstractThe results of a three-dimensional atom probe (3DAP) analysis, on a subnanometer scale, of a ceramic/metal heterophase interface, MgO/Cu, are presented. Segregation of Ag, from the Cu (Ag) matrix, at MgO/Cu interfaces is investigated and the Gibbsian interfacial excess of silver is determined; the range is 2.33 × 1018 to 5.81 × 1018 m−2. Also, silver segregation at the same MgO/Cu interfaces is analyzed employing a new approach that utilizes a proximity histogram or proxigram.

2003 ◽  
Vol 95 ◽  
pp. 199-205 ◽  
Author(s):  
Olof C. Hellman ◽  
John Blatz du Rivage ◽  
David N. Seidman

2002 ◽  
Vol 327 (1) ◽  
pp. 29-33 ◽  
Author(s):  
Olof Hellman ◽  
Justin Vandenbroucke ◽  
John Blatz du Rivage ◽  
David N Seidman

2012 ◽  
Vol 18 (2) ◽  
pp. 359-364 ◽  
Author(s):  
Peter J. Felfer ◽  
Baptiste Gault ◽  
Gang Sha ◽  
Leigh Stephenson ◽  
Simon P. Ringer ◽  
...  

AbstractAtom probe tomography (APT) provides three-dimensional analytical imaging of materials with near-atomic resolution using pulsed field evaporation. The processes of field evaporation can cause atoms to be placed at positions in the APT reconstruction that can deviate slightly from their original site in the material. Here, we describe and model one such process—that of preferential retention of solute atoms in multicomponent systems. Based on relative field evaporation probabilities, we calculate the point spread function for the solute atom distribution in the “z,” or in-depth direction, and use this to extract more accurate solute concentration profiles.


2009 ◽  
Vol 106 (7) ◽  
pp. 076102 ◽  
Author(s):  
Yasuo Shimizu ◽  
Yoko Kawamura ◽  
Masashi Uematsu ◽  
Kohei M. Itoh ◽  
Mitsuhiro Tomita ◽  
...  

2016 ◽  
Author(s):  
Emily M. Peterman ◽  
◽  
Steven Reddy ◽  
David W. Saxey ◽  
David R. Snoeyenbos ◽  
...  
Keyword(s):  

2021 ◽  
Vol 11 (1) ◽  
Author(s):  
Rui Zhai ◽  
Hui Chen ◽  
Zhihua Shan

AbstractElectrochemical modification of animal skin is a new material preparation method and new direction of research exploration. In this study, under the action of the electric field using NaCl as the supporting electrolyte, the effect of electrolysis on Glycyl-glycine(GlyGl), gelatin(Gel) and Three-dimensional rawhide collagen(3DC) were determined. The amino group of GlyGl is quickly eliminated within the anode region by electrolysis isolated by an anion exchange membrane. Using the same method, it was found that the molecular weight of Gel and the isoelectric point of the Gel decreased, and the viscosity and transparency of the Gel solution obviously changed. The electrolytic dissolution and structural changes of 3DC were further investigated. The results of TOC and TN showed that the organic matter in 3DC was dissolved by electrolysis, and the tissue cavitation was obvious. A new approach for the preparation of collagen-based multi-pore biomaterials by electrochemical method was explored.


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