Determination of pesticides and other physiologically active compounds by capillary gas chromatography with an atomic-emission detector without using standard reference materials

2000 ◽  
Vol 55 (1) ◽  
pp. 47-51
Author(s):  
A. S. Ponomarev ◽  
S. N. Shtykov
2009 ◽  
Vol 63 (5) ◽  
Author(s):  
Seiji Takahashi ◽  
Futoshi Nagamura ◽  
Miki Sasaki ◽  
Toshihiro Fujii

AbstractA surface ionization gas chromatographic detector, based upon positive surface ionization, was used in capillary gas chromatography to sensitively and selectively detect nitro pesticides: pendimethalin, trifluralin, flumetralin. Higher sensitivity (better detection limit), substance specificity, and advantageous applicability are reported. Sensitivity to pendimethalin, trifluralin, and flumetralin was 1.4 C g−1, 1.1 C g−1, and 1.0 C g−1, respectively, with the linear range of operation greater than 1 × 105 for these compounds. The minimum detectable level was in the range of 10−13 g s−1. Compared with an atomic emission detector, SID provided a 110 times better detection limit for trifluralin.


2010 ◽  
Vol 65 (8) ◽  
pp. 770-784 ◽  
Author(s):  
E. S. Chernetsova ◽  
A. I. Revel’skii ◽  
I. A. Revel’skii ◽  
Yu. A. Zolotov

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