Effects of austenitizing temperature and austenite grain size on the formation of athermal martensite in an iron-nickel and an iron-nickel-carbon alloy

1974 ◽  
Vol 5 (9) ◽  
pp. 2041-2046 ◽  
Author(s):  
M. Umemoto ◽  
W. S. Owen
2019 ◽  
Vol 944 ◽  
pp. 357-363
Author(s):  
Xiao Dong Zhang ◽  
Dian Xiu Xia ◽  
Shou Ren Wang

The effect of austenitizing temperature on the quenching microstructure and properties of 51CrV4 steel was studied. The results show that with the increase of austenitizing temperature, the austenite grains grow gradually. After quenching, the hardness increased first and then decreased, and the strength increased first and then decreased after tempering at 460°C. When the austenitizing temperature was 880°C, the austenite grains were fine and uniform, about 16μm, the martensite structure was dense, the strength and hardness reached maximum. When the austenitizing temperature was 910°C, the decarburization phenomenon was obvious, and the strength, hardness and plasticity of the test steel decreased obviously. When the austenitizing temperature exceeded 910°C, the austenite grains grow sharply and some grains were abnormally coarse. The austenite grain size reached 20μm and the microstructure was coarser at austenitizing temperature of 950°C. Therefore, in order to ensure uniform grain size and no decarburization under the premise of complete austenitization, the best austenitizing temperature of 51CrV4 steel for good properties is 880°C.


2013 ◽  
Vol 197 ◽  
pp. 53-57
Author(s):  
Grzegorz Golański ◽  
Cezary Kolan ◽  
Jerzy Kupczyk

The GX12CrMoVNbN9-1 (GP91) cast steel belongs to a new group of high-temperature creep resistant cast steels being introduced to the power industry. The cast steel is characterized by higher mechanical properties in comparison with the low alloy Cr – Mo or Cr – Mo – V cast steels used so far. The mechanical properties of martensitic cast steels depend on the parameters of heat treatment, such as the temperature of austenitizing. The paper is to present the results of research on the influence of austenitizing temperature ranging from 980 to 1100oC and hold time of 12 hours on the growth of austenite grain. The tests were carried out on test samples taken from a test coupon. Description of the influence of austenitizing temperature on the austenite grain size was made using the mean diameter of grain. Performed tests have shown that the distributions of mean diameters are of normal character, on the significance levels α = 0.05 and α = 0.04. For the investigated temperature range, the ν coefficient of non-homogeneity of the mean diameter of prior austenite grain was determined. The achieved results have proved that in the temperature range of 1010 to 1070°C the mean diameters stay within the same grade of grain size and the considerable grain growth is visible at the temperature of 1100°C.


Materials ◽  
2019 ◽  
Vol 12 (7) ◽  
pp. 1070 ◽  
Author(s):  
Chao Wang ◽  
Xin Wang ◽  
Jian Kang ◽  
Guo Yuan ◽  
Guodong Wang

Inclusion-induced acicular ferrite (AF) nucleation has been used for microstructure refinement in steel. Austenitization conditions have a significant influence on AF nucleation ability. In this paper, the effects of austenitization temperature and holding time on the transformation behaviors of low carbon steel containing Ti–Ca oxide particles were studied. A thermal treatment experiment, high temperature in situ observation, and calculation of Mn diffusion were carried out. The results indicate that small austenite grain size under low austenitizing temperature promoted grain boundary reaction products. With an increase in austenitizing temperature, the nucleation sites transferred to intragranular particles and AF transformation was improved. The inclusion particles in the Ti–Ca deoxidized steel were featured by an oxide core rich in Ti and a lesser amount of Ca and with MnS precipitation on the local surface, which showed a strong ability to promote AF nucleation. At a low austenitizing temperature, Mn diffusion was limited and the development of Mn-depleted zones (MDZs) around inclusions was not sufficient. The higher diffusion capacity of Mn at a high austenitizing temperature promoted the formation of MDZs to a larger degree and increased the AF nucleation ability. Boron segregation at large-sized austenite grain boundaries played an important role in AF transformation. Austenite grain size, Mn-depleted zone development, and boron segregation at grain boundaries were the decisive factors influencing the transformation behaviors under different austenitization conditions for the test steel.


Metals ◽  
2019 ◽  
Vol 9 (11) ◽  
pp. 1133 ◽  
Author(s):  
Zhang ◽  
Zhao ◽  
Tan ◽  
Ji ◽  
Xiang

The relationship between microstructure parameters and mechanical properties was studied in this paper. The steel was heat-treated at different austenitizing temperatures to acquire varying microstructure. The results showed that austenite grain size increases with austenitizing temperature, while the pearlite colony size was relatively constant. The strength followed a Hall–Petch relationship with the austenite grain size, but the austenite grain size has nothing to do with the impact toughness. The control unit for determining the impact toughness of pearlitic steel is the pearlite colony size using a comparison method. Further studies have found that, in the hypoeutectoid steel and hypereutectoid steel, the pearlite colony size changes with the austenitizing temperature. However, when the eutectoid steel with a carbon content of 0.81% undergoes the isothermal transformation, the number of grain boundary precipitates is very few. There are many nucleation sites at the grain boundary. The pearlite colonies randomly nucleate at the grain boundaries and grow into the interior of the grains. Simultaneously, new pearlite colonies nucleate by the side of the existing pearlite colony. The intragranular pearlite colonies are also randomly nucleated. These nucleation sites increase the chance of the growing pearlite colonies colliding with each other, eventually resulting in a constant pearlite colony size.


Metals ◽  
2021 ◽  
Vol 11 (2) ◽  
pp. 324
Author(s):  
David San-Martin ◽  
Matthias Kuntz ◽  
Francisca G. Caballero ◽  
Carlos Garcia-Mateo

This investigation explores the influence of the austenitisation heat treatment and thus, of the prior austenite grain size (PAGS), on the kinetics of the bainitic transformation, using as A case study two high-carbon, high-silicon, bainitic steels isothermally transformed (TIso = 250, 300, 350 °C), after being austenised at different temperatures (γTγ = 925–1125 °C). A methodology, based on the three defining dilatometric parameters extracted from the derivative of the relative change in length, was proposed to analyse the transformation kinetics. These parameters are related to the time to start bainitic transformation, the time lapse for most of the transformation to take place and the transformation rate at the end of the transformation. The results show that increasing the PAGS up to 70 µm leads to an increase in the bainite nucleation rate, this effect being more pronounced for the lowest TIso. However, the overall transformation kinetics seems to be weakly affected by the applied heat treatment (γTγ and TIso). In one of the steels, PAGS > 70 µm (γTγ > 1050 °C), which weakly affects the progress of the transformation, except for TIso = 250 °C, for which the enhancement of the autocatalytic effect could be the reason behind an acceleration of the overall transformation.


Materials ◽  
2021 ◽  
Vol 14 (8) ◽  
pp. 1988
Author(s):  
Tibor Kvackaj ◽  
Jana Bidulská ◽  
Róbert Bidulský

This review paper concerns the development of the chemical compositions and controlled processes of rolling and cooling steels to increase their mechanical properties and reduce weight and production costs. The paper analyzes the basic differences among high-strength steel (HSS), advanced high-strength steel (AHSS) and ultra-high-strength steel (UHSS) depending on differences in their final microstructural components, chemical composition, alloying elements and strengthening contributions to determine strength and mechanical properties. HSS is characterized by a final single-phase structure with reduced perlite content, while AHSS has a final structure of two-phase to multiphase. UHSS is characterized by a single-phase or multiphase structure. The yield strength of the steels have the following value intervals: HSS, 180–550 MPa; AHSS, 260–900 MPa; UHSS, 600–960 MPa. In addition to strength properties, the ductility of these steel grades is also an important parameter. AHSS steel has the best ductility, followed by HSS and UHSS. Within the HSS steel group, high-strength low-alloy (HSLA) steel represents a special subgroup characterized by the use of microalloying elements for special strength and plastic properties. An important parameter determining the strength properties of these steels is the grain-size diameter of the final structure, which depends on the processing conditions of the previous austenitic structure. The influence of reheating temperatures (TReh) and the holding time at the reheating temperature (tReh) of C–Mn–Nb–V HSLA steel was investigated in detail. Mathematical equations describing changes in the diameter of austenite grain size (dγ), depending on reheating temperature and holding time, were derived by the authors. The coordinates of the point where normal grain growth turned abnormal was determined. These coordinates for testing steel are the reheating conditions TReh = 1060 °C, tReh = 1800 s at the diameter of austenite grain size dγ = 100 μm.


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