Rapid determination of low concentrations of long-lived alpha-emitters in the atmosphere by alpha-spectrometry

1973 ◽  
Vol 13 (1) ◽  
pp. 235-246 ◽  
Author(s):  
R. Winkler ◽  
H. Hötzl
2004 ◽  
Vol 61 (2-3) ◽  
pp. 287-291 ◽  
Author(s):  
N Navarro ◽  
L Rodriguez ◽  
A Alvarez ◽  
C Sancho

1948 ◽  
Vol 26f (8) ◽  
pp. 318-330 ◽  
Author(s):  
Morris Katz ◽  
John Katzman

A granular form of silver permanganate on a zinc oxide carrier has been found to oxidize carbon monoxide in air at ordinary temperatures and at high space velocities. There is no noticeable change in activity over the range of 30 to 100% relative humidity of the air, although a small amount of water vapor is essential to initiate the combustion of carbon monoxide. The above properties have been utilized in the rapid determination of low concentrations by measuring the heat of oxidation in a thermocouple cell. The relation between the potential of the thermocouple junctions and the concentration of carbon monoxide is linear over the range of 0 to 600 p.p.m. at a definite space velocity. With increasing flow rate at a constant concentration the potential rises rapidly to a maximum, but in the range of optimum flow the flow rate may be varied considerably without producing a major change in e.m.f. The thermal efficiency is about 81% at the optimum flow rate. Hydrogen, unless it is present in amounts considerably in excess of the carbon monoxide concentration, does not introduce an appreciable error in the determination. The method is applicable to the field determination of considerably less than 0.005% carbon monoxide in air and the degree of precision is about equal to that of most laboratory methods. Twenty to twenty-five cubic centimeters of the material will give a useful life of over eight hours in continuous tests on concentrations below 0.1% carbon monoxide.


1977 ◽  
Vol 23 (10) ◽  
pp. 1893-1897 ◽  
Author(s):  
C P Price ◽  
B Llyod ◽  
G M Alberti

Abstract We describe an automated kinetic assay for acetoacetate in blood. Acetoacetate is enzymatically reduced to D-beta-hydroxybutyrate and the reaction is monitored for 60 s with a reaction-rate analyzer. This technique allows low concentrations of acetoacetate to be measured with good precision and overcomes many of the problems associated with other automated techniques. Our studies on the stability of acetoacetate emphasize the need for care in handling specimens. The use of a reaction-rate analyzer, an item of equipment common to most laboratories, allows for rapid handling of samples in small or large batches, depending on the needs of the laboratory.


1987 ◽  
Vol 59 (21) ◽  
pp. 2556-2558 ◽  
Author(s):  
Stephen. Donivan ◽  
Mark. Hollenbach ◽  
Mary. Costello

2021 ◽  
Author(s):  
Guillaume Blanchet-Chouinard ◽  
Dominic Larivière

A new sequential cloud point extraction (CPE) procedure was developed and validated for the determination of 210Pb and 210Po by ICP-MS/MS and alpha spectrometry, respectively. Two distinct CPE systems using...


2017 ◽  
Vol 171 ◽  
pp. 169-175 ◽  
Author(s):  
Lijuan Song ◽  
Yonggang Yang ◽  
Maoyi Luo ◽  
Yan Ma ◽  
Xiongxin Dai

1980 ◽  
Vol 26 (13) ◽  
pp. 1890-1895 ◽  
Author(s):  
B S Knox ◽  
J W McKee ◽  
P I Hair ◽  
J T France

Abstract We evaluated five quantitative, commercially available radioimmunoassay methods (Beta-Tec, BIO-RIA, Cambridge Nuclear, Mallinckrodt, and Serono) for rapid determination of the beta-subunit of human choriogonadotropin in serum or plasma. Only three of the kits (Beta-Tec, Mallinckrodt, and Serono) were found suitable for reliable determination of low concentrations of this analyte, which is of importance in the early diagnosis of trophoblastic disease in men and monitoring effectiveness of chemotherapy of trophoblastic tumors in men and women.


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