Rapid determination of 210Pb and 210Po by sequential cloud point extraction for environmental monitoring

2021 ◽  
Author(s):  
Guillaume Blanchet-Chouinard ◽  
Dominic Larivière

A new sequential cloud point extraction (CPE) procedure was developed and validated for the determination of 210Pb and 210Po by ICP-MS/MS and alpha spectrometry, respectively. Two distinct CPE systems using...

2009 ◽  
Vol 166 (3-4) ◽  
pp. 255-260 ◽  
Author(s):  
Matti Niemelä ◽  
Satu M. Huttunen ◽  
Stanislav S. Gornostayev ◽  
Paavo Perämäki

2014 ◽  
Vol 6 (23) ◽  
pp. 9291-9298 ◽  
Author(s):  
Charles Labrecque ◽  
Dominic Larivière

This article describes the development of a procedure for the bulk separation and determination of rare earth elements in soils by combining alkaline fusion, cloud point extraction, and inorganic mass spectrometry.


2015 ◽  
Vol 7 (16) ◽  
pp. 6732-6739 ◽  
Author(s):  
Guilong Peng ◽  
Qiang He ◽  
Guangming Zhou ◽  
Yong Li ◽  
Xiaoxuan Su ◽  
...  

A dual-cloud point extraction (d-CPE) technique combined with inductively coupled plasma mass spectrometry (ICP-MS) was used for preconcentration and determination of Cr, Ga, Ag, Cd, Mn, Fe, In, Cu, Ni, Co, Pb and Zn in real water samples.


ACS Omega ◽  
2021 ◽  
Author(s):  
Yongsheng Ji ◽  
Le Wu ◽  
Ruihong Lv ◽  
Haohao Wang ◽  
Shuhui Song ◽  
...  

2012 ◽  
Vol 95 (3) ◽  
pp. 845-849 ◽  
Author(s):  
Mohammad Mirzaei ◽  
Atieh Karimi Naeini ◽  
Mansoureh Behzadi

Abstract A simple and sensitive method has been developed for preconcentration and determination of genistein in soybeans. This method is based on cloud point extraction (CPE) of genistein from soybeans using ethylene glycol monoalkyl ether (Genapol X-080) as a nonionic surfactant. The concentration of extracted genistein was determined by HPLC with a UV detector. Optimum experimental conditions were established. With 5% Genapol X-080 (v/v), a liquid/solid ratio of 25:1 mL/g, and ultrasonic-assisted extraction at 40°C for 45 min, the extraction percentage of genistein reached its highest value. The preconcentration factor for genistein was about 16.5. The RSD for seven replicate measurements and the LOD were ±4.45% and 15.0 ng/mL, respectively. CPE is simple, inexpensive, and suitable for extraction of genistein from soybean. It uses environmentally friendly surfactants and offers a convenient alternative to more conventional extraction systems.


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