The titrimetric micro determination of sulphate using lead nitrate as titrant and dithizone as indicator

1959 ◽  
Vol 47 (2) ◽  
pp. 254-269 ◽  
Author(s):  
D. C. White
Keyword(s):  
Lead Nitrate

Volumetric Determination of Sulfate by Titration of Excess Lead Nitrate with Potassium Chromate Using Siloxene Indicator

1957 ◽  
Vol 29 (4) ◽  
pp. 543-546 ◽  
Author(s):  
Frederic. Kenny ◽  
R. B. Kurtz ◽  
Inge. Beck ◽  
Irena. Lukosevicius
Keyword(s):  
Lead Nitrate ◽  
Potassium Chromate ◽  
Excess Lead ◽  
Volumetric Determination

Determination of bezafibrate concentration by high performance liquid-chromatography in serum of rats treated with lead nitrate

Il Farmaco ◽  
1998 ◽  
Vol 53 (10-11) ◽  
pp. 690-692 ◽  
Author(s):  
Carlo Anchisi ◽  
Anna Maria Fadda ◽  
Anna Maria Maccioni ◽  
Sandra Dessı̀
Keyword(s):  
High Performance Liquid Chromatography ◽  
Liquid Chromatography ◽  
High Performance ◽  
Lead Nitrate

Automatic Potentiometric Titration of Sodium Sulfate in Certifiable Water-Soluble Colors

1974 ◽  
Vol 57 (2) ◽  
pp. 353-355
Author(s):  
John E Bailey ◽  
Charles Graichen
Keyword(s):  
Sample Preparation ◽  
Potentiometric Titration ◽  
Sodium Sulfate ◽  
Nitrate Solution ◽  
Lead Nitrate ◽  
Reference Electrode ◽  
Water Soluble ◽  
Automatic Titrator

Abstract A method has been developed for the automatic potentiometric titration of sulfate in water-soluble colors, which has the advantage of requiring little sample preparation and attention. A platinum indicating electrode is used with a coated silver reference electrode. The colors are dissolved in 75% alcohol. The sulfate is titrated with lead nitrate solution, using a Hiranuma recording automatic titrator. The method is applicable to the determination of sulfate in all sulfonated certifiable water-soluble colors except External D&C Green No. 1. It is not applicable to the determination of sulfate in the certifiable water-soluble fluorescein colors, namely, FD&C Red No. 3, D&C Orange No. 11, D&C Red No. 22, D&C Red No. 28, and D&C Yellow No. 8. The method is also not applicable to D&C Red No. 19. The

Determination of Lead in Aqueous and Organic Media by Atomic-Absorption Spectroscopy

1967 ◽  
Vol 21 (3) ◽  
pp. 160-164 ◽  
Author(s):  
Chuni L. Chakrabarti
Keyword(s):  
Aqueous Solution ◽  
Atomic Absorption ◽  
Absorption Spectroscopy ◽  
Atomic Absorption Spectroscopy ◽  
Lead Nitrate ◽  
Organic Media ◽  
Threefold Increase ◽  
Isopropyl Ketone ◽  
Ppm Level

The sensitivities of lead in aqueous and organic media by atomic-absorption spectroscopy using lead lines 2170 Å, 2833 A, and 4058 Å, and an oxy-hydrogen or oxy-acetylene flame were studied. When lead in aqueous solution was complexed as K2PbI6 and the complex extracted into methyl isopropyl ketone, a threefold increase in sensitivity relative to the aqueous solution of lead (as lead nitrate) was obtained. Using a 178-mm-long adapter on the top of a Beckman integral aspirator—burner (oxy-hydrogen), a sensitivity (in ppm/1% absorption) of 0.007 and a standard deviation of 0.014 ppm were obtained with a sample containing 0.1 ppm lead. Results obtained with oxy-hydrogen and oxy-acetylene flames have been discussed, and the precision and detection limits indicated. A procedure to determine lead in ppb—ppm level by extracting lead as K2PbI6 in methyl isopropyl ketone has been prescribed.

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