Use of rapid heating for decreasing the harmful influence of gas impregnation in heat treatment of VT23 alloy

1986 ◽  
Vol 21 (5) ◽  
pp. 498-500
Author(s):  
O. M. Ivasishin ◽  
S. P. Oshkaderov ◽  
V. M. Polatai
1998 ◽  
Vol 524 ◽  
Author(s):  
S. J. Doh ◽  
J. M. Lee ◽  
D. Y. Noh ◽  
J. H. Je

ABSTRACTThe surface-front oxidation mechanism of iron was investigated by time-resolved, glancingangle Fe K-edge fluorescence EXAFS measurements at various oxidation temperatures of 200-700 C. The glancing angle was chosen according to the depth of the oxide layer, roughly 1500-2000A. The oxidation behavior under rapid heating(up to 600°C within 10 minutes) was compared with the slowly heated oxidation process using the Quick-EXAFS measurements. In the slowly heated process, Fe3O4 was the dominating phase at a relatively low temperature (300-400 C) initially. However, at a relatively high temperature (above 600°C), the Fe2O3 and FeO crystalline phases are gradually enriched as the successive oxidation process involving intrusive oxygen proceeded. Remarkably under a prolonged heat treatment above 600°C, the stable FeO phase that exists in a deep-lying interface structure and Fe2O3 phase eventually dominates the thick front-surface structure. In a quickly heated process, however, Fe3O4 phase is less dominating, which is contradictory to the commonly accepted oxidation models. The EXAFS results are discussed in conjunction with the x-ray diffraction features under the same heat treatment conditions.


2016 ◽  
Vol 61 (3) ◽  
pp. 1663-1670
Author(s):  
A. Woźnicki ◽  
D. Leśniak ◽  
G. Włoch ◽  
P. Pałka ◽  
B. Leszczyńska-Madej ◽  
...  

AbstractThe influence of cooling rate after homogenization on the 2017A alloy microstructure was analysed. The capability of the θ (Al2Cu) particles, precipitated during various homogenization coolings, for rapid dissolution was estimated. For this purpose, the DSC test was used to determine the effect of the cooling rate after homogenization on the course of melting during a rapid heating. Moreover, the samples after solution heat treatment (with short time annealing) and ageing, were subjected to the microstructure investigations and the microhardness of grains interiors measurements. It was found that cooling after homogenization at 160 °C/h is sufficient for precipitation of fine θ phase particles, which dissolve during the subsequent rapid heating. The cooling at 40 °C/h, causes the precipitation of θ phase in the form of large particles, incapable of further fast dissolution.


2018 ◽  
Vol 11 (11) ◽  
pp. 5909-5920 ◽  
Author(s):  
Alex Mackay ◽  
Sam C. Lin ◽  
Lachlan S. Kenna ◽  
Alex F. Blackwood

Materials ◽  
2020 ◽  
Vol 13 (5) ◽  
pp. 1177 ◽  
Author(s):  
Yi-Ling Chang ◽  
Fei-Yi Hung ◽  
Truan-Sheng Lui

When hot forging 7075 aluminum alloy, as a military material durable enough for most of its applications, it needs to be heat-treated to ensure the target material property achieves the application requirements. However, the material properties change because of heat throughout usage. In this study, a new approach was devised to heat treat the alloy to prevent material property changes. The study further clarified the effect of rapid heat treatment on the high-temperature resistance of a hot forging 7075 aluminum alloy. Infrared (IR) heat treatment was used as a rapid heating technique to effectively replace the conventional resistance heat (RH) treatment method. Our experimental result showed that IR heat treatment resulted in better age hardening at the initial aging stage, where its tensile strength and elongation appeared like that of a resistance heat treatment. More so, based on hardness and tensile test results, the IR-heated treatment process inhibited the phase transformation of precipitations at a higher temperature, improving high-temperature softening resistance and enhancing the thermal stability of the hot forging 7075 aluminum alloy.


1991 ◽  
Vol 33 (12) ◽  
pp. 937-943
Author(s):  
M. Ya. Brun ◽  
A. I. Gordienko ◽  
L. A. Elagina ◽  
V. V. Ivashko

1953 ◽  
Vol 20 (2) ◽  
pp. 177-188 ◽  
Author(s):  
R. C. Wright ◽  
J. Tramer

1. Commercial samples of milk of Swiss origin, sterilized by rapid heating to high temperatures, developed a positive phosphatase reaction on storage.2. The optimum temperatures of storage for the development of this positive phosphatase reaction was 30° C.3. These commercial samples were sterile when received and remained sterile during storage.4. The developed phosphatase is apparently identical with the normal alkaline phosphatase of raw milk as judged by (a) heat stability, (b) pH optimum and rate of hydrolysis at different pHs, (c) comparison of results by Kay-Graham and Aschaffenburg & Mullen tests.


1992 ◽  
Vol 280 ◽  
Author(s):  
Paul C. Mclntyre ◽  
Michael J. Cima

ABSTRACTMicrostructure development in thin films of Ba2YCu3O7-x (BYC) synthesized on (001) LaA1O3 using an ex situ process was characterized by TEM and STEM examination of specimens quenched from different points in the growth heat treatment. The microchemistry of the growing oxide films was characterized by EDS in STEM. Phase development was also studied by X-ray diffraction. Several investigators have suggested that growth of BYC during ex situ processing occurs by nucleation and growth of BYC into an amorphous precursor film. Our observations indicate that this process involves growth into a substantially crystalline matrix. X-ray diffraction was used to identify three phases, BaF2, BaCuO2, and CuO, which are present prior to BYC nucleation. Nucleation of both c-axis normal and a-axis normal BYC occurred at approximately 760°C during rapid heating to 830°C in the growth heat treatment. Rapid growth of the c-axis normal material parallel to the substrate surface caused this orientation to become dominant in the fully converted films. Chemical microanalysis of the quenched films suggests that the BYC grows into an overlying layer that, after quenching, is composed of relatively large (25–100 nm diameter) yttrium- and copper-rich particles in a nanocrystalline barium-rich matrix.


Author(s):  
O.N. Perkov ◽  
I.A. Vakulenko ◽  
V.M Kuzmychov

The aim of this work is to study the basic principles of thermal cyclic processing (TCТ) of metals to obtain structures that determine the optimal complex of mechanical properties. The basic provisions of metal heating centers using periodically repeated heating and cooling cycles are given. The TCТ method, as a heat treatment method, is based on constant accumulation from cycle to cycle of positive changes in the structure of metals. Studies have shown that with rapid heating, the growth of austenitic grain occurs slowly and, therefore, heating to high temperatures (up to 10000C) does not lead to an intensive increase in grain. It has been established that grain size increases at a variable heating temperature 3 times slower than under isothermal conditions at the corresponding temperature. Provided that the growth rate of the new phase (austenite) is small and the nucleation rate of grains is significant, it turns out that by the end of the a®g transformation, a fine-grained structure is retained. Further heating or holding at a constant temperature leads to a rapid coarsening of austenite grains. If cooling (for example, in air) of rapidly heated steel is performed 10–150C higher than the temperature of the Ас1 point, then fine perlite grain is formed due to reverse recrystallization. With one thermal cycle, ferrite in subeutectoid steels almost does not undergo changes. But if several such heating and cooling are performed, then the entire ferrite-pearlite structure undergoes a change. It has been established that the higher the heating rate during heating and heating and the less overheating above Ас1, the finer the grain in carbon structural steel. However, this increases the need to increase the number of heat treatment cycles. The mechanism of structure formation explaining these phenomena and practical recommendations on the implementation of the process of the technical and economic process are presented. This approach makes it possible to form the optimal metal structure. At the same time, opportunities can be significantly expanded in terms of obtaining materials with desired properties and improving on this basis machines, structures, individual units and parts. All this puts TCТ in the category of promising areas in metalworking.


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