High-pressure liquid chromatographic techniques for the separation and quantification of norsesquiterpenes from gyrinids

1978 ◽  
Vol 4 (5) ◽  
pp. 503-510 ◽  
Author(s):  
Alexander T. Newhart ◽  
Ralph O. Mumma
1981 ◽  
Vol 64 (1) ◽  
pp. 54-57 ◽  
Author(s):  
David R Newkirk ◽  
Alan J Sheppard

Abstract A high pressure liquid chromatographic method that uses the benzoate ester of cholesterol has been developed for the measurement of cholesterol in foods. A 300 × 3.9 mm id μBondapak C18 column and a variable wavelength ultraviolet detector are used with a 100% methanol mobile phase. Amounts as low as 10 ng cholesterol benzoate can be detected. The results from the analyses of a variety of foods are given and compared with results from gas-liquid chromatographic analyses. The comparison of the 2 chromatographic techniques is favorable.


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