Crack propagation and failure prediction in silicon nitride at elevated temperatures

1974 ◽  
Vol 9 (2) ◽  
pp. 270-278 ◽  
Author(s):  
A. G. Evans ◽  
S. M. Wiederhorn
1975 ◽  
Vol 58 (11-12) ◽  
pp. 513-516 ◽  
Author(s):  
D. P. H. HASSELMAN ◽  
E. P. CHEN ◽  
C. L. AMMANN ◽  
J. E. DOHERTY ◽  
C. G. NESSLER

2005 ◽  
Vol 79 (10) ◽  
pp. 2789-2791 ◽  
Author(s):  
Shijie Zhu ◽  
Mineo Mizuno ◽  
Yasuo Nagano ◽  
Yutaka Kagawa ◽  
Makoto Watanabe

Author(s):  
Hiro Yoshida ◽  
Takashi Nakashima ◽  
Makoto Yoshida ◽  
Yasushi Hara ◽  
Toru Shimamori

A new high quality turbine system using monolithic silicon-nitride ceramic is under development. In this study particle impact tests of the silicon-nitride have been tried at room and elevated temperatures with and without tensile load, which simulates centrifugal force of blade rotation. In the experiment 1 mm diameter particle is impacted at velocities up to 900 m s−1. In this paper, critical velocities for bending fracture and Hertzian cracks are examined. Moreover, strength degradation at elevated temperature and spall fracture of the blade are discussed. The main results are: 1) The bending fracture mode critical impact velocity for soft particles is higher than that for hard particles. 2)The impact parameter ϕ for initiation of Hertzian cracks ranges 1.08×10−5 – 1.56×10−5 for the materials tested. 3)Strength degradation at elevated temperature was clearly observed. 4) In the impact tests on blades spall fracture, which was caused by interaction of stress waves, appeared.


1992 ◽  
Vol 100 (1158) ◽  
pp. 117-121 ◽  
Author(s):  
Satoshi IIO ◽  
Tomonori NIWA ◽  
Yo TAJIMA ◽  
Masakazu WATANABE

2005 ◽  
Vol 876 ◽  
Author(s):  
Gerald Ziegenbalg ◽  
Carsten Pätzold ◽  
Ute Ŝingliar ◽  
Rico Berthold

AbstractGas phase ammonolysis of volatile metal chlorides at elevated temperatures is a favorable way to produce nitride or oxynitride nanopowders. Their composition as well as the physico-chemical properties is determined by reaction temperature, molar ratio of the reactants and the residence time of the gases in the reaction zone. Both single and multi component powders can be obtained. Typical particle sizes are in the range of 50 to 350 nm. The specific surface can reach values up to 300 m2/g. Microporous analysis revealed the presence of pores with a diameter between 0.6 and 0.7 nm in amorphous silicon nitride. The powders can be used, depending on the characteristics, as catalyst or basic catalyst support. The paper gives an overview about vapor phase synthesis of single and multi component nitrides as well as the use of amorphous silicon nitride as a basic catalyst support for dehydrogenation of propane.


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