Quantitative determination of titanium dioxide in cellulose acetate spinning solutions

1990 ◽  
Vol 21 (6) ◽  
pp. 516-517
Author(s):  
G. E. Konovalova ◽  
S. Z. Rosina ◽  
R. A. Muminova ◽  
Yu. T. Tashpulatov
1984 ◽  
Vol 49 (1) ◽  
pp. 253-266 ◽  
Author(s):  
Jan Novrocík ◽  
Marta Novrocíková ◽  
Jiří Norek ◽  
Ivan Koruna ◽  
Miroslav Ryska

Using synthetic, chromatographic and spectral methods, we studied the side reactions accompanying the preparation of di-2-ethylhexyl phthalate from phthalic anhydride and 2-ethyl-hexane-1-ol in the presence of catalytic amounts of tetra-n-butyl titanate.The catalyst proper was titanium(IV) mono-2-ethylhexyl phthalate. The possibility of a simultaneous gas-chromatographic quantitative determination of mono-2-ethylhexyl phthalate, di-2-ethylhexyl phthalate, 2-ethylhexane-1-ol and tetra-n-butyl titanate, reported in the literature, has been refuted. In the esterification catalysed by hydrated titanium dioxide homogeneous catalysis by the formed organotitanate was dominating. The dissolving of hydrated titanium dioxide in the esterification of phthalic anhydride with 2-ethylhexane-1-ol was studied polarographically.


1972 ◽  
Vol 18 (3) ◽  
pp. 237-238 ◽  
Author(s):  
M C B Pizzolato ◽  
M A Pizzolato ◽  
A Agostoni

Abstract A simple method is described for quantitative determination of IgG, IgA, IgM, α2M, and other proteins without dilution of the sample. Strips of gelatinized cellulose acetate spread with antiserum are used as a supporting medium. The method is accurate, highly reproducible, and seems particularly suitable for routine work because it permits determination of hypo-, normal, and hyperglobulinemia on a single strip.


1973 ◽  
Vol 56 (3) ◽  
pp. 535-537 ◽  
Author(s):  
Joseph L Leone

Abstract A quantitative, colorimetric procedure for the determination of titanium dioxide has been subjected to collaborative study. The method incorporates ashing, dissolution of the ash in sulfuric acid, and color development using hydrogen peroxide. The Spectrophotometric response is compared to a standard prepared similarly. The yellow-to-orange color is quite stable in the absence of Fe. Other interferences are Ni, Cu, Co, Mb, Vd, and Cr. A collaborative study of cheese containing 0.05, 0.10, and 0.4% titanium dioxide gave favorable results. The method has been adopted as official first action.


1999 ◽  
Vol 96 (9/10) ◽  
pp. 1608-1615
Author(s):  
T. E. Malliavin ◽  
H. Desvaux ◽  
M. A. Delsuc

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