Low-temperature synthesis and characterization of ceria-based oxide ion conductors

1996 ◽  
Vol 31 (19) ◽  
pp. 5005-5007 ◽  
Author(s):  
A. K. Bhattacharya ◽  
A. Hartridge ◽  
K. K. Mallick ◽  
J. L. Woodhead
Keyword(s):  
Low Temperature ◽  
Synthesis And Characterization ◽  
Low Temperature Synthesis ◽  
Temperature Synthesis ◽  
Oxide Ion Conductors ◽  
Oxide Ion ◽  
Ion Conductors

scholarly journals Low temperature synthesis and characterization of Mn3O4 nanoparticles

2007 ◽  
Vol 5 (1) ◽  
pp. 169-176 ◽  
Author(s):  
Abdülhadi Baykal ◽  
Yüksel Köseoğlu ◽  
Mehmet Şenel
Keyword(s):  
Particle Size ◽  
Infrared Spectroscopy ◽  
Low Temperature ◽  
Synthesis And Characterization ◽  
Low Temperature Synthesis ◽  
Temperature Synthesis ◽  
X Ray ◽  
Peak Broadening ◽  
Mn3o4 Nanoparticles

AbstractHeating hydrous manganese (II) hydroxide gel at 85 °C for 12 hours produces Mn3O4 nanoparticles. They were characterized by X-ray powder diffraction (XRD) and infrared spectroscopy (FTIR). The particle size estimated from the SEM and X-ray peak broadening is approximately 32 nm, showing them to be nanocrystalline. EPR measurements confirm a typical Mn2+signal with a highly resolved hyperfine structure.

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