[BeBr2(SMe2)2], a Versatile Starting Material for Beryllium Chemistry – One Pot Synthesis from Beryllium Powder

2006 ◽  
Vol 632 (12-13) ◽  
pp. 2021-2023 ◽  
Author(s):  
Daniel Himmel ◽  
Ingo Krossing
2019 ◽  
Vol 15 ◽  
pp. 2840-2846
Author(s):  
Valeriya G Melekhina ◽  
Andrey N Komogortsev ◽  
Boris V Lichitsky ◽  
Vitaly S Mityanov ◽  
Artem N Fakhrutdinov ◽  
...  

The condensation of primary amines with N-(1-(4-hydroxy-6-methyl-2-oxo-2H-pyran-3-yl)-2-oxo-2-arylethyl)acetamides was explored. Thus, a previously unknown recyclization of the starting material was observed in acidic ethanol in the presence of an amine, which provided the corresponding dihydropyrrolone derivative as the major reaction product. Based on this transformation, a practical and convenient one-pot synthetic method for substituted pyrrolo[3,4-b]pyridin-5-ones could be devised.


2013 ◽  
Vol 830 ◽  
pp. 222-225
Author(s):  
Hai Xin Ding ◽  
Si Liu ◽  
Shan Shan Gong ◽  
Qi Sun

P1,P2-Diaciclovir-5'-diphosphate has been synthesized efficiently from aciclovir 5'-H-phosphonate monoester via a one-pot reaction. This method features easily accessibleH-phosphonate starting material, short reaction time, and good isolated yield.


Heterocycles ◽  
1981 ◽  
Vol 16 (1) ◽  
pp. 151 ◽  
Author(s):  
Zen-ichi Yoshida ◽  
Shegeo Yoneda ◽  
Hideo Hirai ◽  
Etsuro Seki

2017 ◽  
Vol 41 (10) ◽  
pp. 581-585 ◽  
Author(s):  
Hao Yang ◽  
Yifan Ouyang ◽  
Yutong Sun ◽  
Zhe Wang ◽  
Xuanli Zhu ◽  
...  

An efficient one-pot synthesis of 1-(4-bromophenyl)-1 H-tetrazol-5-amine was performed using 4-bromoaniline as the starting material. A novel and widely applicable amidation procedure was then employed, whereby 1-(4-bromophenyl)-1 H-tetrazol-5-amine was acylated with different acyl chlorides in the presence of lithium bis(trimethylsilyl)amide as catalyst, for the high-yield synthesis of [1-(4-bromophenyl)-1 H-tetrazol-5-yl]amide derivatives.


2020 ◽  
Author(s):  
Lucien Caspers ◽  
Julian Spils ◽  
Mattis Damrath ◽  
Enno Lork ◽  
Boris Nachtsheim

In this article we describe an efficient approach for the synthesis of cyclic diaryliodonium salts. The method is based on benzyl alcohols as starting materials and consists of an Friedel-Crafts-arylation/oxidation sequence. Besides a deep optimization, particluar focusing on the choice and ratios of the utilized Bronsted-acids and oxidants, we explore the substrate scope of this transformation. We also discuss an interesting isomerism of cyclic iodonium salts substituted with aliphatic substituents at the bridge head carbon. <br>


2017 ◽  
Vol 7 (12) ◽  
pp. 1192-1195
Author(s):  
Y. I. Shaikh ◽  
G. M. Nazeruddin ◽  
Khursheed Ahmed

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