Microwave‐Assisted/Pd‐Catalyzed Domino Synthesis of 2,3,4‐Triiodoanisole from 3‐Anisic Acid: A Superior Substrate for Regioselective Synthesis of 2,3‐Diiodobiphenyls

2020 ◽  
Vol 5 (9) ◽  
pp. 2848-2853
Author(s):  
Raed M. Al‐Zoubi ◽  
Walid K. Al‐Jammal ◽  
Robert McDonald
2010 ◽  
Vol 40 (11) ◽  
pp. 1631-1638 ◽  
Author(s):  
Sarika Malik ◽  
Upender K. Nadir ◽  
Pramod S. Pandey

2007 ◽  
Vol 18 (5) ◽  
pp. 1061-1067 ◽  
Author(s):  
Guirong Qu ◽  
Zhiguang Zhang ◽  
Haiming Guo ◽  
Mingwei Geng ◽  
Ran Xia

2006 ◽  
Vol 84 (5) ◽  
pp. 819-824 ◽  
Author(s):  
Guirong Qu ◽  
Suhui Han ◽  
Zhiguang Zhang ◽  
Mingwei Geng ◽  
Feng Xue

An efficient and green procedure for the synthesis of purine acyclic nucleosides through microwave-assisted alkylation of various purine nucleobases with 2-oxa-1,4-butanediol diacetate in the absence of solvent and catalyst is described. The advantages of using this method include its environmental friendliness, simple manipulation, short reaction time, high regioselectivity, and good yields.Key words: acyclic nucleosides, microwave irradiation, regioselectivity, alkylation, 2-oxa-1,4-butanediol diacetate.


RSC Advances ◽  
2016 ◽  
Vol 6 (15) ◽  
pp. 12402-12407 ◽  
Author(s):  
Soumen Payra ◽  
Arijit Saha ◽  
Subhash Banerjee

Here, we have demonstrated regioselective synthesis of novel 2-alkoxy-3-arylimidazo[1,2-a]pyridines using nano-NiFe2O4 as reusable catalyst via one-pot sequential aza-Michael addition, Fe-promoted ligand transfer and C–H imination reactions.


2019 ◽  
Vol 17 (40) ◽  
pp. 8982-8986
Author(s):  
Kate Lauder ◽  
Domiziana Masci ◽  
Anita Toscani ◽  
Aya Al Mekdad ◽  
Gary W. Black ◽  
...  

A microwave assisted multicomponent protocol on water allows the regioselective synthesis of chiral aryl-1,2-mercaptoamines. The enzymatic resolution of the racemates leads to enantioenriched products.


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