Plastic deformation of selenium single crystals ina glide and X-ray observation of the induced substructure

1976 ◽  
Vol 36 (2) ◽  
pp. 461-470 ◽  
Author(s):  
J. L. Farvacque ◽  
J. C. Doukhan ◽  
B. Escaig ◽  
T. Tuomi
2005 ◽  
Vol 105 ◽  
pp. 207-212
Author(s):  
Yuriy Perlovich ◽  
Margarita Isaenkova ◽  
Vladimir Fesenko ◽  
Hans Joachim Bunge

The substructure inhomogeneity of rolled Ti-48%Ni-2%Fe single crystals was studied by the X-ray method of Generalized Pole Figures. Under rolling of single crystals, along with texture formation, the nonuniform substructure develops. It is conditioned by inhomogeneous reorientation of the crystalline lattice and local differences in predominant plastic deformation mechanisms. The distribution of residual deformation effects is controlled by the orientation of separate regions relative to texture maxima. Rolled single crystals prove to be divided into subcomponents with close orientations and opposite signs of elastic microstrains.


1957 ◽  
Vol 35 (1) ◽  
pp. 38-47 ◽  
Author(s):  
G. B. Craig ◽  
B. Chalmers

The tensile plastic deformation of single-crystal and tricrystal specimens of zinc was investigated by analysis of the external change in shape of the specimens, and of the changes in X-ray diffraction patterns. It was demonstrated that the single crystals deformed by slip on the basal plane, but pyramidal as well as basal slip occurred in specimens containing grain boundaries.


1998 ◽  
Vol 31 (1-2) ◽  
pp. 53-84 ◽  
Author(s):  
Yu. Perlovich ◽  
H. J. Bunge ◽  
M. Isaenkova ◽  
V. Fesenko ◽  
R. Rustamov

Rolled single crystals of the alloy Ti–48%Ni–2%Fe were studied by methods of X-ray diffractometry using a PSD-technique. Single crystals, consisting of the phase B2, were rolled in 11 initial orientations at 350°C with deformation degrees up to ~80%. Texture development in single crystals under rolling was analyzed to determine the acting mechanisms of plastic deformation. Three stable orientations of single crystals were found: {011}〈011〉 ,{111}〈011〉 and {111}〈112〉. It was shown on the basis of texture data, that Ti–Ni single crystals deform by means of combined action of slip in the systems {011}〈001〉 and twinning. For the first time, along with twinning in the known systems {114}〈221〉 , twinning in the systems {118}〈441〉 was revealed. A number of concrete cases was considered to refine the contributions of slip and twinning into reorientation of single crystals depending on their initial orientations as well as to ascertain the interrelation of different mechanisms.


The variation of plastic deformation in aluminium specimens consisting of large crystals has been determined by measuring elongation and hardness at various points after tensile deformation. The deformation varied from grain to grain, and also within each grain the deformation near the boundary was greater or smaller than at the centre according to whether the neighbour was more or less deformed, i. e. there is not necessarily inhibition of slip near grain boundaries. These results were supported by metallographic and X-ray observations. Their importance with respect to the calculation of the stress-strain curve of aggregates from those of single crystals is discussed. It is suggested that a mechanism other than slip operates near the grain boundaries during deformation, and even within the crystals during large extensions.


Author(s):  
M.T. Otten ◽  
P.R. Buseck

ALCHEMI (Atom Location by CHannelling-Enhanced Microanalysis) is a TEM technique for determining site occupancies in single crystals. The method uses the channelling of incident electrons along specific crystallographic planes. This channelling results in enhanced x-ray emission from the atoms on those planes, thereby providing the required site-occupancy information. ALCHEMI has been applied with success to spinel, olivine and feldspar. For the garnets, which form a large group of important minerals and synthetic compounds, the channelling effect is weaker, and significant results are more difficult to obtain. It was found, however, that the channelling effect is pronounced for low-index zone-axis orientations, yielding a method for assessing site occupancies that is rapid and easy to perform.


Author(s):  
M.A. Mogilevsky ◽  
L.S. Bushnev

Single crystals of Al were loaded by 15 to 40 GPa shock waves at 77 K with a pulse duration of 1.0 to 0.5 μs and a residual deformation of ∼1%. The analysis of deformation structure peculiarities allows the deformation history to be re-established.After a 20 to 40 GPa loading the dislocation density in the recovered samples was about 1010 cm-2. By measuring the thickness of the 40 GPa shock front in Al, a plastic deformation velocity of 1.07 x 108 s-1 is obtained, from where the moving dislocation density at the front is 7 x 1010 cm-2. A very small part of dislocations moves during the whole time of compression, i.e. a total dislocation density at the front must be in excess of this value by one or two orders. Consequently, due to extremely high stresses, at the front there exists a very unstable structure which is rearranged later with a noticeable decrease in dislocation density.


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