Colorimetric Determination of Acetyl Sulfisoxazole in the Presence of Its Hydrolysis Products, Sulfisoxazole and Acetic Acid

1971 ◽  
Vol 60 (11) ◽  
pp. 1696-1698 ◽  
Author(s):  
Joseph A. Feldman ◽  
Vishnu U. Patel
Keyword(s):  
Acetic Acid ◽  
Colorimetric Determination ◽  
Hydrolysis Products

Conductometric and Colorimetric Determination of Volatile Acidity of Vinegars by Flow-Injection Analysis

1991 ◽  
Vol 74 (2) ◽  
pp. 346-350 ◽  
Author(s):  
Matthieu Tubino ◽  
Flavio G Barros
Keyword(s):  
Acetic Acid ◽  
Colorimetric Determination ◽  
Bromocresol Purple ◽  
Water Stream ◽  
Ptfe Membrane ◽  
Volatile Acidity ◽  
Relative Standard ◽  
Significant Difference ◽  
Membrane Separator

Abstract Recent methods for determination of the volatile acidity of vinegars are relatively slow (about 40 mln) and involve techniques subject to a variety of errors (ca 2.5%). The present paper describes a method that provides results in a shorter time (ca 2 mln, Including dilution), with a smaller relative error rate (ca 1%). Conductometric analysis consists of the Injection of the sample In a deionlzed water stream that then flows past a PTFE membrane separator. Acetic acid diffuses through the membrane to another deionlzed water stream that passes through a conductivity cell. Colorimetric analysis also consists of sample injection into a deionlzed water stream that passes through the same PTFE membrane separator. However, the acetic acid diffuses into a bromocresol purple solution stream at pH 7. This solution passes through a flow cell In a spectrophotometer set at 540 nm. Before injection, samples were treated with hydrogen peroxide to ensure complete oxidation of sulfite to sulfate. Results of the proposed method were also compared with another similar method. At a 95% confidence level, the statistical t-test Indicates no significant difference between them. Typical estimates of the relative standard deviations obtained with the new methods are ca 1%. Analyses were performed with red and white wine vinegars.

Effects of Tomatine on the Colorimetric Determination of Cholesterol by the Zak Procedure

1967 ◽  
Vol 13 (6) ◽  
pp. 468-474 ◽  
Author(s):  
Cleamond D Eskelson ◽  
Arthur L Dunn ◽  
Clarence R Cazee
Keyword(s):  
Acetic Acid ◽  
Free Cholesterol ◽  
Colorimetric Determination ◽  
Acid Reagent ◽  
Standard Solution

Abstract The iron-acetic acid reagent used for cholesterol determinations produces a color with tomatine, which is reported to be a more specific precipitant for cholesterol. To circumvent the interferen:e of tomatine found in a cholesterol-tomatinide complex, a standard solution containing stoichiometric amounts of tomatine and cholesterol was used and proved to be reliable for the determination of free cholesterol in serum.

Colorimetric Determination of Thymol and Eugenol in Volatile Oils

1978 ◽  
Vol 61 (1) ◽  
pp. 169-171
Author(s):  
Mohamed A Korany ◽  
Nabil Abdel-Salam ◽  
Mohamed Abdel-Salam
Keyword(s):  
Acetic Acid ◽  
Sodium Hydroxide Solution ◽  
Colorimetric Method ◽  
Aqueous Acetic Acid ◽  
Colorimetric Determination ◽  
Clove Oil ◽  
Volatile Oils ◽  
Thyme Oil ◽  
Yellow Color

Abstract A colorimetric method for determining thymol and eugenol in volatile oils is presented. Thymol and eugenol are reacted with sodium cobaltinitrite in aqueous acetic acid. The yellow color produced is measured at 330 and 370 nm in chloroform, and at 396 and 450 nm in sodium hydroxide solution for thymol and eugenol, respectively. The method is applied to the assay of thyme oil (thymol type) and clove oil. The results obtained are reasonably reproducible with a coefficient of variation less than 2%.

Colorimetric determination of ethylenediaminetetra-acetic acid in foods

1985 ◽  
Vol 180 (4) ◽  
pp. 280-283 ◽  
Author(s):  
Takashi Hamano ◽  
Yukimasa Mistuhashi ◽  
Kisaku Tanaka ◽  
Yukio Matsuki ◽  
Yoshikiyo Oji ◽  
...  
Keyword(s):  
Acetic Acid ◽  
Colorimetric Determination

A Method for the Colorimetric Determination of β-Glucuronidase in Urine, Serum, Tissue; Assay of Enzymatic Activity in Health and Disease

1959 ◽  
Vol 36 (2) ◽  
pp. 193-201 ◽  
Author(s):  
Julius A. Goldbarg ◽  
Esteban P. Pineda ◽  
Benjamin M. Banks ◽  
Alexander M. Rutenburg
Keyword(s):  
Enzymatic Activity ◽  
Colorimetric Determination ◽  
Health And Disease ◽  
Urine Serum

Colorimetric Determination of Fluoride in Drinking Groundwater using a Polymeric Zirconium Complex of 5-(2-Carboxyphenylazo)-8-Hydroxyquinoline

2013 ◽  
Vol 12 (7) ◽  
pp. 460-465
Author(s):  
Sameer Amereih ◽  
Zaher Barghouthi ◽  
Lamees Majjiad
Keyword(s):  
Drinking Water ◽  
Detection Limit ◽  
Complex Formation ◽  
Molar Absorptivity ◽  
Colorimetric Determination ◽  
Zirconium Complex ◽  
Reliable Determination ◽  
Percentage Recovery ◽  
Quantitation Limit

A sensitive colorimetric determination of fluoride in drinking water has been developed using a polymeric zirconium complex of 5-(2-Carboxyphenylazo)-8-Hydroxyquinoline as fluoride reagents. The method allowed a reliable determination of fluoride in range of (0.0-1.5) mg L-1. The molar absorptivity of the complex formation is 7695 ± 27 L mol-1 cm-1 at 460 nm. The sensitivity, detection limit, quantitation limit, and percentage recovery for 1.0 mg L-1 fluoride for the proposed method were found to be 0.353 ± 0.013 μg mL-1, 0.1 mg L-1, 0.3 mg L-1, and 101.7 ± 4.1, respectively.

Colorimetric Determination of Amoxicillin in Pure and some Pharmaceutical Formulations Via Reaction with Potassium Permanganate as Oxidant Reagent

2019 ◽  
Vol 10 (02) ◽  
Author(s):  
Abbas Shebeeb Al-kadumi ◽  
Sahar Rihan Fadhel ◽  
Mohammed Abdullah Ahmed ◽  
Luma Amer Musa
Keyword(s):  
Potassium Permanganate ◽  
Pharmaceutical Preparations ◽  
Pharmaceutical Formulations ◽  
Atomic Emission ◽  
Basic Medium ◽  
Photometric Method ◽  
Colorimetric Determination ◽  
Spectrophotometric Methods ◽  
Label Claim

We proposed two simple, rapid, and convenient spectrophotometric methods are described for the determination of Amoxicillin in bulk and its pharmaceutical preparations. They are based on the measurement of the flame atomic emission of potassium ion (in first method) and colorimetric determination of the green colored solution for manganite ion at 610 nm formed after reaction of Amoxicillin with potassium permanganate as oxidant agent (in the second method) in basic medium. The working conditions of the methods were investigated and optimized. Beer's law plot showed a good correlation in the concentration range of 5-45 μg/ml. The detection limits and relative standared deviations were (2.573, 2.814 μg/ml) (2.137, 2.498) for the flame emission photometric method and (1.844, 2.016 μg/ml) (1.645,1.932) for colorimetric methods for capsules and suspensions respectively. The methods were successfully applied to the determination of Amoxicillin in capsules and suspensions, and the obtained results were in good agreement with the label claim. No interference was observed from the commonly encountered additives and expectancies.

Sign in / Sign up

Export Citation Format

Share Document