ChemInform Abstract: Microwave-Assisted Direct Oxidative Synthesis of α-Ketoamides from Aryl Methyl Ketones and Amines by a Water Soluble Cu(I)-Complex.

ChemInform ◽  
2016 ◽  
Vol 47 (41) ◽  
Author(s):  
Shalini Nekkanti ◽  
Karuna Veeramani ◽  
Niggula Praveen Kumar ◽  
Nagula Shankaraiah
Keyword(s):  
Water Soluble ◽  
Methyl Ketones ◽  
Microwave Assisted ◽  
Aryl Methyl

Microwave-assisted direct oxidative synthesis of α-ketoamides from aryl methyl ketones and amines by a water soluble Cu(i)-complex

2016 ◽  
Vol 18 (11) ◽  
pp. 3439-3447 ◽  
Author(s):  
Shalini Nekkanti ◽  
Karuna Veeramani ◽  
Niggula Praveen Kumar ◽  
Nagula Shankaraiah
Keyword(s):  
Water Soluble ◽  
Methyl Ketones ◽  
Microwave Assisted ◽  
Aryl Methyl

A stable and isolable Cu(i) complex has been identified for the direct oxidative synthesis of α-ketoamides in water.

Microwave-assisted selenium dioxide oxidation of aryl methyl ketones to aryl glyoxals

2011 ◽  
Vol 52 (31) ◽  
pp. 4036-4038 ◽  
Author(s):  
Ryan M. Young ◽  
Michael T. Davies-Coleman
Keyword(s):  
Selenium Dioxide ◽  
Methyl Ketones ◽  
Microwave Assisted ◽  
Aryl Methyl

scholarly journals One-Pot Microwave-Assisted Synthesis of Water-Soluble Pyran-2,4,5-triol Glucose Amine Schiff Base Derivative: XRD/HSA Interactions, Crystal Structure, Spectral, Thermal and a DFT/TD-DFT

Crystals ◽  
2021 ◽  
Vol 11 (2) ◽  
pp. 117
Author(s):  
Yousef Hijji ◽  
Rajeesha Rajan ◽  
Hamdi Ben Yahia ◽  
Said Mansour ◽  
Abdelkader Zarrouk ◽  
...  
Keyword(s):  
Schiff Base ◽  
Molecular Orbital ◽  
Density Functional ◽  
Condensation Reaction ◽  
3D Structure ◽  
Water Soluble ◽  
Microwave Assisted Synthesis ◽  
One Pot ◽  
Microwave Assisted ◽  
Td Dft

The(3R,4R,6R)-3-(((E)-2-hydroxybenzylidene)amino)-6-(hydroxymethyl)tetrahydro-2H-pyran-2,4,5-triol water-soluble Glucose amine Schiff base (GASB-1) product was made available by condensation of 2-hydroxybenzaldehyde with (3R,6R)-3-amino-6-(hydroxymethyl)-tetra-hydro-2H-pyran-2,4,5-triol under mono-mode microwave heating. A one-pot 5-minute microwave-assisted reaction was required to complete the condensation reaction with 90% yield and without having byproducts. The 3D structure of GASB-1 was solved from single crystal X-ray diffraction data and computed by DFT/6-311G(d,p). The Hirshfeld surface analysis (HSA), molecular electronic potential (MEP), Mulliken atomic charge (MAC), and natural population analysis (NPA) were performed. The IR and UV-Vis spectra were matched to their density functional theory (DFT) relatives and the thermal behavior was resolved in an open-room condition via thermogravimetry/Derivative thermogravimetry (TG/DTG) and differential scanning calorimetry (DSC). The highest occupied molecular orbital/lowest unoccupied molecular orbital (HOMO/LUMO), density of state (DOS), and time-dependence TD-DFT computations were correlated to the experimental electron transfer in water and acrylonitrile solvents.

ChemInform Abstract: Microwave-Assisted Cleavage of Aryl Methyl Ethers with Lithium Thioethoxide (LiSEt).

ChemInform ◽  
2008 ◽  
Vol 39 (48) ◽  
Author(s):  
Jan Cvengros ◽  
Stefan Neufeind ◽  
Anne Becker ◽  
Hans-Guenther Schmalz
Keyword(s):  
Microwave Assisted ◽  
Aryl Methyl

ChemInform Abstract: A Convenient Conversion of Substituted Cyclohexenones into Aryl Methyl Ketones.

ChemInform ◽  
2012 ◽  
Vol 43 (46) ◽  
pp. no-no
Author(s):  
Andre P. Gehring ◽  
Franz Bracher
Keyword(s):  
Methyl Ketones ◽  
Aryl Methyl

Water-soluble TRIS-terminated PAMAM dendrimers: microwave-assisted synthesis, characterization and Cu(ii) intradendrimer complexes

RSC Advances ◽  
2015 ◽  
Vol 5 (74) ◽  
pp. 60581-60595 ◽  
Author(s):  
Ali Serol Ertürk ◽  
Mustafa Ulvi Gürbüz ◽  
Metin Tülü ◽  
Abdürrezzak Emin Bozdoğan
Keyword(s):  
Drug Carriers ◽  
Pamam Dendrimers ◽  
Water Soluble ◽  
Microwave Assisted Synthesis ◽  
Potential Drug ◽  
Microwave Assisted

Microwave-assisted synthesis, characterization and Cu(ii) complexes of water-soluble TRIS-terminated PAMAM dendrimers as novel potential drug carriers and templates for nanomaterials.

Electrosynthesis of α-keto acetals by a selenium-catalyzed transformation of aryl methyl ketones

1998 ◽  
Vol 43 (3-4) ◽  
pp. 335-339 ◽  
Author(s):  
D.Scott Smith ◽  
Jack Winnick ◽  
Youzhen Ding ◽  
Lawrence A. Bottomley
Keyword(s):  
Methyl Ketones ◽  
Aryl Methyl
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