ChemInform Abstract: Reinvestigation of Palladium-Catalyzed Allylation of the Monoacetate of 4-Cyclopentene-1,3-diol and Synthesis of the Coronafacic Acid Ethyl Ester.

This study evaluated the effect of different concentrations (20, 40 and 60 mg/L) of 3-aminobenzoic acid ethyl ester methanesulfonate (MS-222) on the quality changes in turbot during simulated transport in water. The results showed that the ammonia nitrogen content in the transportation water of each sample increased significantly, and the dissolved oxygen level decreased. The dissolved oxygen content in MS-222-treated samples was higher than that of control group (CK) samples. For turbot flesh quality, simulated transport in water led to a decrease in moisture, fat and protein contents in all samples. The MS-222-treated turbot samples showed higher pH values, glycogen contents, springiness and chewiness values and lower lactic acid contents comparing with the CK samples during simulated transport in water. In addition, the fresh and bitter amino acids in the muscle of turbot increased in each treatment group compared to the non-transported fish at the end of the simulated transport. The results showed that MS-222 treatment could retard the turbot transport stress and improve the quality of turbot during simulated transport in water.

Download Full-text

Sonochemical synthesis of 2-substituted nicotinic acid ethyl ester derivatives: their in vitro and in silico evaluation against SIRT1

Journal of Molecular Structure ◽

10.1016/j.molstruc.2021.131069 ◽

2021 ◽

pp. 131069

Author(s):

Chandra Sekhar Challa ◽

Naresh Kumar Katari ◽

Varadacharyulu Nallanchakravarthula ◽

Devanna Nayakanti ◽

Ravikumar Kapavarapu ◽

...

Keyword(s):

Nicotinic Acid ◽

Ethyl Ester ◽

In Silico ◽

Acid Ethyl Ester ◽

Sonochemical Synthesis

Download Full-text

GC-MS ANALYSIS OF INVASIVE AQUATIC WEED, PISTIA STRATIOTES L. AND EICHHORNIA CRASSIPES (MART.) SOLMS

International Journal of Current Pharmaceutical Research ◽

10.22159/ijcpr.2017.v9i3.19970 ◽

2017 ◽

Vol 9 (3) ◽

pp. 111 ◽

Cited By ~ 3

Author(s):

Tulika Tyagi ◽

Mala Agarwal

Keyword(s):

Methyl Ester ◽

Ethyl Ester ◽

Eichhornia Crassipes ◽

Acid Methyl Ester ◽

Acid Ethyl Ester ◽

Pistia Stratiotes ◽

Aquatic Weed ◽

Hexadecenoic Acid ◽

Hexadecanoic Acid ◽

Acid Methyl

Objective: To investigate the bioactive components of an invasive aquatic weed, Pistia stratiotes L. and Eichhornia crassipes (Mart.) Solms vegetative parts by using Gas Chromatography-Mass Spectrometer (GC-MS).Methods: The chemical compositions of the ethanol extract of whole plant Pistia stratiotes L. and Eichhornia crassipes (Mart.) Solms was investigated using Agilent Technologies GC-MS (GC-7890A, MS 5975C).Results: The results of GC-MS analysis of the ethanolic extract revealed the existence of 28 phytochemical compounds in Pistia stratiotes L. n-Hexadecanoic acid,-11-Hexadecenoic acid, ethyl ester, Hexadecanoic acid, ethyl ester, Octadecanoic acid, ethyl ester, 2-Cyclopenten-1-one, 5-hydroxy-2,3-dimethyl, L-Glutamine, 2-Pentadecanone, 6,10,14-trimethyl, Linolelaidic acid, methyl ester, 9,12,15-Octadecatrienoic acid, methyl ester,(Z,Z,Z), Nonadecane, 12,15-Octadecadiynoic acid, methyl ester, Hexadecanoic acid, 2-hydroxy-1-(hydroxymethyl)ethyl ester, Diisooctyl phthalate, Docosanoic acid, ethyl ester, Stigmasterol, Bis(2-ethylhexyl) phthalate, 1-Monolinoleoylglycerol trimethylsilyl ether, Ethyl iso-allocholate are the major compound.The ethanolic extract of Eichhornia crassipes (Mart.) Solms contains 43 phytochemical compounds of high and low molecular weight n-Hexadecanoic acid, E-11-Hexadecenoic acid, ethyl ester, Palmitic acid, Phytol, 9,12,15-Octadecatrienal, 9,12-Octadecadienoic acid, ethyl ester, Linolenic acid, ethyl ester, Stearic acid, ethyl ester, Hexadecanoic acid, 2-hydroxy-1-(hydroxymethyl)ethyl ester, α-Glyceryl linolenate, 1-Monolinoleoylglycerol trimethylsilyl ether, Linoleic acid, 2,3-bis-(O-TMS)-propyl ester, Stigmasterol, Linolelaidic acid, methyl ester, 9,12,15-Octadecatrienoic acid, ethyl ester, (Z,Z,Z), Ethyl iso-allocholate, Cholesta-22,24-dien-5-ol, 4,4-dimethyl are the major compounds.These results indicates Pistia stratiotes L. and Eichhornia crassipes (Mart.) Solms possess potent antioxidant, anti-inflammatory, anticancer, antitumour, antiarthritic, cancer preventive, antibacterial effects so can be recommended as a plant of phytopharmaceutical importance.Conclusion: The ethanol extract of Pistia stratiotes L. and Eichhornia crassipes (Mart.) Solms proves as a potential source of bioactive compounds of pharmacological importance.

Download Full-text

Bioactive Phenolic Compounds from the Roots of Danshen (Salvia miltiorrhiza)

Natural Product Communications ◽

10.1177/1934578x1801301018 ◽

2018 ◽

Vol 13 (10) ◽

pp. 1934578X1801301

Author(s):

Nguyen Huu Tung ◽

Le Quoc Hung ◽

Ha Van Oanh ◽

Duong Thi Ly Huong ◽

Phuong Thien Thuong ◽

...

Keyword(s):

Phenolic Compounds ◽

Methyl Ester ◽

Ethyl Ester ◽

Rosmarinic Acid ◽

Salvia Miltiorrhiza ◽

Chemical Constituents ◽

Acid Methyl Ester ◽

Acid Ethyl Ester ◽

Salvianolic Acid ◽

Salvianolic Acid A

Danshen ( Salvia miltiorrhiza Bunge) is one of the most used medicinal plants in the Oriental medicine and has been well studied for application in modern medicine. In our continuing study on chemical constituents of danshen cultivated in Vietnam, using chromatography separation resulted in the isolation of six phenolic compounds including a benzophenone, iriflophenone 2- O- α-L-rhamnopyranoside (1), and five phenolic acids including rosmarinic acid (2), rosmarinic acid methyl ester (3), rosmarinic acid ethyl ester (4), salvianolic acid A methyl ester (5) and salvianolic acid A ethyl ester (6) from the butanol portion of the danshen crude extract. Beside the typically main phenolic acid components, to our knowledge, iriflophenone 2- O- α-L-rhamnopyranoside (1) was first isolated from salvia sp. On biological testing, compound 1 showed strong antiproliferative activity on HL-60 leukemia cells with the IC50 of 8.9 μM; compounds 1 and 3–6 inhibited markedly nitric oxide production in lipopolysaccharide-treated RAW 264.7 cells.

Download Full-text