ChemInform Abstract: Traceless Synthetic Approach Towards Oxaza-dicyclopenta[a,h]naphthalenes under Solvent-Free Condition: A Basic Alumina Supported Green Protocol.

ChemInform ◽  
2013 ◽  
Vol 44 (39) ◽  
pp. no-no
Author(s):  
Rupankar Paira ◽  
Shyamal Mondal ◽  
Arpan Chowdhury ◽  
Maitreyee Banerjee ◽  
Arindam Maity ◽  
...  
Keyword(s):  
Solvent Free ◽  
Synthetic Approach ◽  
Free Condition ◽  
Green Protocol ◽  
Basic Alumina ◽  
Solvent Free Condition

Traceless synthetic approach towards oxaza-dicyclopenta[a,h]naphthalenes under solvent-free condition: a basic alumina-supported green protocol

2013 ◽  
Vol 54 (24) ◽  
pp. 3046-3050 ◽  
Author(s):  
Rupankar Paira ◽  
Shyamal Mondal ◽  
Arpan Chowdhury ◽  
Maitreyee Banerjee ◽  
Arindam Maity ◽  
...  
Keyword(s):  
Solvent Free ◽  
Synthetic Approach ◽  
Free Condition ◽  
Green Protocol ◽  
Basic Alumina ◽  
Solvent Free Condition

scholarly journals Green approach to Chemo-Selective N-Boc Protection of Amines using Catalytic amount of Lithium Hydroxide Monohydrate under Solvent Free Condition

2020 ◽  
pp. 06-12
Author(s):  
Sandip P. Gondake ◽  
Santosh R. Kshirsagar ◽  
Ashok S. Pise ◽  
Valmik S. Kapase ◽  
Sagar I. Shinde
Keyword(s):  
Reaction Times ◽  
Catalytic Amount ◽  
Lithium Hydroxide ◽  
Solvent Free ◽  
Side Reactions ◽  
Free Condition ◽  
Green Protocol ◽  
Solvent Free Condition ◽  
Lithium Hydroxide Monohydrate ◽  
Hydroxide Monohydrate

<p>The protecting group plays important role in synthesis of multifunctional targets. A simple rapid efficient and green method for chemo-selective N-Boc protection of amines using Lithium hydroxide as a green catalyst. In the present work amine protection in presence of ditert-butyl carbonate under solvent free condition is carried out. An efficient green protocol for chemoselctive N-Boc protection of aryl, aliphatic, aromatic, acyclic and hetero cyclic amines (1 m mol %)( 10, 20, 30) were carried out with ditert-butyl carbonate (Boc)2 O using Lithium hydroxide monohydrate (10 mol %) at room temperature under solvent free condition to give white solid monitored on TLC. No side reactions are observed .The present protocol were simple, rapid, efficient, shorter reaction times, high yielding, highly selective, economical and eco-friendly</p>

Phase‐controlled synthesis of zeolites from sodium aluminosilicate under OSDA/solvent‐free condition

2021 ◽  
Author(s):  
Yoshitaka Mizuno ◽  
Koji Miyake ◽  
Shunsuke Tanaka ◽  
Norikazu Nishiyama ◽  
Choji Fukuhara ◽  
...  
Keyword(s):  
Solvent Free ◽  
Controlled Synthesis ◽  
Free Condition ◽  
Sodium Aluminosilicate ◽  
Solvent Free Condition

Sunlight‐Assisted Photocatalytic Sustainable Synthesis of 1,4‐Disubstituted 1,2,3‐Triazoles and Benzimidazoles Using TiO 2 −Cu 2 (OH)PO 4 Under Solvent‐Free Condition

2021 ◽  
Vol 6 (6) ◽  
pp. 1210-1215
Author(s):  
Tayyala Kiranmye ◽  
Murugan Vadivelu ◽  
Deviga Magadevan ◽  
Sugirdha Sampath ◽  
Kannabiran Parthasarathy ◽  
...  
Keyword(s):  
Solvent Free ◽  
Free Condition ◽  
Solvent Free Condition
Sign in / Sign up

Export Citation Format

Share Document