scholarly journals Chromatographic parameter determination for complex biological feedstocks

2018 ◽  
Vol 34 (4) ◽  
pp. 1006-1018 ◽  
Author(s):  
Silvia M. Pirrung ◽  
Diogo Parruca da Cruz ◽  
Alexander T. Hanke ◽  
Carmen Berends ◽  
Ruud F.W.C. Van Beckhoven ◽  
...  
Keyword(s):  
Parameter Determination ◽  
Chromatographic Parameter

Parameter Determination for Chloride and Tritium Transport in Undisturbed Lysimeters during Steady Flow

1992 ◽  
Vol 23 (2) ◽  
pp. 89-104 ◽  
Author(s):  
Ole H. Jacobsen ◽  
Feike J. Leij ◽  
Martinus Th. van Genuchten
Keyword(s):  
Experimental Data ◽  
Unsaturated Flow ◽  
Transport Model ◽  
Time Moment ◽  
Breakthrough Curves ◽  
Coarse Sand ◽  
Retardation Factor ◽  
Parameter Determination ◽  
Model Parameters ◽  
Water Fraction

Breakthrough curves of Cl and 3H2O were obtained during steady unsaturated flow in five lysimeters containing an undisturbed coarse sand (Orthic Haplohumod). The experimental data were analyzed in terms of the classical two-parameter convection-dispersion equation and a four-parameter two-region type physical nonequilibrium solute transport model. Model parameters were obtained by both curve fitting and time moment analysis. The four-parameter model provided a much better fit to the data for three soil columns, but performed only slightly better for the two remaining columns. The retardation factor for Cl was about 10 % less than for 3H2O, indicating some anion exclusion. For the four-parameter model the average immobile water fraction was 0.14 and the Peclet numbers of the mobile region varied between 50 and 200. Time moments analysis proved to be a useful tool for quantifying the break through curve (BTC) although the moments were found to be sensitive to experimental scattering in the measured data at larger times. Also, fitted parameters described the experimental data better than moment generated parameter values.

scholarly journals Parameter Determination and Ion Current Improvement of the Ion Current Sensor Used for Flame Monitoring

Sensors ◽  
2021 ◽  
Vol 21 (3) ◽  
pp. 697
Author(s):  
Hanqing Xu ◽  
Weijun Fan ◽  
Jianwei Feng ◽  
Peiliang Yan ◽  
Shuchan Qi ◽  
...  
Keyword(s):  
Contact Area ◽  
High Reliability ◽  
Ion Current ◽  
Parameter Determination ◽  
Current Sensor ◽  
Vertical Position ◽  
Excitation Voltage ◽  
Burner Exit ◽  
And Performance ◽  
Flame Monitoring

Flame monitoring of industrial combustors with high-reliability sensors is essential to operation security and performance. An ion current flame sensor with a simple structure has great potential to be widely used, but a weak ion current is the critical defect to its reliability. In this study, parameters of the ion current sensor used for monitoring flames on a Bunsen burner are suggested, and a method of further improving the ion current is proposed. Effects of the parameters, including the excitation voltage, electrode area, and electrode radial and vertical positions on the ion current, were investigated. The ion current grew linearly with the excitation voltage. Given that the electrodes were in contact with the flame fronts, the ion current increased with the contact area of the cathode but independent of the contact area of the anode. The smaller electrode radial position resulted in a higher ion current. The ion current was insensitive to the anode vertical position but largely sensitive to the cathode vertical position. Based on the above ion current regularities, the sensor parameters were suggested as follows: The burner served as a cathode and the platinum wire acted as an anode. The excitation voltage, anode radial and vertical positions were 120 V, 0 mm, and 6 mm, respectively. The method of further improving the ion current by adding multiple sheet cathodes near the burner exit was proposed and verified. The results show that the ion current sensor with the suggested parameters could correctly identify the flame state, including the ignition, combustion, and extinction, and the proposed method could significantly improve the magnitude of the ion current.

scholarly journals A Mixed Numerical-Experimental Method to Characterize Metal-Polymer Interfaces for Crash Applications

Metals ◽  
2021 ◽  
Vol 11 (5) ◽  
pp. 818
Author(s):  
Jonas Richter ◽  
Moritz Kuhtz ◽  
Andreas Hornig ◽  
Mohamed Harhash ◽  
Heinz Palkowski ◽  
...  
Keyword(s):  
Experimental Parameter ◽  
Dissimilar Materials ◽  
Calibration Method ◽  
Parameter Determination ◽  
Failure Behavior ◽  
Cohesive Elements ◽  
Interface Failure ◽  
Wide Range ◽  
Polymer Metal ◽  
Metal Polymer

Metallic (M) and polymer (P) materials as layered hybrid metal-polymer-metal (MPM) sandwiches offer a wide range of applications by combining the advantages of both material classes. The interfaces between the materials have a considerable impact on the resulting mechanical properties of the composite and its structural performance. Besides the fact that the experimental methods to determine the properties of the single constituents are well established, the characterization of interface failure behavior between dissimilar materials is very challenging. In this study, a mixed numerical–experimental approach for the determination of the mode I energy release rate is investigated. Using the example of an interface between a steel (St) and a thermoplastic polyolefin (PP/PE), the process of specimen development, experimental parameter determination, and numerical calibration is presented. A modified design of the Double Cantilever Beam (DCB) is utilized to characterize the interlaminar properties and a tailored experimental setup is presented. For this, an inverse calibration method is used by employing numerical studies using cohesive elements and the explicit solver of LS-DYNA based on the force-displacement and crack propagation results.

Small specimen techniques for estimation of tensile, fatigue, fracture and crack propagation material model parameters

2021 ◽  
pp. 030932472110252
Author(s):  
Julija Kazakeviciute ◽  
James Paul Rouse ◽  
Davide Focatiis ◽  
Christopher Hyde
Keyword(s):  
Fatigue Fracture ◽  
Structural Integrity ◽  
Standard Specimen ◽  
Creep Behaviour ◽  
Parameter Determination ◽  
Model Parameters ◽  
Small Specimen ◽  
Testing Methods ◽  
Advantages And Disadvantages ◽  
Tensile Fatigue

Small specimen mechanical testing is an exciting and rapidly developing field in which fundamental deformation behaviours can be observed from experiments performed on comparatively small amounts of material. These methods are particularly useful when there is limited source material to facilitate a sufficient number of standard specimen tests, if any at all. Such situations include the development of new materials or when performing routine maintenance/inspection studies of in-service components, requiring that material conditions are updated with service exposure. The potentially more challenging loading conditions and complex stress states experienced by small specimens, in comparison with standard specimen geometries, has led to a tendency for these methods to be used in ranking studies rather than for fundamental material parameter determination. Classifying a specimen as ‘small’ can be subjective, and in the present work the focus is to review testing methods that utilise specimens with characteristic dimensions of less than 50 mm. By doing this, observations made here will be relevant to industrial service monitoring problems, wherein small samples of material are extracted and tested from operational components in such a way that structural integrity is not compromised. Whilst recently the majority of small specimen test techniques development have focused on the determination of creep behaviour/properties as well as sub-size tensile testing, attention is given here to small specimen testing methods for determining specific tensile, fatigue, fracture and crack growth properties. These areas are currently underrepresented in published reviews. The suitability of specimens and methods is discussed here, along with associated advantages and disadvantages.

scholarly journals Physical Parameter Determination for the δ Scuti Star HD 200925

2000 ◽  
Vol 176 ◽  
pp. 467-468 ◽  
Author(s):  
J. H. Peña ◽  
M. Paparó ◽  
R. Peniche ◽  
M. Rodríguez ◽  
M. A. Hobart ◽  
...  
Keyword(s):  
Physical Parameter ◽  
Time Scale ◽  
Parameter Determination ◽  
Theoretical Ratio ◽  
Blazhko Effect ◽  
Metal Abundance ◽  
Scuti Star

HD 200925 is an unusual star: the period is stable on a time scale of many years, yet it shows variations which are either large and irregular, or small, suggesting a possible Blazhko effect (Poretti 1984; Joner & Johnson 1985); it has larger values of Teff and log g derived from uvbyβ than those of dwarf Cepheids of similar period; and it has a somewhat higher metal abundance, [Fe/H], than the Hyades. Furthermore, in conflict to what Joner and McNamara (1983) determined – that m1 index shows no variation with temperature – HD 200925 shows a definite variation, unlike that predicted in Crawford (1979). No explanation of this has yet been found. Johnson & Joner (1986) also derived an unusual and unexpected value of [Fe/H]. Finally, with respect to the pulsation periods of this star, Mantegazza & Poretti (1986) determined the existence of two periods: one definite, 0.26730 d and a possible second one of 0.2138 d which yield a ratio of P2/P1 = 0.800, the theoretical ratio expected between the first and the second overtones, found in other pulsating variables. All of these facts make HD 200925 an interesting star, motivating the present study.

Problems Associated with Kα Doublet in Residual Stress Measurements

1979 ◽  
Vol 23 ◽  
pp. 333-339
Author(s):  
S. K. Gupta ◽  
B. D. Cullity
Keyword(s):  
Residual Stress ◽  
Silicon Powder ◽  
Lattice Parameter ◽  
Diffraction Peak ◽  
Parameter Determination ◽  
X Ray Diffraction ◽  
X Ray ◽  
Analysis Techniques ◽  
The Difference ◽  
Similar Accuracy

Since the measurement of residual stress by X-ray diffraction techniques is dependent on the difference in angle of a diffraction peak maximum when the sample is examined consecutively with its surface at two different angles to the diffracting planes, it is important that these diffraction angles be obtained precisely, preferably with an accuracy of ± 0.01 deg. 2θ. Similar accuracy is desired in precise lattice parameter determination. In such measurements, it is imperative that the diffractometer be well-aligned. It is in the context of diffractometer alignment with the aid of a silicon powder standard free of residual stress that the diffraction peak analysis techniques described here have been developed, preparatory to residual stress determinations.

Sign in / Sign up

Export Citation Format

Share Document