Preparation of a high-temperature-resistant lightening agent and its application in a cement slurry system

2018 ◽  
Vol 136 (13) ◽  
pp. 47292 ◽  
Author(s):  
Rui Zhang ◽  
Qiong Han ◽  
Xuyang Zhu ◽  
Youfeng Cai ◽  
Tongqing Zhang
Keyword(s):  
High Temperature ◽  
Cement Slurry ◽  
Slurry System

scholarly journals Design and Evaluation of High-Temperature Well Cementing Slurry System Based on Fractal Theory

Energies ◽  
2021 ◽  
Vol 14 (22) ◽  
pp. 7552
Author(s):  
Guanyi Zheng ◽  
Xiaoyang Guo ◽  
Zaoyuan Li ◽  
Jinfei Sun
Keyword(s):  
Life Cycle ◽  
High Temperature ◽  
Fractal Theory ◽  
Continuous Distribution ◽  
Cement Slurry ◽  
Accumulation Model ◽  
Deep Wells ◽  
Sealing Performance ◽  
Slurry System ◽  
Long Life

The efficient development of oil and gas resources is inseparable from the progress of drilling technology and the safety of the long life cycle of wellbore. At present, exploration and development is expanding to deep and ultra-deep areas. The long life cycle safety of deep and ultra-deep wells is mainly realized by the sealing performance of cement slurry. Additionally, the accumulation degree of cement slurry particles is closely related to sealing performance. Based on fractal theory, an accumulation model of continuous distribution of additive material particles was designed, which can determine the range of fractal dimension necessary to realize the tight stacking and guide the proportion of solid admixture. The formulation of high temperature-resistant cement slurry was prepared by designing the ratio of solid admixture and optimizing the high temperature-resistant liquid admixture. The evaluation of engineering and temperature resistance of the cement slurry proves the rationality of the accumulation model, which can be applied to the design of a high temperature cementing slurry system in deep and ultra-deep wells.

Zaczyny cementowe z dodatkiem nanorurek węglowych do uszczelniania otworów wiertniczych o wysokiej temperaturze i ciśnieniu złożowym (150°C, 90 MPa)

Nafta-Gaz ◽  
2021 ◽  
Vol 77 (5) ◽  
pp. 323-331
Author(s):  
Miłosz Kędzierski ◽  
◽  
Marcin Rzepka ◽  
Keyword(s):  
Carbon Nanotubes ◽  
Compressive Strength ◽  
High Temperature ◽  
Rheological Parameters ◽  
External Diameter ◽  
Mechanical Parameters ◽  
Cement Slurry ◽  
Significant Information ◽  
High Temperature And Pressure ◽  
Temperature And Pressure

The article presents the results of the influence of carbon nanotubes on the mechanical parameters of cement stones under high temperature and pressure conditions (150°C, 90 MPa). The tests used multi-walled carbon nanotubes (MWCNTs) with an external diameter of 10–20 nm and a length of 10–30 μm. Cement slurries contained 0.1% of CNTs bwoc (by the weight of cement). Laboratory tests of cement slurries were carried out at the Oil and Gas Institute – National Research Institute. The tests were carried out under conditions of increased pressure and temperature at 150°C, 90 MPa. Cement slurries were prepared on the basis of class G drilling cement. Developing recipes were guided by the requirements to be met by cement slurry for the cementing of casing in the conditions of high temperature and reservoir pressures. The densities of tested slurries ranged from 1900 kg/m3 to 2250 kg/m3 (slurries with the addition of hematite). The cement slurries were tested for density, fluidity, rheological parameters, filtration and thickening time. Compressive strength tests and measuring adhesion were carried out after 2, 7, 14 and 28 days. Cement slurry recipes with very good technological parameters were developed and after curing (after 28 days of hydration) had very high values of compressive strength, reaching up to 45 MPa. Cements were characterized by high values of adhesion to pipes reaching up 7 MPa after 28 days. The research showed significant information about possible applications of carbon nanotubes to modify the cement slurry under conditions of high temperature and pressure. The conducted tests confirmed that the addition of even small amounts of CNTs improves the mechanical parameters of the cement stone compared to the base sample without such addition, and also reduces the thickening time of cement slurries and reduces filtration. It is investigated that CNTs addition increases the viscosity and yield point of cement slurry. As a result, slurries with the addition of MWCNTs will more effectively displace the mud from the borehole and significantly affect the quality of cementation.

Research and Application of Ultra-High Cementing Slurry

2016 ◽  
Vol 847 ◽  
pp. 485-489
Author(s):  
Xing Cai Zhang ◽  
Xiao Wei Cheng ◽  
Xiao Yang Guo
Keyword(s):  
High Temperature ◽  
Oil And Gas ◽  
Good Effect ◽  
Fluid Loss ◽  
Cement Slurry ◽  
Sedimentation Stability ◽  
Temperature Resistance ◽  
Deep Wells ◽  
High Temperature Resistance ◽  
Shallow Wells

With the exploration of oil and gas in depth, shallow wells already can’t satisfy the requirement, therefore to explore and develop deep reservoirs is necessary. In the case of deep wells the loop temperature of bottom can reach to 150°C-200°C, which put forward a higher requirement for the high temperature resistance property of cement slurry. At present, many problems existed in the most of high temperature cement slurry. For example, high temperature resistance is not well, cement thickening time can’t adjust easily, mega-thermal sedimentation stability is unsatisfactory, and ultra-retarding phenomenon appeared for the top prone. After research indoors, we developed the ultra-high temperature slurry system by means of the investigation on cementing additives and select proper materials from high temperature resistant fluid loss additives, retarders, flowable agent at the same time. This system needs a lots of properties, such as, adjustable slurry thickening time below 200°C, great slurry sedimentation stability, API loss can be controlled at the range of 0-50ml, insensitive to temperature and density, could be used in low-density and conventional density cement etc. This system be used successfully in the well that loop temperature of bottom reaches to 185°C and get a good effect finally.

Performance Evaluation of Polycarboxylic Acid Dispersant for Oil Well Cementing

2020 ◽  
Vol 993 ◽  
pp. 1341-1350
Author(s):  
Xiu Jian Xia ◽  
Yong Jin Yu ◽  
Jian Zhou Jin ◽  
Shuo Qiong Liu ◽  
Ming Xu ◽  
...  
Keyword(s):  
High Temperature ◽  
Salt Resistance ◽  
Strength Development ◽  
Fluid Loss ◽  
Oil Well ◽  
Polycarboxylic Acid ◽  
Cement Slurry ◽  
Deep Wells ◽  
Oil Well Cement ◽  
Well Cement

The conventional oil-well cement dispersant has the characteristics of poor dispersion at high temperature, poor compatibility with other additives, and environmental pollution during the production process. In this article, with ultra-early strong polyether monomer, acrylic acid, 2-acrylamine-2-methylpropyl sulfonic acid, sodium methacrylate as copolymer monomers, an environmentally friendly polycarboxylic acid dispersant, DRPC-1L, was prepared by the aqueous solution free-radical polymerization. The chemical composition and thermal stability of the synthetic copolymer were characterized by FTIR and TGA techniques. The evaluation results show that DRPC-1L has a wide temperature range (30~210 °C), good salt-resistance and dispersing effect. It can significantly improve the rheological performance of cement slurry, and it is well matched with oil-well cement additives such as fluid loss agent, retarder and so on. Moreover, it is beneficial to the mechanical strength development of set cement, especially the early compressive strength. It can also inhibit the abnormal gelation phenomenon of cement slurry, flash set, that occurs during high temperature thickening experiments, which plays an important role in enhancing the comprehensive performance of cement slurry. Consequently, the novel polycarboxylic acid dispersant has good application prospects in deep and ultra-deep wells cementing.

Experimental and Theoretical Study on Slag MTC Improving the Cementing Quality of the Second Interface

2011 ◽  
Vol 361-363 ◽  
pp. 456-460 ◽  
Author(s):  
Hua Jie Liu ◽  
Yu Huan Bu ◽  
Fei Li
Keyword(s):  
Experimental Study ◽  
Theoretical Study ◽  
Theoretical Research ◽  
Chemical Shrinkage ◽  
Low Density ◽  
Cement Slurry ◽  
Shrinkage Ratio ◽  
Mud Cake ◽  
Slurry System

In view of the complicated issue that how to improve the cementing quality of the second interface in cementing engineering, experimental and theoretical research on slag MTC slurry improving the quality of the second interface was carried out in the paper. Experimental study shows that slag MTC and mud cake can achieve overall cementing; the volume shrinkage ratio of slag MTC is far less than the cement slurry system; and the strength of slag MTC cannot be affected by the presence of mud cake and is greater than low-density cement slurry. Theoretical analysis shows that the alkali activator and Ca(OH)2 produced by hydration can react with SiO2 which exists in mud cake and dead mud to get C-S-H gel with a low ratio of calcium to silicon, and improving the quality of the second interface. The study on the chemical shrinkage ratio of the products of slag MTC hydration was made by using the method of chemical analysis, and low-shrinkage mechanism of MTC was revealed. The results show that mud cake solidification, dead mud solidification and low-shrinkage ratio are fundamental to improve the cementing quality of slag MTC and formation.

scholarly journals Analyzing Cement Rheological Properties Using Different Additive Schemes at High Pressure and High Temperature Conditions

2020 ◽  
Vol 39 (3) ◽  
pp. 466-474
Author(s):  
Khalil Rehman Memon ◽  
Aftab Ahmed Mahesar ◽  
Shahzad Ali Baladi ◽  
Muhannad Talib Sukar
Keyword(s):  
High Pressure ◽  
High Temperature ◽  
Rheological Properties ◽  
Silica Fume ◽  
Gel Strength ◽  
Water Quantity ◽  
Fluid Loss ◽  
Cement Slurry ◽  
Three Samples ◽  
Loss Control

The experimental study was conducted on rheological properties in laboratory to measure the integrity of cement slurry. Three samples were used and analyzed at different parameters to check the elasticity of cement slurry. Additives with various concentrations, i.e. silica fume % BWOC (Present by Weight on Cement) (15, 17, 19 and 21), dispersant % Wt (Percent Weight) (0.21, 0.26 and 0.31) and additional 1; % Wt of fluid losscontrol were used to improve the performance of the cement slurry at the temperature of 123oC. The results have shown that increase in the concentration of dispersants that have caused to decrease in the Plastic Viscosity (PV), Yield Point (YP) and GS (Gel Strength). The rheological properties of cement were improved with the addition of fluid loss control additive in 21 % BWOC (Present by Weight on Cement) silica fume increase the water quantity in cement slurry that improve its durability and to reduce the strength retrogression in High Temperature High Pressure (HTHP) environment. Results were achieved through HTHP OFITE Viscometer (Model 1100).

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