Spontaneous interfacial cellular convection accompanying mass transfer: Ethylene glycol-acetic acid-ethyl acetate

AIChE Journal ◽  
1962 ◽  
Vol 8 (3) ◽  
pp. 350-356 ◽  
Author(s):  
Aluf Orell ◽  
J. W. Westwater
1978 ◽  
Vol 24 (12) ◽  
pp. 2135-2138 ◽  
Author(s):  
K W Jackson

Abstract Each of 65 laboratories analyzed 10 whole-blood samples for erythrocyte protoporphyrin by one or more of several analytical procedures. These procedures were of two types: (a) extraction of protoporphyrin from the erythrocytes into ethyl acetate/acetic acid, re-extraction into hydrochloric acid, and fluorometric measurement; or (b) direct reading in a portable fluorometer (hematofluorometer), with no pretreatment of the blood sample. Interlaboratory correlation was generally poor, especially between laboratories using extraction procedures. Hematofluorometric results intercorrelated better, but they had a low bias as compared to the extraction approach. Nationwide standardization of the test is required to assure satisfactory interlaboratory performance and to identify laboratories whose results are sufficiently accurate to be used for interpretations according to guidelines set forth by the Center for Disease Control for erythrocyte protoporphyrin testing.


Author(s):  
Xue Yang ◽  
Yongling Liu ◽  
Tao Chen ◽  
Nana Wang ◽  
Hongmei Li ◽  
...  

Abstract Separation of natural compounds directly from the crude extract is a challenging work for traditional column chromatography. In the present study, an efficient method for separation of three main compounds from the crude extract of Dracocephalum tanguticum has been successfully established by high-speed counter-current chromatography (HSCCC). The crude extract was directly introduced into HSCCC by using dimethyl sulfoxide as cosolvent. Ethyl acetate/n-butyl alcohol/0.3% glacial acetic acid (4: 1: 5, v/v) system was used and three target compounds with purity higher than 80% were obtained. Preparative HPLC was used for further purification and three target compounds with purity higher than 98% were obtained. The compounds were identified as chlorogenic acid, pedaliin and pedaliin-6″-acetate.


2007 ◽  
Vol 258 (2) ◽  
pp. 115-124 ◽  
Author(s):  
Bastian Schmid ◽  
Michael Döker ◽  
Jürgen Gmehling

Desalination ◽  
2003 ◽  
Vol 154 (2) ◽  
pp. 147-152 ◽  
Author(s):  
Lixin Yu ◽  
Tao Lin ◽  
Qingfeng Guo ◽  
Jihua Hao

2018 ◽  
Vol 63 (1) ◽  
pp. 170-178 ◽  
Author(s):  
László Kiss

In this article, the feasibility of the CuxS modified carbon microdisc electrode was examined by exposure to four different volatile organic compounds (2-propanol, acetic acid, ethyl acetate and n-butylamine) directly in their vapour phase using cyclic voltammetry and amperometry. The performance of the modified microdisc was compared with the bare carbon microdisc (30 μm in diameter) which was involved in a narrow-gap cell. By using both methods high current increase was observed for 2-propanol with the modified electrode and its sensitivity was sufficiently higher than with the bare electrode. The modified electrode showed lower current signals in case of acetic acid and n-butylamine. The latter formed a condensation layer at the interelectrode gap. Neither the bare nor the modified electrode was sensitive to ethyl acetate.


2017 ◽  
Vol 32 (1) ◽  
pp. 1-11 ◽  
Author(s):  
Andreia Miranda ◽  
Vanda Pereira ◽  
Marisela Pontes ◽  
Francisco Albuquerque ◽  
José C. Marques

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