scholarly journals APPLICATION OF MATHEMATICAL MODEL OF NAIK FOR DETERMINATION OF TOTAL EXTRACT YIELD OF HYSSOP OBTAINED BY SUPERCRITICAL EXTRACTION WITH CARBON DIOXIDE

2017 ◽  
Vol 8 (1) ◽  
Author(s):  
Vladan Mićić ◽  
Sabina Begić ◽  
Pero Dugić ◽  
Zoran Petrović

In this paper, supercritical extraction of hyssop (Hyssopus officinalis L.) is performed by using carbon dioxide as extractant. Effect of pressure (80, 100 and 150 bar) on the yield of total extract at a temperature 313 K, flow 0.00323 kg/min and the average diameter of particles 0.49 mm is investigated. For modeling of extraction system hyssop – supercritical CO2, Naik's model is applied, where in the total yield of extract is determined. On the basis of the value of the correlation coefficient |r| (0.976 – 0.992), it was concluded that a very strong correlation was obtained between reciprocal values of the total extract yield and extraction time (1/y i 1/t), so it can be concluded that Naik's model can succesfully be applied for determining yield of total extract.

2008 ◽  
Vol 44 (1) ◽  
pp. 125-131 ◽  
Author(s):  
V. Micic ◽  
Z. Lepojevic ◽  
B. Mandic ◽  
M. Jotanovic ◽  
G. Tadic ◽  
...  

The supercritical fluid extraction (SFE) by carbon dioxide (CO2) of Salvia officinalis L. was investigated. SFE by CO2 was performed at different pressure (80, 100, 150, 200 and 300 bar) and constant temperature of 40?C (all other extraction conditions, such are flow rate, particle diameter of Salvia officinalis, extraction time were kept constant. The GC-MS method was used for determination of qualitative and quantitative composition of obtained extracts and essential oils.


2018 ◽  
Vol 240 ◽  
pp. 01036
Author(s):  
Marcin Wołowicz ◽  
Jarosław Milewski ◽  
Piotr Lis

The paper aims to compare the models of working fluids against experimental data for carbon dioxide close to its critical conditions. Fortunately, most of the work is already done and published where the authors compared the models based on the equation of the state (EoS). There are a few other models which were not investigated, thus we would like to add a few new results here and focus only on near-critical properties where the biggest deviation between experimental and calculated properties can be observed. The area of interest was pressure range of 7.39 – 20 MPa and temperature range of 304-340 K just above fluid critical point (7.39 MPa, 304.25 K). Model validation was performed for density and heat capacity as one of the most important parameters in preliminary cycle analysis.


PLoS ONE ◽  
2015 ◽  
Vol 10 (8) ◽  
pp. e0134489 ◽  
Author(s):  
Bruna Aparecida Souza Machado ◽  
Gabriele de Abreu Barreto ◽  
Aline Silva Costa ◽  
Samantha Serra Costa ◽  
Rejane Pina Dantas Silva ◽  
...  

2011 ◽  
Vol 3 (1-2) ◽  
Author(s):  
Kiril Lisichkov ◽  
Stefan Kuvendziev ◽  
Borce Lisichkov

The goal of this work is isolation of tomato seed oil from the tomato waste (skin and seed) from tomato processing industry by utilization of non-conventional, green solvent technology. In the frames of experimental research, the influence of working parameters (temperature, pressure and extraction time) on the total yield of isolated tomato seed oil. Dynamic method for determination of solubility parameter in a supercritical CO2 has been used to determine the solubility of tomato seed oil in the supercritical CO2. Obtained results regarding the influence of operating parameters on total yield of extracted tomato seed oil are presented graphically. The influence of the supercritical fluid’ density on the tomato seed oil’ solubility was determined based on those results. The chemical composition of isolated tomato seed oil was determined by application of Gas Chromatography.


Molecules ◽  
2020 ◽  
Vol 25 (18) ◽  
pp. 4088
Author(s):  
Alexander Zakharenko ◽  
Denis Romanchenko ◽  
Pham Duc Thinh ◽  
Konstantin Pikula ◽  
Cao Thi Thuy Hang ◽  
...  

Extraction process of Cucumaria frondosa japonica Semper, 1868, which are subspecies of Cucumaria frondosa (Gunnerus, 1767), were studied. It was shown that supercritical carbon dioxide extraction of holothuria was more effective than conventional solvent extraction. Step-by-step extraction with carbon dioxide followed by supercritical extraction with the addition of a co-solvent of ethanol can almost double the yields of extracts of triterpene glycosides, styrenes and carotenoids. Moreover, the fraction of triterpene glycosides practically does not contain colored impurities, in contrast to traditional ethanol extraction. The obtained extracts by HPLC in combination with tandem mass spectrometry (HPLC-MS/MS) identified 15 triterpene glycosides, 18 styrene compounds and 14 carotenoids. Supercritical extraction made it possible to obtain extracts with yields superior to conventional hexane and alcohol extracts. Moreover, such an approach with the use of supercritical fluid extraction (SFE) and subsequent profiling of metabolites can help with the study of holothuria species that are not as well studied.


Author(s):  
Olexandr Pavlenko ◽  
Serhii Dun ◽  
Maksym Skliar

In any economy there is a need for the bulky goods transportation which cannot be divided into smaller parts. Such cargoes include building structures, elements of industrial equipment, tracked or wheeled construction and agricultural machinery, heavy armored military vehicles. In any case, tractor-semitrailer should provide fast delivery of goods with minimal fuel consumption. In order to guarantee the goods delivery, tractor-semitrailers must be able to overcome the existing roads broken grade and be capable to tow a semi-trailer in off-road conditions. These properties are especially important for military equipment transportation. The important factor that determines a tractor-semitrailer mobility is its gradeability. The purpose of this work is to improve a tractor-semitrailer mobility with tractor units manufactured at PJSC “AutoKrAZ” by increasing the tractor-semitrailer gradeability. The customer requirements for a new tractor are determined by the maximizing the grade to 18°. The analysis of the characteristics of modern tractor-semitrailers for heavy haulage has shown that the highest rate of this grade is 16.7°. The factors determining the limiting gradeability value were analyzed, based on the tractor-semitrailer with a KrAZ-6510TE tractor and a semi-trailer with a full weight of 80 t. It has been developed a mathematical model to investigate the tractor and semi-trailer axles vertical reactions distribution on the tractor-semitrailer friction performances. The mathematical model has allowed to calculate the gradeability value that the tractor-semitrailer can overcome in case of wheels and road surface friction value and the tractive force magnitude from the engine. The mathematical model adequacy was confirmed by comparing the calculations results with the data of factory tests. The analysis showed that on a dry road the KrAZ-6510TE tractor with a 80 t gross weight semitrailer is capable to climb a gradient of 14,35 ° with its coupling mass full use condition. The engine's maximum torque allows the tractor-semitrailer to overcome a gradient of 10.45° It has been determined the ways to improve the design of the KrAZ-6510TE tractor to increase its gradeability. Keywords: tractor, tractor-semitrailer vehicle mobility, tractor-semitrailer vehicle gradeability.


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