Glycerol Conversion to Diglycerol via Etherification under Microwave Irradiation

2020 ◽  
Author(s):  
Muhammad Ayoub ◽  
Wan Jie Wei ◽  
Manzoor Ahmad ◽  
Ranitha Mathialagan ◽  
Sarah Farrukh ◽  
...  
Keyword(s):  
Microwave Irradiation ◽  
Glycerol Conversion

scholarly journals Catalytic Activity of Intercalated Montmorillonite Clay for Glycerol Conversion to Oligomers via Microwave Irradiation

2020 ◽  
Vol 99 (1) ◽  
pp. 16-19
Author(s):  
Muhammad SAJID ◽  
Muhammad AYOUB ◽  
Yoshimitsu UEMURA ◽  
Suzana YUSUP ◽  
Bawadi B ABDULLAH ◽  
...  
Keyword(s):  
Catalytic Activity ◽  
Microwave Irradiation ◽  
Montmorillonite Clay ◽  
Glycerol Conversion

Comparative study of glycerol conversion to polyglycerol via conventional and microwave irradiation reactor

2019 ◽  
Vol 16 ◽  
pp. 2101-2107
Author(s):  
Muhammad Sajid ◽  
Muhammad Ayoub ◽  
Yoshimitsu Uemura ◽  
Suzana Yusup ◽  
Mahmood Saleem ◽  
...  
Keyword(s):  
Microwave Irradiation ◽  
Comparative Study ◽  
Glycerol Conversion

scholarly journals Synthesis of Triacetin Catalyzed by Activated Natural Zeolite Under Microwave Irradiation

2019 ◽  
Vol 8 (1) ◽  
pp. 01-07
Author(s):  
Dzikri Hamzah ◽  
Taufik Rinaldi ◽  
Marwan Marwan ◽  
Wahyu Rinaldi
Keyword(s):  
Acetic Acid ◽  
Quantitative Analysis ◽  
Microwave Irradiation ◽  
Natural Zeolite ◽  
Ester Group ◽  
Microwave Oven ◽  
Molar Ratio ◽  
Catalyst Loading ◽  
Glycerol Conversion ◽  
Microwave Transmission

Esterification of glycerol with acetic acid under microwave irradiation in the presence of activated natural zeolite was investigated. Natural zeolite was collected from Ujung Pancu (Aceh Besar) and chemically activated with hydrochloric acid. The reaction was carried out in a stirred glass flask reactor placed inside microwave oven. Experimental variables include microwave transmission time, molar ratio of glycerol to acetic acid, and catalyst loading. XRD profile of activated zeolite showed an increase of Si/Al ratio to 6.042 and the crystallinity decreased slightly by 12.23%, mainly due to dealumination during chemical treatment. Qualitative analysis by FTIR shows that the reaction product obtained by microwave heating contains ester group (triacetin) at wavelength 1706.669 cm-1, while the quantitative analysis by acidi-alkalimetry titration indicates the highest glycerol conversion of 93.033% at the reaction condition of the molar ratio of 1:9, catalyst loading of 3%, and microwave transmission of 10 minutes. The present work suggests that microwave can be utilized as efficient heating technique in esterification of glycerol to triacetin.

Eco-Friendly Synthesis of Pyrazoline Derivatives

2017 ◽  
Vol 9 (04) ◽  
Author(s):  
Mahesh G. Kharatmol ◽  
Deepali Jagdale
Keyword(s):  
Ionic Liquids ◽  
Microwave Irradiation ◽  
Organic Synthesis ◽  
Ultrasonic Irradiation ◽  
Minimal Energy ◽  
Anticancer Activities ◽  
Conventional Methods

Pyrazoline class of compounds serve as better moieties for an array of treatments, they have antibacterial, antifungal, antiinflammatory, antipyretic, diuretic, cardiovascular activities. Apart from these they also have anticancer activities. So, pertaining to its importance, many attempts are made to synthesize pyrazolines. Since conventional methods of organic synthesis are energy and time consuming. There are elaborate pathways for green and eco-friendly synthesis of pyrazoline derivatives including microwave irradiation, ultrasonic irradiation, grinding and use of ionic liquids which assures the synthesis of the same within much lesser time and by use of minimal energy

DESIGN AND PERFORMANCE EVALUATION OF A PLANT FOR GLYCEROL CONVERSION TO ACROLEIN

2015 ◽  
Vol 14 (3) ◽  
pp. 509-517 ◽  
Author(s):  
Ionut Banu ◽  
Georgiana Guta ◽  
Costin Sorin Bildea ◽  
Grigore Bozga
Keyword(s):  
Performance Evaluation ◽  
Glycerol Conversion ◽  
And Performance

Growth Process of SiC Grains Prepared by High-energy Microwave Irradiation

2014 ◽  
Vol 29 (2) ◽  
pp. 149-154 ◽  
Author(s):  
Shan HUANG ◽  
Ji-Gang WANG ◽  
Song LIU ◽  
Fan LI
Keyword(s):  
Microwave Irradiation ◽  
Growth Process ◽  
High Energy

Atom Transfer Radical Copolymerization of Acrylamide Under Microwave Irradiation

2013 ◽  
Vol 30 (4) ◽  
pp. 398
Author(s):  
Wei DING ◽  
Ling WANG ◽  
Tao YU ◽  
Guangmiao QU ◽  
Xiang GAO ◽  
...  
Keyword(s):  
Microwave Irradiation ◽  
Radical Copolymerization ◽  
Atom Transfer
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