scholarly journals Polycrystalline Diamond Characterisations for High End Technologies

Author(s):  
Awadesh Kumar Mallik
Author(s):  
D.P. Malta ◽  
S.A. Willard ◽  
R.A. Rudder ◽  
G.C. Hudson ◽  
J.B. Posthill ◽  
...  

Semiconducting diamond films have the potential for use as a material in which to build active electronic devices capable of operating at high temperatures or in high radiation environments. A major goal of current device-related diamond research is to achieve a high quality epitaxial film on an inexpensive, readily available, non-native substrate. One step in the process of achieving this goal is understanding the nucleation and growth processes of diamond films on diamond substrates. Electron microscopy has already proven invaluable for assessing polycrystalline diamond films grown on nonnative surfaces.The quality of the grown diamond film depends on several factors, one of which is the quality of the diamond substrate. Substrates commercially available today have often been found to have scratched surfaces resulting from the polishing process (Fig. 1a). Electron beam-induced current (EBIC) imaging shows that electrically active sub-surface defects can be present to a large degree (Fig. 1c). Growth of homoepitaxial diamond films by rf plasma-enhanced chemical vapor deposition (PECVD) has been found to planarize the scratched substrate surface (Fig. 1b).


Author(s):  
E. F. Koch

Because of the extremely rigid lattice structure of diamond, generating new dislocations or moving existing dislocations in diamond by applying mechanical stress at ambient temperature is very difficult. Analysis of portions of diamonds deformed under bending stress at elevated temperature has shown that diamond deforms plastically under suitable conditions and that its primary slip systems are on the ﹛111﹜ planes. Plastic deformation in diamond is more commonly observed during the high temperature - high pressure sintering process used to make diamond compacts. The pressure and temperature conditions in the sintering presses are sufficiently high that many diamond grains in the sintered compact show deformed microtructures.In this report commercially available polycrystalline diamond discs for rock cutting applications were analyzed to study the deformation substructures in the diamond grains using transmission electron microscopy. An individual diamond particle can be plastically deformed in a high pressure apparatus at high temperature, but it is nearly impossible to prepare such a particle for TEM observation, since any medium in which the diamond is mounted wears away faster than the diamond during ion milling and the diamond is lost.


Author(s):  
Priyanka Ghosh ◽  
Manuela Pacella ◽  
Christopher Cox ◽  
Mahdi Mohammadpour ◽  
Anish Roy

2007 ◽  
Vol 1039 ◽  
Author(s):  
Philippe Bergonzo ◽  
Hassen Hamrita ◽  
Dominique Tromson ◽  
Caroline Descamps ◽  
Christine Mer ◽  
...  

AbstractCVD diamond combines attractive properties for the fabrication of detection devices operating in specific environments. One problem that remains critical for device stability is the presence of defect levels that alter the detection performances, and the detection characteristics often appear as they are very depending on time, temperature, and history of the preceding irradiations.One issue we have proposed is to adapt one technique that is commonly used for time of flight spectroscopy in order to maintain a uniform electric field in the probed device, and based on the synchronisation of the device bias with the period of the excitation source. This can be applied to several types of detection applications, as long as we can rely on periodical triggering in order to synchronise the device polarisation. We apply it here to a LINAC electron accelerator used for photon pulse generation at the frequency of 25Hz. The result is a remarkable improvement of the performance of a polycrystalline diamond detector that exhibits a particularly defective response when used in the steady state excitation, to reach that of a perfectly stable and reproducible device response in the pulsed mode. We claim this method to be applicable to several types of excitations and particularly to present a high interest for monitoring accelerator sources, e.g. for medical dosimetry applications.


2021 ◽  
Vol 9 (6) ◽  
pp. 682
Author(s):  
Yu-Gang Ren ◽  
Lei Yang ◽  
Yan-Jun Liu ◽  
Bao-Hua Liu ◽  
Kai-Ben Yu ◽  
...  

Due to the need for accurate exploration of deep-sea scientific research, drilling techniques by combining the operational advantages of the Jiaolong manned submersible is considered one of the most feasible methods for deep-sea bedrock drilling. Based on deep sea bedrock cutting model and discrete element simulation, as well as efficient drilling as the design criterion, the development of a deep sea 7000 m electromechanical coring apparatus was carried out. The outstanding feature of this technology is that the bit load produced by the drill pressure is usually within the range 100–400 N while the recommended load for diamond drilling is 1–3 KN or even more. Therefore, searching for the drilling bits that can drill in extremely hard formations with minimal load and acceptable rates of penetration and rotary speed is the necessary step to prove the feasibility of electromechanical deep-sea drilling technology. A test has been designed and constructed to examine three types of drill bits. The results of experiments show that the new low-load polycrystalline diamond compact (PDC) bit has the highest penetration length of 138 mm/15 min under a 300 N load and 250 rpm rotary speed. Finally, field tests with the Jiaolong submersible were used to conduct deep sea experiments and verify the load model, which provides theoretical and technical data on the use of a low-load core sampling drill developed specifically for a deep sea submersible.


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