scholarly journals Toughness Assessment and Fracture Mechanism of Brittle Thin Films Under Nano-Indentation

Author(s):  
Kunkun Fu ◽  
Youhong Tang ◽  
Li Chang
2009 ◽  
Vol 1239 ◽  
Author(s):  
Yong Sun ◽  
Zaiwang Huang ◽  
Xiaodong Li

AbstractA facile electrophoretic deposition method was successfully applied to achieve novel nanoclay-reinforced polyacrylamide nanocomposite thin films. A special curled architecture of the re-aggregated nanoclay-platelets was identified, providing a possible source for realizing the interlocking mechanism in the nanocomposites. The curled architecture could be the result from strain releasing when the thin films were peeled off from the substrates. Through micro-/nano-indentation and in situ observation of the deformation during tensile test with an atomic force microscope (AFM), the localized deformation mechanism of the synthesized materials was investigated in further details. The results implied that a localized crack diversion mechanism worked in the synthesized nanocomposite thin films, which resembled its nature counterpart-nacre. The deformation behavior and fracture mechanism were discussed with reference to lamellar structure, interfacial strength between the nanoclays and the polyacrylamide matrix, and nanoclay agglomeration.


2021 ◽  
Vol 736 ◽  
pp. 138906
Author(s):  
Zenglu Song ◽  
Xiao Tang ◽  
Xiang Chen ◽  
Tao Fu ◽  
Huanping Zheng ◽  
...  

2002 ◽  
Vol 750 ◽  
Author(s):  
Koichiro Hattori ◽  
Junhua Xu ◽  
Hidetoshi Nakano ◽  
Isao Kojima

ABSTRACTWe have evaluated the hardness and elastic properties of thin films by using a simple procedure to calibrate the tip shape effect of the nano-indentation data. For the simplification, a truncated-shape approximation and linear fit are used to estimate the tip-shape and contact stiffness, respectively, substituting for polynomial area-function and power-law fit. The parameters used in the correction were determined by a fused silica and a single crystal silicon (100) surface. Different film/substrate systems are designed in order to assess these fitted parameters used in the correction. The transition behavior observed from the film to the substrate is well coincide with the other film thickness results, where the indentation depth above 50nm.


1999 ◽  
Vol 41 (9) ◽  
pp. 951-957 ◽  
Author(s):  
S. Suresh ◽  
T.-G. Nieh ◽  
B.W. Choi

Author(s):  
Manish Roy

Various thin films used for tribological applications are classified under four heads. Based on their load vs. displacement curves, which have some characteristics features, the ratio of nanohardness to elastic modulus and the ratio of cube of nanohardness to square of elastic modulus are evaluated in this chapter. It is demonstrated that depending on the type of film used, these ratios vary within a certain range. For soft self-lubricating films, these ratios are very low; whereas for hard self-lubricating film, these ratios are quite high.


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