scholarly journals Characterization of the chemical structure and innate immune-stimulating activity of an extracellular polysaccharide from Rhizobium sp. strain M2 screened using a silkworm muscle contraction assay

2017 ◽  
Vol 11 (5) ◽  
pp. 238-245 ◽  
Author(s):  
Makoto Urai ◽  
Tomoko Aizawa ◽  
Katsutoshi Imamura ◽  
Hiroshi Hamamoto ◽  
Kazuhisa Sekimizu
2017 ◽  
Vol 11 (5) ◽  
pp. 288-290
Author(s):  
Hiroko Maruki-Uchida ◽  
Masahiko Sai ◽  
Kazuhisa Sekimizu

2020 ◽  
Vol 17 (10) ◽  
pp. 760-771
Author(s):  
Qirui Gong ◽  
Niangui Wang ◽  
Kaibo Zhang ◽  
Shizhao Huang ◽  
Yuhan Wang

A phosphaphenanthrene groups containing soybean oil based polyol (DSBP) was synthesized by epoxidized soybean oil (ESO) and 9,10-dihydro-oxa-10-phosphaphenanthrene-10-oxide (DOPO). Soybean oil based polyol (HSBP) was synthesized by ESO and H2O. The chemical structure of DSBP and HSBP were characterized with FT-IR and 1H NMR. The corresponding rigid polyurethane foams (RPUFs) were prepared by mixing DSBP with HSBP. The results revealed apparent density and compression strength of RPUFs decreased with increasing the DSBP content. The cell structure of RPUFs was examined by scanning electron microscope (SEM) which displayed the cells as spherical or polyhedral. The thermal degradation and flame retardancy of RPUFs were investigated by thermogravimetric analysis, limiting oxygen index (LOI), and UL 94 vertical burning test. The degradation activation energy (Ea) of first degradation stage reduced from 80.05 kJ/mol to 37.84 kJ/mol with 80 wt% DSBP. The RUPF with 80 wt% DSBP achieved UL94 V-0 rating and LOI 28.3. The results showed that the flame retardant effect was mainly in both gas phase and condensed phase.


2021 ◽  
pp. 004051752110277
Author(s):  
Qilu Cui ◽  
Jiawei Li ◽  
Chongwen Yu

In this paper, the extraction process of flavonoids from hemp fibers was studied. Response surface methodology (RSM) analysis of the extraction parameters indicated that optimized results would be ethanol concentration 76 vol.%, bath ratio 1:50, and reaction time 139 min; therefore, an optimal extraction rate of flavonoids of 0.2275% can be obtained. The chemical structure, surface morphology and element composition of flavonoid extracts were analyzed. The test results indicated that hemp extract contains flavonoids, which can be used to extract flavonoids from hemp fiber, so as to comprehensively develop hemp fiber and reduce the discharge of waste liquid in the traditional degumming process.


2013 ◽  
Vol 130 (1) ◽  
pp. 710-710
Author(s):  
Ali Abdulkhani ◽  
Alinaghi Karimi ◽  
Ahmad Mirshokraie ◽  
Yahya Hamzeh ◽  
Nathalie Marlin ◽  
...  

2013 ◽  
Vol 132 ◽  
pp. 178-181 ◽  
Author(s):  
Yin Chen ◽  
Wenjun Mao ◽  
Baofeng Wang ◽  
Lina Zhou ◽  
Qianqun Gu ◽  
...  

2014 ◽  
Vol 1048 ◽  
pp. 452-455
Author(s):  
Qiang Wang ◽  
Shi Dong Wang ◽  
Ming Chen Qi ◽  
Shu Liang Zang

Two new imidazole ionic liquid salts, 1-allyl-3-methylimidazolium chloride ([AMIM]Cl) and 1-allyl-3-methy-imidazolium hydrogen sulfate ([EMIM]HSO4), were synthesized with direct synthesis and two-step synthesis method, using a viscosity meter, PH meter, conductivity meter, densitometer, infrared spectrometer determined its chemical structure and properties. The results show that two ionic liquids in the range is slightly different, the trend is roughly same. As the temperature increases, the viscosity decreases, PH gradually increased, the density decreases slightly, can be regarded as constant, the conductivity gradually increased. Ionic liquids of the two IR spectra analysis show its structure and synthetic route consistent with the structure of matter.


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