scholarly journals Densification and Microstructural Evolutions during Reaction Sintering of SiC-Si-C Powder Compacts

2011 ◽  
Vol 2011 ◽  
pp. 1-7 ◽  
Author(s):  
H. Asgharzadeh ◽  
N. Ehsani
Keyword(s):  
Powder Mixture ◽  
Coming Out ◽  
Sintering Temperature ◽  
Ceramic Materials ◽  
Carbon Powder ◽  
Reaction Sintering ◽  
Ceramic Specimen ◽  
Powder Compacts ◽  
Porous Sic ◽  
Sic Particle

Porous SiC-Si-C ceramics were produced by reaction sintering (RS) of silicon carbide, silicon, and carbon powder compacts in the temperature range of 1400–1600°C. The effects of chemical composition of the starting powder, initial SiC particle size, and reaction sintering temperature and duration on the densification and microstructure of ceramic materials were studied. The results showed that increasing the amount of Si and/or C powders in the starting powder mixture had a detrimental influence on the densification of ceramic material as a result of higher amount of remained silicon and carbon phases in the ceramic specimen. Increasing the RS temperature also degraded densification due to the melting of Si and coming out of it from compact during heating. Nevertheless, densification was improved by increasing the RS duration. Using nanometric SiC particles in the starting powder mixture improved the densification compared to that of micrometric ones especially at longer RS processing duration.

Effects of Compaction and Sintering Temperature to the Alloyability of FeCrCu Powder Mixture

2016 ◽  
Vol 1133 ◽  
pp. 264-268 ◽  
Author(s):  
Mujibur M. Rahman ◽  
S.R. Yogaswerarow
Keyword(s):  
Compressive Strength ◽  
Elevated Temperature ◽  
Iron Powder ◽  
Powder Mixture ◽  
Room Temperature ◽  
Sintering Temperature ◽  
Argon Gas ◽  
Die Compaction ◽  
Powder Forming ◽  
Powder Compacts

This paper presents the alloyability of FeCrCu powder compacts formed through warm powder compaction route. A lab-scale uni-axial die compaction rig was designed and fabricated which enabled the powder forming at elevated temperature. Iron powder ASC 100.29 was mechanically mixed with other alloying elements, i.e., copper (Cu) and chromium (Cr) as well as carbon (C) as additive for 60 minutes. Green samples were formed at 30°C (room temperature), 100°C, and 180°C through simultaneous upward and downward axial loadings. The defect-free green compacts were subsequently sintered in argon gas fired furnace at 900°C and 1000°C for 60 minutes at a rate of 5°C/minute. The alloyability of the sintered products was analyzed through XRD testing. The compressive strength of the sintered samples was also measured. The results revealed that FeCrCu alloy was formed at different intensity depended upon the forming and sintering temperature. The compressive strength was found to be highest for sample formed at 180°C and sintered at 1000°C.

Decrease of sintering temperature by CuO doping of the 0.8Pb(Mg1/3Nb2/3)O3-0.2PbTiO3 ceramics prepared by reaction-sintering method

2011 ◽  
Vol 209 (2) ◽  
pp. 254-261 ◽  
Author(s):  
Bijun Fang ◽  
Na Jiang ◽  
Chenlu Ding ◽  
Qingbo Du ◽  
Jianning Ding
Keyword(s):  
Sintering Temperature ◽  
Reaction Sintering ◽  
Sintering Method

scholarly journals Role of Sintering Temperature in Production of Nepheline Ceramics-Based Geopolymer with Addition of Ultra-High Molecular Weight Polyethylene

Materials ◽  
2021 ◽  
Vol 14 (5) ◽  
pp. 1077
Author(s):  
Romisuhani Ahmad ◽  
Mohd Mustafa Al Bakri Abdullah ◽  
Wan Mastura Wan Ibrahim ◽  
Kamarudin Hussin ◽  
Fakhryna Hannanee Ahmad Zaidi ◽  
...  
Keyword(s):  
Molecular Weight ◽  
High Molecular Weight ◽  
Sintering Temperature ◽  
Ceramic Materials ◽  
Microstructural Properties ◽  
Sintering Process ◽  
Final Microstructure ◽  
Change Of Microstructure ◽  
Ultra High Molecular Weight

The primary motivation of developing ceramic materials using geopolymer method is to minimize the reliance on high sintering temperatures. The ultra-high molecular weight polyethylene (UHMWPE) was added as binder and reinforces the nepheline ceramics based geopolymer. The samples were sintered at 900 °C, 1000 °C, 1100 °C, and 1200 °C to elucidate the influence of sintering on the physical and microstructural properties. The results indicated that a maximum flexural strength of 92 MPa is attainable once the samples are used to be sintered at 1200 °C. It was also determined that the density, porosity, volumetric shrinkage, and water absorption of the samples also affected by the sintering due to the change of microstructure and crystallinity. The IR spectra reveal that the band at around 1400 cm−1 becomes weak, indicating that sodium carbonate decomposed and began to react with the silica and alumina released from gels to form nepheline phases. The sintering process influence in the development of the final microstructure thus improving the properties of the ceramic materials.

Effects of TiN Content on Mechanical Properties and Microstructure of ATN Materials

2013 ◽  
Vol 589-590 ◽  
pp. 590-593 ◽  
Author(s):  
Min Wang ◽  
Jun Zhao
Keyword(s):  
Mechanical Properties ◽  
Mechanical Property ◽  
Fracture Toughness ◽  
Vickers Hardness ◽  
Bending Strength ◽  
Sintering Temperature ◽  
Ceramic Materials ◽  
Hot Press ◽  
Hot Press Sintering ◽  
Tin Content

In order to investigate the effects of TiN content on Al2O3/TiN ceramic material (ATN), the ATN ceramic materials were prepared of TiN content in 30%, 40%, 50%, 60% in the condition of hot press sintering. The sintering temperature is 1700°C, the sintering press is 32MPa, and the holding time are 5min, 10min, 15min. The effects of TiN content on mechanical properties and microstructure of ATN ceramic materials were investigated by analyzing the bending strength, hardness, fracture toughness. The results show that ATN50 has the best mechanical property, its bending strength is 659.41MPa, vickers hardness is 13.79GPa, fracture toughness is 7.06MPa·m1/2. It is indicated that the TiN content has important effect on microstructure and mechanical properties of ATN ceramic materials.

Effect of sintering temperature on the transport properties of La2Ce2O7 ceramic materials

2021 ◽  
Author(s):  
Bishnu Choudhary ◽  
Sharmistha Anwar ◽  
Medvedev Dmitry Andreevich ◽  
Laxmidhar Besra ◽  
Shahid Anwar
Keyword(s):  
Transport Properties ◽  
Sintering Temperature ◽  
Ceramic Materials

scholarly journals SYNTHESIS AND CHARACTERIZATION OF GREENER CERAMIC MATERIALS WITH LOWER THERMAL CONDUCTIVITY USING OLIVE MILL SOLID BYPRODUCT

2020 ◽  
Vol 1 ◽  
pp. 96-106 ◽  
Author(s):  
Xenofon Spiliotis ◽  
Vayos Karayannis ◽  
Stylianos Lamprakopoulos ◽  
Konstantinos Ntampegliotis ◽  
George Papapolymerou
Keyword(s):  
Thermal Conductivity ◽  
Solid Waste ◽  
Energy Savings ◽  
Sintering Temperature ◽  
Ceramic Body ◽  
Ceramic Materials ◽  
Raw Material ◽  
Gravimetric Analysis ◽  
Olive Mill Solid Waste ◽  
Olive Mill

In the current research, the valorization of olive mill solid waste as beneficial admixture into clay bodies for developing greener ceramic materials with lower thermal conductivity, thus with increased thermal insulation capacity towards energy savings, is investigated. Various clay/waste mixtures were prepared. The raw material mixtures were characterized and subjected to thermal gravimetric analysis, in order to optimize the mineral composition and maintain calcium and magnesium oxides content to a minimum. Test specimens were formed employing extrusion and then sintering procedure at different peak temperatures. Apparent density, water absorption capability, mechanical strength, porosity and thermal conductivity were determined on sintered specimens and examined in relation to the waste percentage and sintering temperature. The experimental results showed that ceramic production from clay/olive-mill solid waste mixtures is feasible. In fact, the mechanical properties are not significantly impacted with the incorporation of the waste in the ceramic body. However, the thermal conductivity decreases significantly, which can be of particular interest for thermal insulating materials development. Furthermore, the shape of the produced ceramics does not appear to change with the sintering temperature increase.

Preparation and Investigation on Properties of the MgTiO3-CaTiO3 Microwave Ceramic Materials

2014 ◽  
Vol 997 ◽  
pp. 419-423 ◽  
Author(s):  
Li Dong ◽  
Gui Xia Dong ◽  
Yuan Yuan Li ◽  
Xi Zhang
Keyword(s):  
Dielectric Constant ◽  
Sintering Temperature ◽  
Ceramic Materials ◽  
Volume Density ◽  
Second Phase ◽  
Pressureless Sintering ◽  
Solid Reaction ◽  
Reaction Method ◽  
Microwave Ceramic ◽  
Sintering Method

The MgTiO3 and CaTiO3 powders were synthesized by solid reaction method, and MgTiO3-CaTiO3 ceramic was prepared using pressureless sintering method. The experiment prepared MgTiO3-CaTiO3 ceramics with high compactness and stable permittivity by the way of changing the mole ratio of MgTiO3 and CaTiO3 to investigate the effect of CaTiO3 on the performances of MgTiO3-CaTiO3 ceramics. The results show that Mg2TiO4 formed as second phase during sintering. Volume density and dielectric constant of MgTiO3-CaTiO3 ceramics with 10%mol CaTiO3 reach maximum of 3.612g/cm3 and 17.8, respectively, under 1460°C sintering temperature. And for the MgTiO3-CaTiO3 ceramics with 5%mol CaTiO3 the maximum values which are 3.5g/cm3 and 16.6, respectively, appear under 1510°C sintering temperature.

Multicomponent toughened ceramic materials obtained by reaction sintering

1985 ◽  
Vol 20 (8) ◽  
pp. 2711-2718 ◽  
Author(s):  
M. F. Melo ◽  
J. S. Moya ◽  
P. Pena ◽  
S. De Aza
Keyword(s):  
Ceramic Materials ◽  
Reaction Sintering
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