Evaluation of Color Changes of Dental Luting Materials in Food Colorant Solutions

2017 ◽  
Vol 40 (9) ◽  
pp. 503-509 ◽  
Author(s):  
Canan Akay ◽  
Merve Ç. Taniş

Background The purpose of this study was to compare the color stability and water absorption of 3 commercially available resin cements in vitro by storing them in 0.15% erythrosine, dark brown and sunset yellow for 30 days. Methods 2 self-adhesive resin cements and 1 dual/light curing, resin-based dental luting material were evaluated (total 120 samples). The CIE L, a, b of 10 mm diameter-2.0 mm height disk shaped samples was measured using a spectrophotometer for color stability on a white background, 10 mm diameter-1.0 mm height disk shaped samples were measured for water absorption before and after storage in food colorant solutions. Results The self-adhesive resin cement-sunset yellow group caused the most severe discoloration (27.89 ± 3.64) that is clinically unacceptable. The lowest discoloration was seen in the self-adhesive resin cement control group (3.35 ± 1.13). The highest water absorption was observed in the self-adhesive resin cement-dark brown group (2.41 ± 0.60) and the lowest water absorption in the dental luting material-control group (0.65 ± 0.17). Conclusions: Storage food colorant solutions affected the color stability and water absorption of different resin cement materials.

Author(s):  
Masoumeh Hasani Tabatabae ◽  
Fatemeh Matinfard ◽  
Elham Ahmadi ◽  
Ladan Ranjbar Omrani ◽  
Farzaneh Sadeghi Mahounak

Objectives: Color change of cements over time can be detected through translucent ceramic veneers, compromising the aesthetic appearance of restorations in the long-term. This study aimed to assess the color stability of ceramic laminate veneers cemented with self-adhesive resin cements after accelerated aging. Materials and Methods: In this study, 21 IPS e.max ceramic discs, measuring 8mm in diameter and 0.7 mm in thickness, were fabricated and divided into three groups (n=7) for the application of Choice 2 total-etch light-cure resin cement, RelyX U200 dual-cure self-adhesive resin cement, and SpeedCEM self-cure self-adhesive resin cement. The ceramic discs in each group were cemented on the prepared facial surface of bovine teeth. The color parameters were assessed using a spectrophotometer. Subsequently, the samples were subjected to accelerated aging for 100 hours, and the color parameters were measured again. The data were analyzed using two-way repeated-measures analysis of variance (ANOVA) and Tamhane’s post-hoc test (P<0.05). Results: Aging significantly affected the ceramic laminate color parameters in all three groups (P<0.05). SpeedCEM cement showed the lowest color stability (∆E=4.2) after aging, and its color change was clinically unacceptable (∆E>3.5). The color change of the other two groups was clinically acceptable (1<∆E<3.5). Conclusion: The self-adhesive dual-cure cement showed color stability comparable to that of the total-etch light-cure cement for cementation of IPS e.max ceramic laminates. The color stability of both cements was superior to that of the self-adhesive self-cure cement.


Materials ◽  
2019 ◽  
Vol 12 (20) ◽  
pp. 3321 ◽  
Author(s):  
Dae-Sung Kim ◽  
Jong-Ju Ahn ◽  
Eun-Bin Bae ◽  
Gyoo-Cheon Kim ◽  
Chang-Mo Jeong ◽  
...  

The purpose of this study was to evaluate the effect of non-thermal atmospheric pressure plasma (NTP) on shear bond strength (SBS) between yttria-stabilized tetragonal zirconia polycrystal (Y-TZP) and self-adhesive resin cement. For this study, surface energy (SE) was calculated with cube-shaped Y-TZP specimens, and SBS was measured on disc-shaped Y-TZP specimens bonded with G-CEM LinkAce or RelyX U200 resin cylinder. The Y-TZP specimens were classified into four groups according to the surface treatment as follows: Control (no surface treatment), NTP, Sb (Sandblasting), and Sb + NTP. The results showed that the SE was significantly higher in the NTP group than in the Control group (p < 0.05). For the SBS test, in non-thermocycling, the NTP group of both self-adhesive resin cements showed significantly higher SBS than the Control group (p < 0.05). However, regardless of the cement type in thermocycling, there was no significant increase in the SBS between the Control and NTP groups. Comparing the two cements, regardless of thermocycling, the NTP group of G-CEM LinkAce showed significantly higher SBS than that of RelyX U200 (p < 0.05). Our study suggests that NTP increases the SE. Furthermore, NTP increases the initial SBS, which is higher when using G-CEM LinkAce than when using RelyX U200.


2018 ◽  
Vol 43 (4) ◽  
pp. 391-397 ◽  
Author(s):  
RC Ferreira-Filho ◽  
C Ely ◽  
RC Amaral ◽  
JA Rodrigues ◽  
J-F Roulet ◽  
...  

SUMMARY Objective: The purpose of this study was to investigate the immediate and three-month water storage behavior of adhesives when used for immediate dentin sealing (IDS). Methods and Materials: Four adhesive systems were used to perform IDS: a one-step self-etch (Xeno V), a two-step self-etch (Clearfil SE Bond), a two-step etch-and-rinse (XP Bond), and a three-step etch-and-rinse (Optibond FL). For the control group, IDS was not performed. The self-adhesive resin cement RelyX Unicem was used for the luting procedures. After seven days of water storage, specimens (n=6) were sectioned into beams (n=5) with an approximately 1-mm2 cross-sectional area. Half of the specimens were tested in tension after seven days of water storage at 37°C, while the other half was stored for three months prior to testing in tension using a universal testing machine (1 mm/min). The failure pattern was determined using a stereomicroscope and scanning electron microscopy. Microtensile bond strength (μTBS) data were statistically analyzed by two-way analysis of variance and Tukey post hoc test (α=0.05). Results: After seven days, the control group presented the lowest μTBS but did not differ from XP Bond and Clearfil SE Bond. After three months, there was no μTBS difference between the IDS groups and the control. Conclusions: After seven days of water storage, the groups with IDS presented higher μTBS values than the control group, although XP Bond and Clearfil SE Bond did not present significant differences. However, after three months of storage in water, IDS groups did not differ significantly from control group, which did not receive IDS.


2021 ◽  
Vol 12 (1) ◽  
pp. e36-e36
Author(s):  
Paria Dehghanian ◽  
Fereshteh Shafiei ◽  
Nasrin Kianimanesh

Introduction: Considering the recent trend to use mineral trioxide aggregate (MTA) and Biodentine and resin cements, more conservative approaches concurrent with adequate bond strength have always been requested. The present study aimed to evaluate the effect of pretreatment with Er:YAG laser etching versus acid-etching for 5 and 15 seconds on the micro shear bond strength of self-adhesive resin cement (SRC) to MTA and Biodentine. Materials and Methods: Forty-eight samples of each cement (MTA and Biodentine) were prepared and distributed into four groups based on surface pretreatment: 1) control, no treatment; 2) Er:YAG laser etching with energy of 60 mJ; 3) 5-second acid-etching; 4) 15-second acid-etching. All specimens were cemented using SRC. Microshear bond strengths were tested following 24-hour water storage. Debonded specimens were examined and surface topography was assessed using an atomic force machine (AFM). Data analysis was performed using the two-way ANOVA and Tukey multiple comparisons test. Results: The three testing groups of laser etch and 5-s and 15-s acid-etch demonstrated a significantly higher SBS than the control group (P<0.05) with negligible differences among them (P > 0.05). Furthermore, Biodentine showed better adhesive bonding than MTA in all groups. Conclusion: Laser etching of 60 mJ and 5-s acid-etching were as beneficial as 15-s acid-etching in terms of bond strength of SRC to MTA and Bodentine.


2010 ◽  
Vol 22 (1) ◽  
Author(s):  
Myrna Nurlatifah Zakaria ◽  
Moch. Richata Fadil ◽  
Milly Armilia

Resin based luting cement application generally requires pre-treatment procedure such as etching and adhesive application prior to cementation. This multi-step application technique might compromise bonding alternative effectiveness and is time consuming. An alternative for multi-step resin cement is the self-adhesive resin cement that combines the use of etch, adhesive and cement in one single application. The objective of this study was to compare the bonding effectiveness of the multi-step resin cement and the self-adhesive resin cement using tensile bond strength method towards indirect composite block dentin surface. This study was a true experimental research conducted by in vitro method on 30 flat dentin surfaces created from extracted lower premolars samples. Samples were divided into two groups, each 15 samples for multi-step and self-adhesive resin cements. An indirect composite block (2x2x10 mm) was then cemented to each dentin surface using multi-step resin cement (Rely X ARC, 3M ESPE) or self-adhesive resin cement (Rely X Unicem, 3M ESPE) according to manufacture’s instruction. Samples were storage for 24 hours in saline water and tensile bond strength of each samples were tested using the LRX Plus Lyod Instrument at 1 mm/minute speed. The result of the study concluded that the tensile bond strength of multi-step resin cement towards indirect composite restoration and dentin surface was significantly higher than the self-adhesive resin cement.


2019 ◽  
Vol 21 (5) ◽  
pp. 477-482
Author(s):  
Lucas Campagnaro Maciel ◽  
Amanda Pádua Proeza ◽  
Hélyda Coelho Guimarães Balbino ◽  
Marcela Moráo Corteletti ◽  
Ricardo Huver De Jesus ◽  
...  

AbstractThe evolution of dental materials and the improvement of ceramic systems stimulated the increased use of Y-TZP zirconia-based ceramics. Despite the excellent mechanical performance, this material has low adhesion potential. The objective of this work was to evaluate the surface treatments and resin cements influence on bond strength between Y-TZP zirconia and composite resin interface. A total of 60 blocks of Y-TZP zirconia (3x8x8mm) were prepared and divided into 3 groups according to the surface treatments: (C) control - extra fine diamond bur, (J) sandblasting with Al2O3 and (JP) sandblasting with Al2O3 + ceramic primer. Each group was subdivided into two groups according to type of resin cement used for cementing composite resin discs (2mm thick x 5mm diameter): self-adhesive and conventional (n=10). The samples were stored in distilled water for 24 hours at 37±1°C in a incubator and subsequently submitted to the shear bond test to determine the bond strength (RU). There was no significant difference in RU among the  surface treatments when using conventional resin cement. For the self-adhesive resin cement, Al2O3 blasting and Al2O3 + primer blasting increased the RU but did not present significant differences between them (p<0.05). Comparing the cements, it was observed that regardless of the surface treatment, the highest values were for the self-adhesive resin cement (p<0.05). Application of the primer after blasting with Al2O3 did not increase RU. Keywords: Dental Prosthesis. Ceramics. Dental cements. Shear Strength.  ResumoA evolução dos materiais odontológicos e o aprimoramento dos sistemas cerâmicos impulsionaram o aumento da utilização da cerâmica a base de zircônia Y-TZP. Apesar do excelente desempenho mecânico, este material apresenta baixo potencial de adesão. O objetivo deste trabalho foi avaliar a influência dos tratamentos de superfícies e dos cimentos resinosos na resistência de união entre a interface zircônia Y-TZP e resina composta. Foram confeccionados 60 blocos de zircônia Y-TZP (3x8x8 mm) e divididos em 03 grupos de acordo com os tratamentos de superfícies que receberam: (C) controle - ponta diamantada extrafina, (J) jateamento com Al2O3 e (JP) jateamento com Al2O3 + primer cerâmico. Cada grupo foi subdividido em dois novos grupos de acordo com tipo de cimento resinoso utilizado para cimentação de discos de resina composta (2mm de espessura x 5mm de diâmetro): autoadesivo e resinoso convencional (n=10). As amostras foram armazenadas em água destilada por 24 horas a 37±1°C em estufa e posteriormente submetidas ao teste de cisalhamento para averiguar a resistência de união (RU). Não houve diferença significativa na RU entre os tratamentos de superfície quando utilizado o cimento resinoso convencional. Para o cimento resinoso autoadesivo o jateamento com Al2O3 e o jateamento de Al2O3 + primer aumentaram a RU porém não apresentaram diferenças significativas entre si (p<0,05). Comparando os cimentos observou-se que, independente do tratamento de superfície, os maiores valores foram para o cimento resinoso autoadesivo (p<0,05). A aplicação do primer após o jateamento com Al2O3 não proporcionou aumento da RU. Palavras-chave: Prótese Dentária. Cerâmica. Cimentos Dentários. Resistência ao Cisalhamento.


2015 ◽  
Vol 2015 ◽  
pp. 1-6 ◽  
Author(s):  
Jin-Soo Ahn ◽  
Young-Ah Yi ◽  
Yoon Lee ◽  
Deog-Gyu Seo

Purpose. This study was conducted to evaluate the effects of different phosphate monomer-containing primers on the shear bond strength between yttria-tetragonal zirconia polycrystal (Y-TZP) ceramics and MDP-containing self-adhesive resin cement.Materials and Methods. Y-TZP ceramic surfaces were ground flat with #600-grit SiC paper and divided into six groups (n=10). They were treated as follows: untreated (control), Metal/Zirconia Primer, Z-PRIME Plus, air abrasion, Metal/Zirconia Primer with air abrasion, and Z-PRIME Plus with air abrasion. MDP-containing self-adhesive resin cement was applied to the surface-treated Y-TZP specimens. After thermocycling, a shear bond strength test was performed. The surfaces of the Y-TZP specimens were analyzed under a scanning electron microscope. The bond strength values were statistically analyzed using one-way analysis of variance and the Student–Newman–Keuls multiple comparison test (P<0.05).Results. The Z-PRIME Plus treatment combined with air abrasion produced the highest bond strength, followed by Z-PRIME Plus application, Metal/Zirconia Primer combined with air abrasion, air abrasion alone, and, lastly, Metal/Zirconia Primer application. The control group yielded the lowest results (P<0.05).Conclusion. The application of MDP-containing primer resulted in increased bond strength between Y-TZP ceramics and MDP-containing self-adhesive resin cements.


2017 ◽  
Vol 2017 ◽  
pp. 1-6 ◽  
Author(s):  
Adricyla Teixeira Rocha ◽  
Leticia Machado Gonçalves ◽  
Ana Júlia de Carvalho Vasconcelos ◽  
Etevaldo Matos Maia Filho ◽  
Ceci Nunes Carvalho ◽  
...  

Aim. The aim of the study was to evaluate, by means of the push-out test, the effect of the anatomical customization of the fiber post on the bond strength of a self-adhesive resin cement. Methods. Twelve endodontically treated, human, upper central incisors were randomly divided into two groups (n=6): control (glass fiber posts cemented with Relyx® U200) and customized (glass fiber posts anatomically customized with translucent composite resin cemented with Relyx U200). The roots were sectioned into three slices, cervical, middle, and apical, and photographed with a digital camera attached to a stereomicroscopic loupe. The images were analyzed by software, for evaluation of the cement line. The slices were subsequently submitted to the push-out test until the post had completely extruded, and the fracture mode was analyzed with a stereomicroscopic loupe. Results. The results showed significant differences between the groups in the different root thirds in relation to the area occupied by air bubbles (p<0.05). Bond strength, when all the thirds are considered, was 8.77 ± 4.89 MPa for the control group and 16.96 ± 4.85 MPa for the customized group. Conclusion. The customized group showed greater bond resistance than the control group and a more uniform cement layer.


2009 ◽  
Vol 25 (5) ◽  
pp. 601-604 ◽  
Author(s):  
Michael Behr ◽  
Martin Rosentritt ◽  
Jutta Wimmer ◽  
Reinhold Lang ◽  
Carola Kolbeck ◽  
...  

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