Semi-Ebonite. Part 2
Abstract In Part 1 (Rubber Chem. and Tech., 8, 554 (1935)) frequent reference was made to the volatile products emitted during the aging of semi-ebonite under different conditions. In this section an experiment is described wherein the various products were detected and some attempt made to estimate the relative amounts of each. The experiment in its original form presented considerable difficulty, and many disappointments were experienced before a modified apparatus was finally adopted. Experimental Method.—Eight test-pieces, one from each of the accelerated cures (see Part 1), were cut to a convenient size, six inches by one inch. The test-pieces were carefully weighed and their thickness determined as the average of several readings on the micrometer. The strips were suspended from a bent glass rod projecting from a cork-bearing inlet and outlet tubes (see Fig. 5). The cork was then inserted in a clean conical flask and the latter sealed with wax until it withstood a considerable vacuum. The flask was placed in a Geer oven automatically maintained at 70° C. The outlet tube was attached to an absorption train and the inlet tube to a purifying train.