Tensile Stress—Strain Measurements for Characterization of Gum Elastomers and Filled Compounds

1990 ◽  
Vol 63 (4) ◽  
pp. 624-636 ◽  
Author(s):  
N. Nakajima ◽  
M. H. Chu ◽  
R. Babrowicz

Abstract For a gum elastomer in its amorphous, isotropic state, shear modulus and tensile modulus are related with a factor of three. This relation is maintained in the range of temperature and time scale defining the rubbery region of the material behavior. When a large deformation is imposed, for example, in tensile stress—strain measurements, the above relation may still be preserved, if the nonlinear behavior can be linearized. The strain—time correspondence principle is the linearization scheme of this work. When a gum elastomer contains various structural constraints, the factor three relation does not apply, even after the application of the above linearization scheme. Example of constraints are excessive amounts of long branches, gel, molecular associations, and reinforcing fillers. These constraints usually make the factor larger than three. This is because the constraints make the large, elongational deformation more difficult to achieve compared to shear deformation. An example of gum elastomer in this work is a polyethylacrylate containing a significant amount of gel. With this polymer, both the presence of gel and the molecular association act as the constraints. However, when 50 phr of carbon blacks are added, the fillers do not act as strong constraints as they do when they are in the diene rubbers. This is because the polyethylacrylate is known to have a weaker affinity to carbon black compared to the diene rubbers. Triblock copolymers, styrene—isoprene—styrene, were examined according to the above treatment; 25% polystyrene copolymer exhibited crosslink-like behavior by the polystyrene domains. However, 14% polystyrene copolymers acted as if they are no crosslinks. When these copolymers are diluted to 44% with an addition of 56% tackifier, the ratio of tensile to shear modulus became less than three. The styrene domains must have effective crosslinks at the small shear deformation, but at large tensile deformations such crosslinks must not be present.

2011 ◽  
Vol 284-286 ◽  
pp. 1969-1973
Author(s):  
Xiao Ling Hu ◽  
Yong Ouyang ◽  
Xiong Zhou ◽  
Wen Bo Luo

The tensile stress-strain relationship of rubbers is fairly linear and can be used for obtaining tensile modulusE. In this work we analyzed the tensile stress-strain relationship of filled rubber experimentally and employed the extended 2D homogenization method to compute the modulus of the carbon black (CB) filled rubbers with various CB volume fractions ranging from 5% to 25%. The results reveal that the modulus of CB-filled rubbers increased with the increase in CB volume fraction and in CB aggregation.


1997 ◽  
Vol 119 (4) ◽  
pp. 380-386 ◽  
Author(s):  
J. N. Scheuring ◽  
A. F. Grandt

This paper evaluates changes in the behavior of aircraft materials which result from aging and/or corrosion that occurs during long periods of service usage. The primary objective was to determine whether damage tolerant analyses for older aircraft should employ updated properties that more accurately represent the current state of the material, or if the virgin material properties continue to properly characterize the aged/corroded alloy. Specifically, tensile stress-strain curves, cyclic stress life (SN) tests, and fatigue crack growth tests were used to characterize the “aged aircraft” material. These properties were compared with handbook properties for virgin material of the same pedigree. The aluminum alloys tested were obtained from fuselage and wing panels of retired KC-135 aircraft. Computer controlled tests were conducted using specimens machined from the retired aircraft components. Different configurations were used to observe the effects of aging and/or corrosion on material behavior. In the crack growth specimens, various levels of corrosion were observed, thus the crack growth rates could be categorized as a function of the level of corrosion present. The SN and da/dN-ΔK curves for the “aged” only materials were compared with the fatigue properties of virgin material of the same alloy. Similar comparisons were performed for the tensile stress-strain properties.


1997 ◽  
Vol 67 (9) ◽  
pp. 654-664 ◽  
Author(s):  
Jin-Lian Hu ◽  
Yi-Tong Zhang

Many fabric mechanics researchers have reported that specimens being tested on the KES shear tester are not subjected to pure shear deformation; therefore, test results cannot lead directly to a determination of the fabric shear modulus and stress/strain relationship, particularly in the nonlinear range of stress-strain. Combined with finite element analysis, this paper presents an analytical solution for the distribution of shear stresses and strains in fabric specimens tested on the kes tester. A fabric is treated as an orthotropic sheet during the analysis, which leads to a closed-form solution for the shear modulus as a function of fabric tensile and shear moduli from the kes shear test. A modified shear stress-strain relationship can also be derived. From calculations for fabrics used here, the difference between modified and tested shear modulus values is about 25–30%. The study also suggests that although the shear modulus and curves obtained on the kes shear tester are significantly different from those under the pure shear state, the kes results can still reflect the nature of a fabric under shear deformation and are valid for general objective evaluations. The exact shear stress-strain relationship and actual shear modulus may be modified only when they are required for fabric complex deformation analysis.


1974 ◽  
Vol 47 (4) ◽  
pp. 778-787 ◽  
Author(s):  
N. Nakajima ◽  
E. A. Collins ◽  
P. R. Kumler

Abstract The dynamic viscoelastic properties of four samples of butadiene—acrylonitrile raw elastomers, were obtained with a Rheovibron at 110 Hz and temperature range of −80 to 160°C. The complex properties were in agreement with the master curves obtained previously from stress-strain measurements. A master curve encompassing 13 decades of time was constructed using data from Mooney rheometer shear stress-strain, MTS high speed tensile stress-strain, and the Rheovibron. The master curve represents the rubbery region of viscoelastic behavior in terms of time, temperature, and the magnitude of deformation up to the breaking point. This study demonstrates that corresponding states can be found between small (ca. 1 per cent) and large deformation up to break (e.g., 1400 per cent).


1988 ◽  
Vol 61 (1) ◽  
pp. 137-148 ◽  
Author(s):  
N. Nakajima ◽  
J. J. Scobbo

Abstract This work is based on data previously obtained by the tensile stress-strain and dynamic-shear measurements with several gum rubbers and carbon-black-filled compounds. The gum rubbers were three NBR's of different molecular architecture and two SBR's, one of which was oil extended. The compounds contained 40 phr of N550 carbon black. Through the data treatment procedure developed in this work, the strain amplifications in the dynamic shear and tensile stress-strain measurements were evaluated with the uncrosslinked compounds. Each compound showed a unique pattern of strain amplification.


1985 ◽  
Vol 58 (2) ◽  
pp. 407-420 ◽  
Author(s):  
G. R. Hamed ◽  
J. H. Song

Abstract The anisotropy induced in an ungelled SBR elastomer upon large scale deformation and the rate at which the deformed elastomer returns to its original state upon removal of the deforming force were investigated. In these experiments, a standard birefringence technique was unsuitable for measuring the extent of orientation after release, however, tensile stress-strain measurements successfully showed the presence of anisotropy. After prestraining and then releasing, samples have an initial resistance to deformation which is the same both parallel and perpendicular to the prestraining direction. However, testpieces cut parallel with the prestraining direction show stress-strain curves that lie above those for cross-cut specimens at high elongations, while cross-cut samples have stress-strain curves remarkably similar to those of the isotropic controls. With increasing time after prestraining or for larger prestrains, the normalized anisotropy, at intermediate elongations, becomes negative; that is, in this region, it becomes easier to deform “parallel” specimens than to deform “perpendicular” specimens. This phenomenon is proposed to be the result of two opposing entanglement networks—an original one, which remains in tension, and a compressed one, which was formed by chains re-entangling while the sample was extended. Although the shapes of the “parallel” and “perpendicular” stress-strain curves may be quite different, the total energy required to rupture the samples in both cases is similar. Finally, for a lightly crosslinked sample, it is demonstrated that after various prestrains, hold times, and relaxation times before testing after prestraining, the normalized anisotropy is a unique function of the residual extension at the moment when the specimens were tested.


1982 ◽  
Vol 4 (2) ◽  
pp. 103-106 ◽  
Author(s):  
P. G. Krouwel ◽  
A. Harder ◽  
N. W. F. Kossen

2020 ◽  
Vol 29 ◽  
pp. 2633366X2095872
Author(s):  
Yang Wei ◽  
Mengqian Zhou ◽  
Kunpeng Zhao ◽  
Kang Zhao ◽  
Guofen Li

Glulam bamboo has been preliminarily explored for use as a structural building material, and its stress–strain model under axial loading has a fundamental role in the analysis of bamboo components. To study the tension and compression behaviour of glulam bamboo, the bamboo scrimber and laminated bamboo as two kinds of typical glulam bamboo materials were tested under axial loading. Their mechanical behaviour and failure modes were investigated. The results showed that the bamboo scrimber and laminated bamboo have similar failure modes. For tensile failure, bamboo fibres were ruptured with sawtooth failure surfaces shown as brittle failure; for compression failure, the two modes of compression are buckling and compression shear failure. The stress–strain relationship curves of the bamboo scrimber and laminated bamboo are also similar. The tensile stress–strain curves showed a linear relationship, and the compressive stress–strain curves can be divided into three stages: elastic, elastoplastic and post-yield. Based on the test results, the stress–strain model was proposed for glulam bamboo, in which a linear equation was used to describe the tensile stress–strain relationship and the Richard–Abbott model was employed to model the compressive stress–strain relationship. A comparison with the experimental results shows that the predicted results are in good agreement with the experimental curves.


2003 ◽  
Vol 18 (9) ◽  
pp. 2068-2078 ◽  
Author(s):  
A. DiCarlo ◽  
H. T. Y. Yang ◽  
S. Chandrasekar

A method for determining the stress–strain relationship of a material from hardness values H obtained from cone indentation tests with various apical angles is presented. The materials studied were assumed to exhibit power-law hardening. As a result, the properties of importance are the Young's modulus E, yield strength Y, and the work-hardening exponent n. Previous work [W.C. Oliver and G.M. Pharr, J. Mater. Res. 7, 1564 (1992)] showed that E can be determined from initial force–displacement data collected while unloading the indenter from the material. Consequently, the properties that need to be determined are Y and n. Dimensional analysis was used to generalize H/E so that it was a function of Y/E and n [Y-T. Cheng and C-M. Cheng, J. Appl. Phys. 84, 1284 (1999); Philos. Mag. Lett. 77, 39 (1998)]. A parametric study of Y/E and n was conducted using the finite element method to model material behavior. Regression analysis was used to correlate the H/E findings from the simulations to Y/E and n. With the a priori knowledge of E, this correlation was used to estimate Y and n.


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