Studies on Morphologies and Mechanical Properties of Multi-walled Carbon Nanotubes/Epoxy Matrix Composites

2010 ◽  
Vol 31 (5) ◽  
pp. 1237-1240 ◽  
Author(s):  
Min-Kang Seo ◽  
Joon-Hyung Byun ◽  
Soo-Jin Park
2007 ◽  
Vol 334-335 ◽  
pp. 797-800
Author(s):  
Peng Cheng Ma ◽  
Jang Kyo Kim ◽  
Ben Zhong Tang

This paper presents a method for chemical functionalization of CNTs through the combined process of UV/O3 treatment and silanization process. FT-IR and TEM were employed to characterize the changes in surface functionalities and morphology. The results indicate improved dispersion and attachment of silane molecules on the surface of CNTs. Epoxy matrix nanocomposites containing functionalized CNTs showed much better dispersion with associated higher mechanical properties than those without functionalization. These findings confirmed the improved interfacial interactions due to covalent bonding between the functionalized CNTs and epoxy resin.


2018 ◽  
Vol 7 (4.36) ◽  
pp. 1149 ◽  
Author(s):  
Nguyen Tuan Anh ◽  
Nguyen Quang Tung ◽  
Bach Trong Phuc ◽  
Nguyen Xuan Canh

In this study, the flame retardants epoxy nanocomposites were prepared by combining mechanical stir and sonication of epoxy Epikote 240 (EE240) resin, chlorinated paraffin, atimony oxide, multi-walled carbon nanotubes (MWCNTs) and montmotillonite clay. Resultants of CNTs, montmorillonite and flame retardant additives were investigated limiting oxygen (LOI) and UL-94, combustion rate. The SEM, FE-SEM, TEM were measured to analyze the dispersion of MWCNTs and montmorillonite clay in epoxy matrix. The mechanical properties including tensile strength, compressive strength, flexural strength and impact strength Izod were studied. The results of testing burning and mechanical properties indicated that CNTs were more efficient than clay in improving the flame retardancy of materials. The dispersion method combining of mechanical stir and sonication is the good choice to distribute additive agents into epoxy matrix.  


2011 ◽  
Vol 13 (2) ◽  
pp. 62-69 ◽  
Author(s):  
Maria Wladyka-Przybylak ◽  
Dorota Wesolek ◽  
Weronika Gieparda ◽  
Anna Boczkowska ◽  
Ewelina Ciecierska

The effect of the surface modification of carbon nanotubes on their dispersion in the epoxy matrix Functionalization of multi-walled carbon nanotubes (MWCNTs) has an effect on the dispersion of MWCNT in the epoxy matrix. Samples based on two kinds of epoxy resin and different weight percentage of MWCNTs (functionalized and non-functionalized) were prepared. Epoxy/carbon nanotubes composites were prepared by different mixing methods (ultrasounds and a combination of ultrasounds and mechanical mixing). CNTs modified with different functional groups were investigated. Surfactants were used to lower the surface tension of the liquid, which enabled easier spreading and reducing the interfacial tension. Solvents were also used to reduce the liquid viscosity. Some of them facilitate homogeneous dispersion of nanotubes in the resin. The properties of epoxy/nanotubes composites strongly depend on a uniform distribution of carbon nanotubes in the epoxy matrix. The type of epoxy resin, solvent, surfactant and mixing method for homogeneous dispersion of CNTs in the epoxy matrix was evaluated. The effect of CNTs functionalization type on their dispersion in the epoxy resins was evaluated on the basis of viscosity and microstructure studies.


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