scholarly journals Agglomeration of hydrolyzed collagen with blackberry pulp in a fluidized bed

Author(s):  
Thayná R Viegas ◽  
Osvaldir Pereira Taranto

Hydrolyzed collagen (HC) is a fine powder applied in the pharmaceutical and food industries which has shown good results in the treatment of diseases related to bones, skin and joints. In this  study, HC particles were agglomerated in order to increase particle size, optimizing its use as a food ingredient, its handling and its storage. Agglomeration is a process that not only enlarge the size of fine particles, but also improves its properties, such as instantanization time and flowability. The aim of this work was the agglomeration of HC in a fluidized bed having blackberry pulp as a liquid binder. A full factorial design 22 was used to study the effect of the temperature of the fluidizing air (60, 70, 80ºC) and the flow rate of the liquid binder (0.8, 1.2, 1.6 mL/min) on the process yield, mean particle size, water activity and total anthocyanins content. It was observed that anthocyanins content from the blackberry pulp had higher values with lower temperatures. Water activity had lower values with higher temperatures, but in all conditions, it was lower than 0.6. The enlargement of the granules was observed in all conditions studied, increasing up to 275%. Process yield varied from 67,9 to 80,0%. In all conditions, the instantanization time and flowability improved compared to hydrolyzed collagen before agglomeration.Keywords: hydrolyzed collagen; agglomeration; granulation; fluidized bed; blackberry pulp   

Author(s):  
Juliana G Rosa ◽  
R. F. Nascimento ◽  
K. Andreola ◽  
O. P. Taranto

Acacia gum is an important food emulsifier that presents poor instant properties which can be improved by fluidized bed agglomeration. This study investigated the influence of drying conditions on particle growth kinetics using an in-line particle size monitoring by spatial filter velocimetry. The drying conditions varied according to the binder flow rate and the fluidizing air temperature. The particle growth kinectis showed drying conditions dependence. At mild drying conditions the growth rate and the process yield were higher. The in-line particle size monitoring was useful to observe the influence of the drying conditions on the growth kinetics.Keywords: fluidized bed agglomeration; acacia gum; particle growth kinectis; in-line monitoring.  


Author(s):  
Shohei Koizumi ◽  
Koji Takasu ◽  
Hidehiro Koyamada ◽  
Hiroki Suyama

It has been clarified that the particle shape and particle size distribution of fine aggregate have influenced the fresh properties of concrete and mortar in the past research. But it has not been sufficiently studied how each particle size and particle size distribution of fine aggregate affects the fresh properties of mortar and concrete. In this study, we adjusted the particle size of fine aggregate, and evaluated fresh properties of mortar by indicators. We investigated the fluidity of mortar, which changed depending on the composition of particle size distribution. In addition, the behavior of fresh properties of mortar contained powder substituted as part of cement and fine aggregate adjusted particle size distribution was compared with that when no powder was mixed. Its behavior was discussed. It became clear that, the factor influencing the fluidity varied depending on the composition of particle size distribution. The influence of fine particles on fluidity of mortar varied depending on the content of fine particle and the particles size distribution. When combined with the large particles, the fluidity was improved as compared with the combination with the intermediate particles. In addition, the same tendency as in powder-free mixing was confirmed at powder mixing and increase rate of the relative flow area ratio when fly ash was contained became larger than when the limestone fine powder was contained.


2014 ◽  
Vol 3 (5) ◽  
pp. 83 ◽  
Author(s):  
Sandro Cid-Ortega ◽  
Jose Angel Guerrero-Beltran

<p>The effect of average particle size (APS), type of solvent, and extraction times (ET) on the physicochemical (moisture, pH, total soluble solids (TSS), titratable acidity, color, water activity (<em>a<sub>w</sub></em>), density), and phytochemical (total anthocyanins and phenols content)propertiesin <em>Hibiscus sabdariffa</em> (Roselle) calyces was analyzed. The phytochemical properties evaluation was performed using a factorial design 2×3×3: two APS (median diameters, d<sub>50</sub>, of 0.55 ± 0.016 (fine powder) and 0.97 ± 0.034 (ground powder) mm), three solvents (water, 2% citric acid, and 50% ethanol) and three ET (30, 45, and 60 min). All extractions were performed at 50 °C. The APS was determined by sieve analysis using Tyler sieves of different number of mesh. Regarding physicochemical properties, no significant differences (p &gt; 0.05) were observed in moisture content, pH, and titratable acidity; however, the 0.55 mm fine powder (FP) of <em>Hibiscus</em> calyces had lower <em>a<sub>w</sub></em>(0.37±0.01) and higher TSS (5.53±0.05%) than the 0.97 mm ground powder (GP). The extracts obtained fromGP showed a deeper red color than those of FP. The best combination of independent variables, in order to obtain the highest concentration of anthocyanins (451.4±28.1 mg/100 g d.s.) and total phenols (2016.2 ± 159.8 mg/100 g d.s.) were APS of 0.55 mm, 50% ethanol, and ETof 30 min.</p>


Author(s):  
Yimei Zhu ◽  
Masaki Suenaga ◽  
R. L. Sabatini ◽  
Youwen Xu

The (110) twin structure of YBa2Cu3O7 superconductor oxide, which is formed to reduce the strain energy of the tetragonal to orthorhombic phase transformation by alternating the a-b crystallographic axis across the boundary, was extensively investigated. Up to now the structure of the twin boundary still remained unclear. In order to gain insight into the nature of the twin boundary in Y-Ba-Cu-O system, a study using electron diffraction techniques including optical and computed diffractograms, as well as high resolution structure imaging techniques with corresponding computer simulation and processing was initiated.Bulk samples of Y-Ba-Cu-O oxide were prepared as described elsewhere. TEM specimens were produced by crushing bulk samples into a fine powder, dispersing the powder in acetone, and suspending the fine particles on a holey carbon grid. The electron microscopy during this study was performed on both a JEOL 2000EX and 2000FX electron microscopes operated at 200 kV.


Author(s):  
Shoichiro Fukusako ◽  
Masahiko Yamada ◽  
Akihiko Horibe ◽  
T. Ohmichi

2016 ◽  
Vol 12 (3) ◽  
pp. 4307-4321 ◽  
Author(s):  
Ahmed Hassan Ibrahim ◽  
Yehia Abbas

The physical properties of ferrites are verysensitive to microstructure, which in turn critically dependson the manufacturing process.Nanocrystalline Lithium Stannoferrite system Li0.5+0.5XFe2.5-1.5XSnXO4,X= (0, 0.2, 0.4, 0.6, 0.8 and 1.0) fine particles were successfully prepared by double sintering ceramic technique at pre-sintering temperature of 500oC for 3 h andthepre-sintered material was crushed and sintered finally in air at 1000oC.The structural and microstructural evolutions of the nanophase have been studied using X-ray powder diffraction (XRD) and the Rietveld method.The refinement results showed that the nanocrystalline ferrite has a two phases of ordered and disordered phases for polymorphous lithium Stannoferrite.The particle size of as obtained samples were found to be ~20 nm through TEM that increases up to ~ 85 nmand isdependent on the annealing temperature. TEM micrograph reveals that the grains of sample are spherical in shape. (TEM) analysis confirmed the X-ray results.The particle size of stannic substituted lithium ferrite fine particle obtained from the XRD using Scherrer equation.Magneticmeasurements obtained from lake shore’s vibrating sample magnetometer (VSM), saturation magnetization ofordered LiFe5O8 was found to be (57.829 emu/g) which was lower than disordered LiFe5O8(62.848 emu/g).Theinterplay between superexchange interactions of Fe3+ ions at A and B sublattices gives rise to ferrimagnetic ordering of magnetic moments,with a high Curie-Weiss temperature (TCW ~ 900 K).


2020 ◽  
Vol 71 (1) ◽  
pp. 1-12
Author(s):  
Salman H. Abbas ◽  
Younis M. Younis ◽  
Mohammed K. Hussain ◽  
Firas Hashim Kamar ◽  
Gheorghe Nechifor ◽  
...  

The biosorption performance of both batch and liquid-solid fluidized bed operations of dead fungal biomass type (Agaricusbisporus ) for removal of methylene blue from aqueous solution was investigated. In batch system, the adsorption capacity and removal efficiency of dead fungal biomass were evaluated. In fluidized bed system, the experiments were conducted to study the effects of important parameters such as particle size (701-1400�m), initial dye concentration(10-100 mg/L), bed depth (5-15 cm) and solution flow rate (5-20 ml/min) on breakthrough curves. In batch method, the experimental data was modeled using several models (Langmuir,Freundlich, Temkin and Dubinin-Radushkviechmodels) to study equilibrium isotherms, the experimental data followed Langmuir model and the results showed that the maximum adsorption capacity obtained was (28.90, 24.15, 21.23 mg/g) at mean particle size (0.786, 0.935, 1.280 mm) respectively. In Fluidized-bed method, the results show that the total ion uptake and the overall capacity will be decreased with increasing flow rate and increased with increasing initial concentrations, bed depth and decreasing particle size.


Atmosphere ◽  
2019 ◽  
Vol 10 (5) ◽  
pp. 278 ◽  
Author(s):  
Niloofar Ordou ◽  
Igor E. Agranovski

Particle size distribution in biomass smoke was observed for different burning phases, including flaming and smouldering, during the combustion of nine common Australian vegetation representatives. Smoke particles generated during the smouldering phase of combustions were found to be coarser as compared to flaming aerosols for all hard species. In contrast, for leafy species, this trend was inversed. In addition, the combustion process was investigated over the entire duration of burning by acquiring data with one second time resolution for all nine species. Particles were separately characterised in two categories: fine particles with dominating diffusion properties measurable with diffusion-based instruments (Dp < 200 nm), and coarse particles with dominating inertia (Dp > 200 nm). It was found that fine particles contribute to more than 90 percent of the total fresh smoke particles for all investigated species.


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