scholarly journals Development of a Qualitative near Infrared Screening Method for Quality Consistency Assessment of Virgin Sunflower Oil

2017 ◽  
Vol 05 (03) ◽  
pp. 25-36
Author(s):  
Fredrick Luyangi ◽  
Eliangiringa Kaale ◽  
Vicky Manyanga ◽  
Veronica Mugoyela
2019 ◽  
Vol 149 ◽  
pp. 104057 ◽  
Author(s):  
Poliana Macedo Santos ◽  
Maria Lúcia Ferreira Simeone ◽  
Marco Aurélio Guerra Pimentel ◽  
Marcelo Martins Sena

Author(s):  
Musleh Uddin ◽  
Sandor Turza ◽  
Emiko Okazaki

A near-infrared spectrometer equipped with surface interactance optical fiber probe (400-1100 nm) was used to determine the fat content in intact sardine Sardinops melanostictus which is considered one of the important fish species of world aquaculture as well as human food source. The fat contents were 2.64–25.52 % and fish weight ranges were between 45.23g and 133.76g. Partial least square regression was used to develop predictive equations for fat where two models (with and without multiplicative scatter correction known as MSC) showed relatively good performances with regression coefficients higher than 0.9 and errors below 1% on a fresh weight basis. Results showed that NIR interactance was a suitable non-destructive screening method for fat content in intact small pelagic fish like sardine.


NIR news ◽  
2018 ◽  
Vol 29 (3) ◽  
pp. 6-11 ◽  
Author(s):  
Michael K-H Pfister ◽  
Bettina Horn ◽  
Janet Riedl ◽  
Susanne Esslinger ◽  
Carsten Fauhl-Hassek

Fourier transform infrared spectroscopy becomes increasingly important for detecting adulterations in food due to a minimal sample preparation and a fast nondestructive measurement. Sunflower oil is a popular food ingredient, which might be contaminated or even adulterated by compounds with health concerns such as mineral oil. In this context a feasibility study was performed to compare the suitability of near- and mid-infrared spectroscopy for detecting mineral oil in sunflower oil. For this purpose, sunflower oils spiked with mineral oil in the concentration range of 0.001–1.0% w/w were analyzed by Fourier transform near- and mid-infrared spectroscopy, respectively, and spectra data were preprocessed prior to partial least squares regression. Hereby, the data preparation was optimized for each technique to account for model performance influences. The model performance was fairly similar for both approaches with a slightly better precision and thus limit of detection (near infrared 0.12% w/w, mid infrared 0.16% w/w) for the near-infrared-based model compared to the mid-infrared model. Consequently, both techniques are considered suitable for the determination of mineral oil in sunflower oil in the context of food authentication.


Molecules ◽  
2018 ◽  
Vol 23 (12) ◽  
pp. 3263 ◽  
Author(s):  
Marisa Rodrigues ◽  
João Lopes ◽  
Mafalda Sarraguça

A recurrent problem faced by the pharmaceutical industry when formulating drug products concerns poorly soluble drugs, which, despite having desirable pharmacological activity, present limited bioavailability. Cocrystallization is growing up as a possible approach to tackle this problem. Cocrystals are crystalline materials comprising at least two components, solid at room temperature, and held together by non-covalent bonds. The increasing interest in these compounds is steadily demanding faster, simpler, and more reliable methods for the task of screening new cocrystals. This work aims at comparing the performance of three vibrational spectroscopy techniques (mid infrared, near infrared, and Raman spectroscopy) for cocrystals screening. Presented results are based on hydrochlorothiazide, a poorly soluble drug belonging to class IV of the Biopharmaceutical Classification System. The implemented cocrystal screening procedure tested six coformers (all considered safe for human administration) added according to a drug:coformer ratio of 1:1 and 1:2 and seven solvents with different polarity. The screening method chosen was based on slurry cocrystallization performed by sonication (ultrasound assisted) in a 96-well plate. Results show that all evaluated vibrational spectroscopy techniques provided important information regarding cocrystal formation, including information on the groups involved in the cocrystallization and purity, and can be used for the screening task.


PLoS ONE ◽  
2021 ◽  
Vol 16 (6) ◽  
pp. e0253323
Author(s):  
Mário L. R. Monteiro ◽  
Rafael M. Sousa ◽  
Rafael B. Araújo ◽  
Daniel Ferraz ◽  
Mohammad A. Sadiq ◽  
...  

Purpose To evaluate the ability of confocal near-infrared reflectance (NIR) to diagnose retrograde microcystic maculopathy (RMM) in eyes with temporal visual field (VF) loss and optic atrophy from chiasmal compression. To compare NIR findings with optical coherence tomography (OCT) findings in the same group of patients. Methods Thirty-four eyes (26 patients) with temporal VF loss from chiasmal compression and 41 healthy eyes (22 controls) underwent NIR fundus photography, and macular OCT scanning. VF loss was estimated and retinal layers thickness were measured on OCT. Two examiners blinded to the diagnosis randomly examined NIR images for the presence of hyporeflective abnormality (HA) and OCT scans for the presence of microcystic macular abnormalities (MMA). The total average and hemi-macular HA area and number of microcysts were determined. The groups were compared and the level of agreement was estimated. Results The OCT-measured macular retinal nerve fiber and ganglion cell layers were thinner and the inner nuclear layer was thicker in patients compared to controls. HA and MMA were detected in 22 and 12 patient eyes, respectively, and in 0 controls (p<0.001, both comparisons). HA was significantly more frequent than MMA in patients with optic atrophy, and agreement between HA and MMA (both total and hemi-macular) was fair (kappa range: 0.24–0.29). The mean HA area was significantly greater in the nasal than temporal hemi-macula. A re-analysis of the 14 eyes with discrepant findings allowed to confirm RMM in 20 eyes (20/34) indicating that OCT detected RMM in 12 and missed it in 8 eyes. On the other hand, NIR correctly detected 18 out of 20 eyes, overcalled 4 and missed 2. Conclusions RMM is a frequent finding in eyes with severe VF loss from long-standing chiasmal compression. NIR photography appears to be more sensitive than OCT for detecting RMM and may be useful as screening method for its presence.


Author(s):  
Carolina Sheng Whei Miaw ◽  
Mário Lúcio Campos Martins ◽  
Marcelo Martins Sena ◽  
Scheilla Vitorino Carvalho de Souza

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