scholarly journals Surface Treatment of Fine Powder. New Surface Treatment of Powders by Sputtering.

1996 ◽  
Vol 47 (11) ◽  
pp. 900-904 ◽  
Author(s):  
Eiki TAKESHIMA ◽  
Kaoru KOJIMA ◽  
Takashi SHIROKURA
Keyword(s):  
Surface Treatment ◽  
Fine Powder

Twin boundary structure of a Y-Ba-Cu-O superconductor

1989 ◽  
Vol 47 ◽  
pp. 168-169
Author(s):  
Yimei Zhu ◽  
Masaki Suenaga ◽  
R. L. Sabatini ◽  
Youwen Xu
Keyword(s):  
Twin Boundary ◽  
Fine Particles ◽  
Imaging Techniques ◽  
Fine Powder ◽  
Orthorhombic Phase ◽  
Boundary Structure ◽  
Crystallographic Axis ◽  
System A ◽  
High Resolution Structure ◽  
Electron Microscopes

The (110) twin structure of YBa2Cu3O7 superconductor oxide, which is formed to reduce the strain energy of the tetragonal to orthorhombic phase transformation by alternating the a-b crystallographic axis across the boundary, was extensively investigated. Up to now the structure of the twin boundary still remained unclear. In order to gain insight into the nature of the twin boundary in Y-Ba-Cu-O system, a study using electron diffraction techniques including optical and computed diffractograms, as well as high resolution structure imaging techniques with corresponding computer simulation and processing was initiated.Bulk samples of Y-Ba-Cu-O oxide were prepared as described elsewhere. TEM specimens were produced by crushing bulk samples into a fine powder, dispersing the powder in acetone, and suspending the fine particles on a holey carbon grid. The electron microscopy during this study was performed on both a JEOL 2000EX and 2000FX electron microscopes operated at 200 kV.

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