Critical Process Parameters And Failure Analysis For Temporary Bonded Wafer Stacks

2016 ◽  
Vol 2016 (DPC) ◽  
pp. 001255-001276 ◽  
Author(s):  
Elisabeth Brandl ◽  
Karine Abadie ◽  
Markus Wimplinger ◽  
Juergen Burggraf ◽  
Thomas Uhrmann ◽  
...  

Temporary bonding is a ley process for almost any 3D integration scheme. It offers not only more stability during the thinning process but also allows handling for backside processing of thin wafers like interposers during subsequent process steps [1–2]. Although the temporary bonding technology is already used in high volume manufacturing and has proven high yield process, nevertheless, some limitation appears for some specific applications [3-4-5]. One critical failure origin is delamination, which can lead to wafer breakage and therefore yield loss. This separation of the device wafer and the carrier wafer typically occurs when the temporary bonded wafer stack (device wafer, carrier wafer and temporary bonding adhesive in between) experiences further processing done under high temperature and low vacuum like PECVD deposition. Further insight into processing parameters and a better understanding of the key contributing factors as well as its dependencies help to prevent this failure. To investigate the root cause of the delamination, thermoplastic materials, which are widely used for temporary bonding and debonding applications have been used as temporary bonding adhesives in this work. Different process parameters were investigated individually but also in combination to find the origin of the delamination. These parameters include post thinning annealing temperature, which was varied up to 370C, vacuum level, thermal gradient, bow and warp and intrinsic stress of the thin device wafer. After evaluation of the main parameters affecting the delamination appearance, two extreme cases were experimented in order to check the hypothesis. The first one exhibits delaminations even using a very soft processing conditions for a temporary bonding integration and the second case is able to withstand extreme processing conditions like high temperature up to 370C under vacuum of about 1mbar without delamination appearance. In addition, during this work, the mechanical coupling existing between the carrier and the device wafer thanks to the adhesive has been investigated. Here, a thermoplastic material was used in a temporary bonded structures using wafers with different coefficients of thermal expansion (CTE). During thermal treatment, this CTE difference induce important internal stress bow of the wafer stack. The temperature dependence of the mechanical coupling is monitored during the annealing. A mechanical decoupling between the two wafers occurs when above the polymer glass transition temperature. As a result, the rheology of the thermoplastic layer is found as a contributor to the delamination mechanism. Critical combinations of process parameters in temporary bonding process are then clearly identified and will be presented in this work.

Materials ◽  
2020 ◽  
Vol 13 (3) ◽  
pp. 538 ◽  
Author(s):  
Fabrizia Caiazzo ◽  
Vittorio Alfieri ◽  
Giuseppe Casalino

Laser powder bed fusion (LPBF) can fabricate products with tailored mechanical and surface properties. In fact, surface texture, roughness, pore size, the resulting fractional density, and microhardness highly depend on the processing conditions, which are very difficult to deal with. Therefore, this paper aims at investigating the relevance of the volumetric energy density (VED) that is a concise index of some governing factors with a potential operational use. This paper proves the fact that the observed experimental variation in the surface roughness, number and size of pores, the fractional density, and Vickers hardness can be explained in terms of VED that can help the investigator in dealing with several process parameters at once.


Energies ◽  
2021 ◽  
Vol 14 (16) ◽  
pp. 4773
Author(s):  
Jianyu Li ◽  
Hong Li ◽  
Zheming Zhu ◽  
Ye Tao ◽  
Chun’an Tang

Geothermal power is being regarded as depending on techniques derived from hydrocarbon production in worldwide current strategy. However, it has artificially been developed far less than its natural potentials due to technical restrictions. This paper introduces the Enhanced Geothermal System based on Excavation (EGS-E), which is an innovative scheme of geothermal energy extraction. Then, based on cohesion-weakening-friction-strengthening model (CWFS) and literature investigation of granite test at high temperature, the initiation, propagation of excavation damaged zones (EDZs) under unloading and the EDZs scale in EGS-E closed to hydrostatic pressure state is studied. Finally, we have a discussion about the further evolution of surrounding rock stress and EDZs during ventilation is studied by thermal-mechanical coupling. The results show that the influence of high temperature damage on the mechanical parameters of granite should be considered; Lateral pressure coefficient affects the fracture morphology and scale of tunnel surrounding rock, and EDZs area is larger when the lateral pressure coefficient is 1.0 or 1.2; Ventilation of high temperature and high in-situ stress tunnel have a significant effect on the EDZs scale; Additional tensile stress is generated in the shallow of tunnel surrounding rock, and the compressive stress concentration transfers to the deep. EDZs experiences three expansion stages of slow, rapid and deceleration with cooling time, and the thermal insulation layer prolongs the slow growth stage.


Minerals ◽  
2021 ◽  
Vol 11 (2) ◽  
pp. 162
Author(s):  
A.A. Jameei ◽  
S. Pietruszczak

This paper provides a mathematical description of hydromechanical coupling associated with propagation of localized damage. The framework incorporates an embedded discontinuity approach and addresses the assessment of both hydraulic and mechanical properties in the region intercepted by a fracture. Within this approach, an internal length scale parameter is explicitly employed in the definition of equivalent permeability as well as the tangential stiffness operators. The effect of the progressive evolution of damage on the hydro-mechanical coupling is examined and an evolution law is derived governing the variation of equivalent permeability with the continuing deformation. The framework is verified by a numerical study involving 3D simulation of an axial splitting test carried out on a saturated sample under displacement and fluid pressure-controlled conditions. The finite element analysis incorporates the Polynomial-Pressure-Projection (PPP) stabilization technique and a fully implicit time integration scheme.


2007 ◽  
Vol 26-28 ◽  
pp. 367-371
Author(s):  
Hong Zhen Guo ◽  
Zhang Long Zhao ◽  
Bin Wang ◽  
Ze Kun Yao ◽  
Ying Ying Liu

In this paper the effect of isothermal forging process parameters on the microstructure and the mechanical properties of TA15 titanium alloy was researched. The results of the tests indicate that, in the range of temperature of 850 °C~980 °C and deformation degree of 20%~60%, with the increase of temperature or deformation, as the reinforcement of deformation recrystallization, the primary α-phase tends to the spherical shape and secondary α-phase transforms from the acicular shape to fine and spherical shape with disperse distribution, which enhance the tensile properties at room and high temperature. With the increment of forging times, the spheroidization of primary α-phase aggrandizes and secondary α-phase transforms from spherical and acicular shape to wide strip shape, which decrease the tensile properties at room and high temperature. The preferable isothermal forging process parameters are temperature of 980 °C, deformation degree of 60%, and few forging times.


2014 ◽  
Vol 12 (1) ◽  
pp. 639-664 ◽  
Author(s):  
Samrand Saeidi ◽  
Masoud Talebi Amiri ◽  
Nor Aishah Saidina Amin ◽  
Mohammad Reza Rahimpour

Abstract High-temperature Fischer–Tropsch (HTFT) process aims to produce lighter cuts such as gasoline and diesel. For many years there have been studies and improvements on HTFT process to make the existing reactors more efficient. Recent studies proposed new configurations such as dual-type membrane reactor and coupling configurations reactor, which improved the performances of this process. This achievement persuades us to update the existing knowledge about the available reactors for HTFT process. In this article, features and performances overview of two classes of reactors are reviewed. The first class consists of the reactors which are based on older studies, and the second one includes recent studies which are called product intensifier reactors. Finally, it is shown that the product intensifier reactors have higher CO conversions and lower selectivity of undesired by-products which results in higher production yield of gasoline. Furthermore, the place of product intensifier reactor among common reactors with regard to the influence of the process parameters on the product distribution has been estimated.


2020 ◽  
Vol 2020 (1) ◽  
pp. 000302-000306
Author(s):  
Yuta Akasu ◽  
Emi Miyazawa ◽  
Tetsuya Enomoto ◽  
Yasuyuki Oyama ◽  
Shogo Sobue ◽  
...  

Abstract We have developed a new temporary bonding film (TBF) and new debonding system with Xe flash light irradiation, named photonic release system, for advanced package assembly process. Since new TBF has a high Tg over 200 °C after curing and shows good chemical resistance to developer, resist stripper, and plating chemicals, no delamination, voiding, and swelling were observed after thermal and chemical treatment in the bonded structure of wafer and glass carrier. In addition, by adopting a metal-sputtered glass carrier, wafer could be debonded by Xe flash light irradiation in less than 1 ms through the glass carrier with no damage. Residual TBF on the wafer surface could be peeled off smoothly at ambient temperature without residue on the wafer. In this research, we also demonstrated the good applicability of this temporary bonding film to the typical packaging process by using test vehicle including 12 inch mold wafer and the advantage of photonic release system.


Materials ◽  
2019 ◽  
Vol 12 (6) ◽  
pp. 930 ◽  
Author(s):  
Martin Malý ◽  
Christian Höller ◽  
Mateusz Skalon ◽  
Benjamin Meier ◽  
Daniel Koutný ◽  
...  

The aim of this study is to observe the effect of process parameters on residual stresses and relative density of Ti6Al4V samples produced by Selective Laser Melting. The investigated parameters were hatch laser power, hatch laser velocity, border laser velocity, high-temperature preheating and time delay. Residual stresses were evaluated by the bridge curvature method and relative density by the optical method. The effect of the observed process parameters was estimated by the design of experiment and surface response methods. It was found that for an effective residual stress reduction, the high preheating temperature was the most significant parameter. High preheating temperature also increased the relative density but caused changes in the chemical composition of Ti6Al4V unmelted powder. Chemical analysis proved that after one build job with high preheating temperature, oxygen and hydrogen content exceeded the ASTM B348 limits for Grade 5 titanium.


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