SS: Special Session Title: High Pressure Gas-Liquid Separation. Droplet size measuring technique and application

2010 ◽  
Author(s):  
Jorge Mario Marchetti ◽  
Luciano Emanuel Patruno ◽  
Ansor Gaebler ◽  
A.G. Winterthur ◽  
Hallvard Svendsen
2010 ◽  
Vol 5 (04) ◽  
pp. 183-191
Author(s):  
Luciano E. Patruno ◽  
Jorge Marchetti ◽  
Carlos Dorao ◽  
Hugo Jakobsen ◽  
Hallvard Svendsen ◽  
...  

2010 ◽  
Author(s):  
P.M. Dupuy ◽  
M. Fernandino ◽  
H.A. Jakobsen ◽  
H. Svendsen

Author(s):  
Ah Pis Yong ◽  
Md. Aminul Islam ◽  
Nurul Hasan

The aims of this study are to revisit the effect of high pressure on homogenization and the influence of pH on the emulsion droplet sizes. The high-pressure homogenization (HPH) involves two stages of processing, where the first stage involves in blending the coarse emulsion by a blender, and the second stage requires disruption of the coarse emulsion into smaller droplets by a high-pressure homogenizer. The pressure range in this review is in between 10-500 MPa. The homogenised droplet sizes can be reduced by increasing the homogenization recirculation, and there is a threshold point beyond that by applying pressure only, the size cannot be further reduced. Normally, homogenised emulsions are classified by their degree of kinetic stability. Dispersed phase present in the form of droplets while continuous phase also known as suspended droplets. With a proper homogenization recirculation and pressure, a more kinetically stable emulsion can be produced. The side effects of increasing homogenization pressure are that it can cause overprocessing of the emulsion droplets where the droplet sizes become larger rather than the expected smaller size. This can cause kinetic instability in the emulsion. The droplet size is usually measured by dynamic light scattering or by laser light scattering technique. The type of samples used in this reviews are such as chocolate and vanilla based powders; mean droplet sizes samples; basil oil; tomato; lupin protein; oil; skim milk, soymilk; coconut milk; tomato homogenate; corn; egg-yolk, rapeseed and sunflower; Poly(4-vinylpyridine)/silica; and Complex 1 until complex 4 approaches from author case study. A relationship is developed between emulsion size and pH. Results clearly show that lower pH offers smaller droplet of emulsion and the opposite occurs when the pH is increased.


2018 ◽  
Vol 24 (8) ◽  
pp. 5953-5959
Author(s):  
J. S Swathy ◽  
Prabhakar Mishra ◽  
Amitava Mukherjee ◽  
Natarajan Chandrasekaran

The current experimentation deals about the comparative study of two different high-energy emulsification techniques used for nanoemulsion formulation. The preparation of clove oil nanoemulsion accomplished through high-energy methods such as ultrasonication and high pressure homogenization. The coarse emulsion formed after mixing the oil phase consisting of clove oil and the aqueous phase comprising of Tween 80 and Milli-Q water was subjected to the both high energy method in order to compare the efficiency. The comparative study was carried out based on droplet size, nanoemulsion stability and its antimicrobial potential. Significant differences has been observed in the droplet size and antibacterial activity of nanoemulsion prepared by ultrasonication and high pressure homogenization. The nanoemulsion prepared from high pressure homogenizer exhibit good stability compared to nanoemulsion prepared using ultrasonication technique, with a low droplet size. Further the antimicrobial activity of nanoemulsion prepared via ultrasonication and high pressure homogenization was evaluated against bacterial pathogen P. alcaligenes (in-vitro studies), among which nanoemulsion prepared through high pressure homogenization exhibited significant antimicrobial potential. Therefore the nanoemulsion prepared using high pressure homogenization showed effective antimicrobial potential against P. alcaligenes with low droplet size and higher stability.


Fig. 31 Internals of colloid mill. (From Ref. 29.) colloid mills, typically equipped with rotor diameters of 10-30 cm, provide flow rates in the area of 4000-6000 L/hr, depending upon the viscosity. The key operating requirements of colloid mills are to feed the mill with a well-blended premix and to set the gap at the correct and reproducible setting. There is of-ten some difficulty with setting the gap at exactly the required distance, since the cali-bration of the gap can only be done at the manufacturer. This is less of a problem if the mill is well made and the product is not abrasive. If abrasive wear attacks the ro-tor or stator, the gap may become larger than the setting on the machine indicates. Colloid mills are generally used as "polishing" machines for emulsions or sus-pensions. That is, after the product has been totally and uniformly blended, the batch is passed through the colloid mill one or two times to further reduce the droplet or particle size. Whether or not multiple recycling passes are required depends on prod-uct requirements. Generally speaking, the colloid mill produces emulsions and suspen-sions with particle-size distributions smaller than the particle sizes obtainable using fixed gap rotor/stator mixers. They do represent an extra step in the process, and their use is suggested only when it is found that this added ability to disperse is necessary to produce a fine enough particle- or droplet-size product to enhance a product's stabil-ity. 3. Piston Homogenizers The most powerful device for producing emulsions and suspensions is the piston ho-mogenizer or high-pressure homogenizer. This device uses a high-power positive dis-placement piston-type pump to produce pressures of 3000-10,000 psig and then force

1998 ◽  
pp. 361-363

AIAA Journal ◽  
2019 ◽  
Vol 57 (3) ◽  
pp. 1260-1274 ◽  
Author(s):  
Amirreza Amighi ◽  
Nasser Ashgriz

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