Synthesis and Characterization of Chitosan-Poly Vinyl Alcohol-Graphene Oxide Nanocomposites

Author(s):  
Fariba Saeedi ◽  
Arash Montazeri ◽  
Yaser Bahari ◽  
Malihe Pishvaee ◽  
Mohammad Ranjbar

In this article, nanocomposites based on Chitosan (CS)/ poly vinyl alcohol (PVA) and graphene oxide (GO) nanoparticles were prepared by casting the stable aqueous mixture of the components in a mold. The prepared nanocomposites were characterized using Fourier-transform infrared spectroscopy (FTIR), X-ray diffractions (XRD) and viscosity measurement. Scanning Electron Microscopy (SEM) results indicated that the GO was uniformly dispersed in the polymer matrix. The water uptake ability of nanocomposites increased with an increasing the PVA content. While, the addition of GO to CS/PVA lead to a decrease in the degree of water absorption. According to the rheological analysis the viscosity of the samples decreased with increasing the GO weight percent in CS/PVA mixture.

2011 ◽  
Vol 327 ◽  
pp. 115-119 ◽  
Author(s):  
Duo Wang ◽  
Jie Gao ◽  
Wei Fang Xu ◽  
Feng Bao ◽  
Rui Ma ◽  
...  

Graphene oxide (GO) was made by a modified Hummers method. Graphene oxide modified phenolic resin nanocomposites (GO/PF) were prepared by Steglich esterification, catalyzed by dicyclohexyl carbodiimide and 4-dimethylaminopyridine. The composites were characterized by Fourier transform infrared spectrometry, differential scanning calorimetry, X-ray powder diffraction, and scanning electron microscopy. The result revealed that the graphene oxide was absolutely exfoliated and covalent linked GO/PF composite was obtained. The thermal stability of PF is remarkably improved by modification with GO.


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