Microwave-Assisted Synthesis and Crystal Structure of Novel 2-Dichloromethyl-1,3-dioxolanes

Heterocycles ◽  
2013 ◽  
Vol 87 (2) ◽  
pp. 407 ◽  
Author(s):  
Ying Fu ◽  
Fei Ye ◽  
Ying Li ◽  
Shuang Gao ◽  
Li-Xia Zhao
Molecules ◽  
2009 ◽  
Vol 14 (9) ◽  
pp. 3610-3620 ◽  
Author(s):  
Tatiana Amarante ◽  
Filipe Almeida Paz ◽  
Sandra Gago ◽  
Isabel Gonçalves ◽  
Martyn Pillinger ◽  
...  

2017 ◽  
Vol 73 (11) ◽  
pp. 1647-1651 ◽  
Author(s):  
Linh Nguyen Ngoc ◽  
Trung Vu Quoc ◽  
Hoan Duong Quoc ◽  
Manh Vu Quoc ◽  
Luong Truong Minh ◽  
...  

The title compound, C11H7NS2, was prepared in high yield (87%) using a solvent-free microwave-assisted synthesis. The structure shows whole-molecule disorder with occupancies for two orientations (A and B) of 0.4884 (10) and 0.5116 (10), respectively. The thiophene and benzothiazole rings are almost planar and make dihedral angles of 10.02 (18) and 12.54 (19)° for orientations A and B, respectively. Slipped π–π stacking between the aromatic rings, together with C—H...π, C—H...S and C—H...N interactions, result in a herringbone motif in the crystal packing.


2003 ◽  
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Beeranahally H. DORESWAMY ◽  
BASAPPA ◽  
Madegowda MAHENDRA ◽  
Kempegowda MANTELINGU ◽  
Sridhar M. ANANDALWAR ◽  
...  

2009 ◽  
Vol 515 (1) ◽  
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Ali Saberi ◽  
H. R. Manjunath ◽  
S. Naveen ◽  
T. N. Mahadeva Prasad ◽  
K. S. Rangappa ◽  
...  

ChemInform ◽  
2006 ◽  
Vol 37 (34) ◽  
Author(s):  
Weerachai Phutdhawong ◽  
Duang Buddhasukh ◽  
Stephen G. Pyne ◽  
Apinpus Rujiwatra ◽  
Chaveng Pakawatchai

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