scholarly journals Pore-scale Imaging and Characterization of Hydrocarbon Reservoir Rock Wettability at Subsurface Conditions Using X-ray Microtomography

Author(s):  
Amer M. Alhammadi ◽  
Ahmed AlRatrout ◽  
Branko Bijeljic ◽  
Martin J. Blunt
2019 ◽  
Vol 15 (3) ◽  
pp. 472-477
Author(s):  
Mohammad Syamsu Rosid ◽  
Bagus Dwi Prasetyo ◽  
Junita Trivianty ◽  
Humbang Purba

The separation process of lithology and fluid reservoir is an important part in the characterization of reservoir. It will explain the physical properties of reservoir rock lithology and fluid content by integrating the geophysics and petrophysical data. This process is difficult to do in the field "B" by using parameters of acoustic impedance and lambda mu rho (LMR), because it still has a fairly high degree of ambiguity. Poisson impedance (PI) has been implemented as a solution to address the problem. In cross-plot between Acoustic Impedance (AI) and Shear Impedance (SI), a rotation of both axes was conducted according to the trend of lithology-fluid to satisfy the equation of PI = AI – cSI. To improve the accuracy of PI calculation, the value of c (optimization factor of rotation) was calculated through the method of TCCA (Target Correlation Coefficient Analysis). The correlation with to be predicted wells data then be done. Analysis of sensitivity parameter was performed on two wells in the field "B". Parameters Zp, Zs and density which obtained from the simultaneous inversion then transformed into PI.  PI models clearly showed the separation of rock lithology of hydrocarbon reservoir. Lithology impedance (LI) as a result of the PI-GR correlation was able to separate sand and shale very well. Similarly, the impedance Fluid (FI) as a result of PI-SW correlation was also able to separate the water content in the reservoir with high SW value relative to gas with a low value of SW. Hydrocarbon zone proven at 2360-2400 m. The slicing result of the volumes of Poisson impedance inversion has provided a clear distribution and interpretation of lithology and fluid content reservoir at the field "B" of South Sumatera.


SPE Journal ◽  
2005 ◽  
Vol 10 (04) ◽  
pp. 475-484 ◽  
Author(s):  
Christoph H. Arns ◽  
Fabrice Bauget ◽  
Ajay Limaye ◽  
Arthur Sakellariou ◽  
Timothy Senden ◽  
...  

Energies ◽  
2021 ◽  
Vol 14 (16) ◽  
pp. 5103
Author(s):  
Irena Viktorovna Yazynina ◽  
Evgeny Vladimirovich Shelyago ◽  
Andrey Andreevich Abrosimov ◽  
Vladimir Stanislavovich Yakushev

This paper considers a new method for “pore scale” oil reservoir rock quantitative estimation. The method is based on core sample X-ray tomography data analysis and can be directly used to both classify rocks by heterogeneity and assess representativeness of the core material collection. The proposed heterogeneity criteria consider the heterogeneity of pore size and heterogeneity of pore arrangement in the sample void and can thus be related to the drainage effectiveness. The classification of rocks by heterogeneity at the pore scale is also proposed when choosing a reservoir engineering method and may help us to find formations that are similar at pore scale. We analyzed a set of reservoir rocks of different lithologies using the new method that considers only tomographic images and clearly distributes samples over the structure of their pore space.


Author(s):  
R. E. Herfert

Studies of the nature of a surface, either metallic or nonmetallic, in the past, have been limited to the instrumentation available for these measurements. In the past, optical microscopy, replica transmission electron microscopy, electron or X-ray diffraction and optical or X-ray spectroscopy have provided the means of surface characterization. Actually, some of these techniques are not purely surface; the depth of penetration may be a few thousands of an inch. Within the last five years, instrumentation has been made available which now makes it practical for use to study the outer few 100A of layers and characterize it completely from a chemical, physical, and crystallographic standpoint. The scanning electron microscope (SEM) provides a means of viewing the surface of a material in situ to magnifications as high as 250,000X.


Author(s):  
W. W. Barker ◽  
W. E. Rigsby ◽  
V. J. Hurst ◽  
W. J. Humphreys

Experimental clay mineral-organic molecule complexes long have been known and some of them have been extensively studied by X-ray diffraction methods. The organic molecules are adsorbed onto the surfaces of the clay minerals, or intercalated between the silicate layers. Natural organo-clays also are widely recognized but generally have not been well characterized. Widely used techniques for clay mineral identification involve treatment of the sample with H2 O2 or other oxidant to destroy any associated organics. This generally simplifies and intensifies the XRD pattern of the clay residue, but helps little with the characterization of the original organoclay. Adequate techniques for the direct observation of synthetic and naturally occurring organoclays are yet to be developed.


Author(s):  
L. T. Germinario

Understanding the role of metal cluster composition in determining catalytic selectivity and activity is of major interest in heterogeneous catalysis. The electron microscope is well established as a powerful tool for ultrastructural and compositional characterization of support and catalyst. Because the spatial resolution of x-ray microanalysis is defined by the smallest beam diameter into which the required number of electrons can be focused, the dedicated STEM with FEG is the instrument of choice. The main sources of errors in energy dispersive x-ray analysis (EDS) are: (1) beam-induced changes in specimen composition, (2) specimen drift, (3) instrumental factors which produce background radiation, and (4) basic statistical limitations which result in the detection of a finite number of x-ray photons. Digital beam techniques have been described for supported single-element metal clusters with spatial resolutions of about 10 nm. However, the detection of spurious characteristic x-rays away from catalyst particles produced images requiring several image processing steps.


Author(s):  
J. H. Resau ◽  
N. Howell ◽  
S. H. Chang

Spinach grown in Texas developed “yellow spotting” on the peripheral portions of the leaves. The exact cause of the discoloration could not be determined as there was no evidence of viral or parasitic infestation of the plants and biochemical characterization of the plants did not indicate any significant differences between the yellow and green leaf portions of the spinach. The present study was undertaken using electron microscopy (EM) to determine if a micro-nutrient deficiency was the cause for the discoloration.Green leaf spinach was collected from the field and sent by express mail to the EM laboratory. The yellow and equivalent green portions of the leaves were isolated and dried in a Denton evaporator at 10-5 Torr for 24 hrs. The leaf specimens were then examined using a JEOL 100 CX analytical microscope. TEM specimens were prepared according to the methods of Trump et al.


Author(s):  
V. Serin ◽  
K. Hssein ◽  
G. Zanchi ◽  
J. Sévely

The present developments of electron energy analysis in the microscopes by E.E.L.S. allow an accurate recording of the spectra and of their different complex structures associated with the inner shell electron excitation by the incident electrons (1). Among these structures, the Extended Energy Loss Fine Structures (EXELFS) are of particular interest. They are equivalent to the well known EXAFS oscillations in X-ray absorption spectroscopy. Due to the EELS characteristic, the Fourier analysis of EXELFS oscillations appears as a promising technique for the characterization of composite materials, the major constituents of which are low Z elements. Using EXELFS, we have developed a microstructural study of carbon fibers. This analysis concerns the carbon K edge, which appears in the spectra at 285 eV. The purpose of the paper is to compare the local short range order, determined by this way in the case of Courtauld HTS and P100 ex-polyacrylonitrile carbon fibers, which are high tensile strength (HTS) and high modulus (HM) fibers respectively.


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