scholarly journals Laser Marking of PLA FDM Printed Products

2019 ◽  
Vol 57 (2) ◽  
pp. 228-238
Author(s):  
Ionel Danut Savu ◽  
Sorin Vasile Savu ◽  
Nicusor-Alin Sirbu ◽  
Mirela Ciornei ◽  
Robert Cristian Marin ◽  
...  
Keyword(s):  
3D Printing ◽  
Storage Modulus ◽  
Laser Heating ◽  
Loss Modulus ◽  
Elastic Response ◽  
Heating Cycle ◽  
Laser Marking ◽  
Printing Process ◽  
Elongation Viscosity ◽  
High Elasticity

The paper aimed to reveal, qualitatively and quantitatively, the modifications suffered by the PLA during the complex heating cycle specific to the 3D printing followed by laser marking. The obtained results showed that the melting point of the PLA decreases from 162.2oC (which is specific to PLA filament) to 153.1oC after the 3D printing process and to 149.7oC after the laser heating. The glass transition suffered the same lowering after the printing process but an important increasing after the laser heating. The elastic modulus evolution proved a decreasing of the plasticity and that is hapenning when the material suffers an increasing of its rigidity. The elongation viscosity was analyzed and its values were decreasing with the increasing of the temperature that happened on the material. The decreasing was produced by the reduction of the elasticity, when the chain branches are decreasing their length. The decreasing is more pronounced with the increasing of the temperature. The ratio between the loss modulus to the storage modulus and quantifies the way in which the PLA absorbs and disperses energy moves its peak from 65oC (curve specific to the PLA filament) to 45oC (curve specific to the last layer deposited by 3D printing process and re-heated by laser beam for marking). The peak means the lowest storage modulus, which is a measure of elastic response of a material, so the transition from glass to high elasticity moves to the lower temperatures.

Printability assessment of psyllium husk (isabgol)/gelatin blends using rheological and mechanical properties

2020 ◽  
pp. 088532822097947
Author(s):  
Piyush Sunil Agarwal ◽  
Suruchi Poddar ◽  
Neelima Varshney ◽  
Ajay Kumar Sahi ◽  
Kiran Yellappa Vajanthri ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
3D Printing ◽  
Storage Modulus ◽  
Loss Tangent ◽  
Loss Modulus ◽  
Three Dimensional ◽  
Elastic Behavior ◽  
Flow Index ◽  
Plastic Behavior ◽  
Psyllium Husk

The primary goal of this study is to highlight the rheological and mechanical properties of a new blend composed of naturally-derived hydrogel materials- psyllium husk (PH) and gelatin (G) for its potential use in three-dimensional (3D) printing technology. The mixtures were prepared at various weight ratios of 100PH, 75PH + 25G and 50PH + 50G. A suitable selection of the printable ink was made based on the preliminary screening steps of manual filament drop test and layer stacking by 3D printing. Printing of the common features such as hexagon and square grids helped evaluating shape fidelity of the chosen ink. Although 50PH + 50G blend was found meeting most of the criteria for an ideal 3D printable ink, rheological and mechanical characterizations have been performed for all the ratios of polymeric blends. This study documents the correlation between various factors of rheology that should be taken into account while categorizing any biomaterial as a printable ink. Yield stress was measured as 18.59 ± 4.21 Pa, 268.74 ± 13.56 Pa and 109.16 ± 9.85 Pa for 50PH + 50G, 75PH + 25G and 100PH, respectively. Similarly, consistency index (K) and flow index (n) were calculated using the power law equation and found as 49.303 ± 4.17, 530.59 ± 10.92, 291.82 ± 10.53 and 0.275 ± 0.04, 0.05 ± 0.005, 0.284 ± 0.04 for 50PH + 50G, 75PH + 25G and 100PH, respectively. The loss modulus (G″) was observed dominating over storage modulus (G′) for 50PH + 50G, that depicts its liquid-like property; whereas storage modulus (G′) was found dominating in case of 75PH + 25G and 100PH, indicating their solid-like characteristics. In addition, the loss tangent value (tan δ) of 50PH + 50G was observed exceeding unity (1.05), supporting its plastic behavior, unlike 75PH + 25G (0.5) and 100PH (0.33) whose loss tangent values were estimated less than unity revealing their elastic behavior. Also, 50PH + 50G was found to have the highest mechanical strength amongst the three blends with a Young’s modulus of 9.170 ± 0.0881 kPa.

scholarly journals PP in 3D Printing - Technical and Economic Aspects

2019 ◽  
Vol 56 (4) ◽  
pp. 931-936
Author(s):  
Ionel Danut Savu ◽  
Sorin Vasile Savu ◽  
Dalia Simion ◽  
NicuȘor-Alin Sirbu ◽  
Mirela Ciornei ◽  
...  
Keyword(s):  
Thermal Analysis ◽  
3D Printing ◽  
Entire Range ◽  
Microscopic Analysis ◽  
Heating Cycle ◽  
Economic Aspects ◽  
Dynamic Shear ◽  
Elongation Viscosity ◽  
Lower Viscosity ◽  
Storage Energy

FDM is 3D printing technology using mainly PLA and ABS as filament materials. PP has close characteristics to PLA and, due to that, is a potential material for for deposition. Paper aims to analyse the behaviour of PP during heating cycle specific to 3D printing process. Macroscopic and microscopic analysis of the deposited strings have been performed. They revealed less stiffness of the PP deposition comparing to PLA, which is due to the lower viscosity of PP. DSC Thermal analysis has been done at it revealed a 30% higher heat flux in PP comparing to PLA and that increases its fluidity. It was recorded a difference between the elongation viscosity of the PP filament and the PP deposited by FDM process. After 5s the deposited PP proves higher values for the elongation viscosity. Dynamic shear rheology measurements the was applied on samples deformed under 210 kN at 190oC. It has been found that the PP requires lower storage energy and that means that it has a lower viscosity for the entire range of applied frequencies. In the same time, the complex viscosities prove different behavior. To improve the control of the deposition shape, it is necessary to reduce the extrusion temperature with 4-5%. That leads to economy in power consumption.

Influence of Constructive and Technological Parameters at Generated Spiral Parts with DLP 3D Printing Process

2019 ◽  
Vol 56 (4) ◽  
pp. 801-811
Author(s):  
Mircea Dorin Vasilescu
Keyword(s):  
3D Printing ◽  
Great Influence ◽  
Polymerization Process ◽  
Generation Process ◽  
Technological Parameters ◽  
Printing Process ◽  
The Third ◽  
Solid Models ◽  
Specific Factors ◽  
Printing Processes

This work are made for determine the possibility of generating the specific parts of a threaded assembly. If aspects of CAD generating specific elements was analysed over time in several works, the technological aspects of making components by printing processes 3D through optical polymerization process is less studied. Generating the threaded appeared as a necessity for the reconditioning technology or made components of the processing machines. To determine the technological aspects of 3D printing are arranged to achieve specific factors of the technological process, but also from the specific elements of a trapezoidal thread or spiral for translate granular material in supply process are determined experimentally. In the first part analyses the constructive generation process of a spiral element. In the second part are identified the specific aspects that can generation influence on the process of realization by 3D DLP printing of the two studied elements. The third part is affected to printing and determining the dimensions of the analysed components. We will determine the specific value that can influence the process of making them in rapport with printing process. The last part is affected by the conclusions. It can be noticed that both the orientation and the precision of generating solid models have a great influence on the made parts.

Influence of κ-Carrageenan, Modified Starch and Inulin Addition on Rheological and Sensory Properties of Non-fat and Non-added Sugar Dairy Dessert

2020 ◽  
Vol 16 (4) ◽  
pp. 462-469
Author(s):  
Zhaleh Sheidaei ◽  
Bahareh Sarmadi ◽  
Seyede M. Hosseini ◽  
Fardin Javanmardi ◽  
Kianoush Khosravi-Darani ◽  
...  
Keyword(s):  
Storage Modulus ◽  
Loss Modulus ◽  
Viscoelastic Behavior ◽  
Textural Properties ◽  
Complex Viscosity ◽  
Sensory Properties ◽  
Modified Starch ◽  
Consumer Health ◽  
Added Sugar ◽  
Textural Parameters

<P>Background: The high amounts of fat, sugar and calorie existing in dairy desserts can lead to increase the risk of health problems. Therefore, the development of functional and dietary forms of these products can help the consumer health. </P><P> Objective: This study aims to investigate the effects of &#954;-carrageenan, modified starch and inulin addition on rheological and sensory properties of non-fat and non-added sugar dairy dessert. </P><P> Methods: In order to determine the viscoelastic behavior of samples, oscillatory test was carried out and the values of storage modulus (G′), loss modulus (G″), loss angle tangent (tan &#948;) and complex viscosity (&#951;*) were measured. TPA test was used for analysis of the desserts’ texture and textural parameters of samples containing different concentrations of carrageenan, starch and inulin were calculated. </P><P> Results: All treatments showed a viscoelastic gel structure with the storage modulus higher than the loss modulus values. Increasing amounts of &#954;-carrageenan and modified starch caused an increase in G′ and G″ as well as &#951;* and a decrease in tan &#948;. Also, firmness and cohesiveness were enhanced. The trained panelists gave the highest score to the treatment with 0.1% &#954;-carrageenan, 2.5% starch and 5.5% inulin (sucralose as constant = 0.25%) and this sample was the best treatment with desirable attributes for the production of non-fat and non-added sugar dairy dessert. </P><P> Conclusion: It can be concluded that the concentration of &#954;-carrageenan and starch strongly influenced the rheological and textural properties of dairy desserts, whereas the inulin content had little effect on these attributes.</P>

scholarly journals Rheological and Textural Properties of Apple Pectin-Based Composite Formula with Xanthan Gum Modification for Preparation of Thickened Matrices with Dysphagia-Friendly Potential

Polymers ◽  
2021 ◽  
Vol 13 (6) ◽  
pp. 873
Author(s):  
Huaiwen Yang ◽  
Chai-Chun Tsai ◽  
Jung-Shiun Jiang ◽  
Chi-Chung Hua
Keyword(s):  
Storage Modulus ◽  
Water Consumption ◽  
Xanthan Gum ◽  
Loss Modulus ◽  
Textural Properties ◽  
Apple Pectin ◽  
Composite Matrix ◽  
Low Concentrations ◽  
Composite Formula

Modifying the consistency of a given edible fluid matrix by incorporating food thickeners is a common nursing remedy for individuals with dysphagia when adequate water consumption is a concern. As apple pectin (AP) offers nutraceutical benefits, properly formulated apple pectin (AP)-based thickeners featuring xanthan gum (XG) can be superior candidates for preparation of dysphagia-friendly matrices (DFMs). Our recruited DFMs exhibit fluid-like behavior (loss modulus > storage modulus, G” > G’) at lower AP concentrations (2 and 5%, w/w); they turn into weak/critical gels (G’ ≈ G”) as the concentration becomes higher (9%). In contrast, XG-DFMs display gel-like attributes with G’ > G”, even at rather low concentrations (<1%) and become more resistant to sugar, Na+, and Ca2+ modifications. The composite matrix of AP1.8XG0.2 (constraint at 2%) exhibits a confined viscosity of 278 ± 11.7 mPa∙s, which is considered a DFM, in comparison to only AP- or XG-thickened ones. The hardness measurements of XG0.6 and AP1.2XG0.8 are 288.33 ± 7.506 and 302.00 ± 9.849 N/m2, respectively, which potentially represent a promising formulation base for future applications with DFMs; these textural values are not significantly different from a commercially available product (p > 0.05) for dysphagia nursing administrations.

Effect of silane coupling on the properties of polylactic acid/barium ferrite magnetic composite filament for the 3D printing process

2021 ◽  
pp. 50965
Author(s):  
Kankavee Sukthavorn ◽  
Natkritta Phengphon ◽  
Nollapan Nootsuwan ◽  
Pongsakorn Jantaratana ◽  
Chatchai Veranitisagul ◽  
...  
Keyword(s):  
3D Printing ◽  
Polylactic Acid ◽  
Barium Ferrite ◽  
Magnetic Composite ◽  
Printing Process ◽  
Silane Coupling ◽  
Composite Filament
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