scholarly journals Bio-activation of Inert pHEMA Matrices with Phosphate Loaded Cellulose Fibers in Order to Induce Mineralization

2017 ◽  
Vol 54 (2) ◽  
pp. 235-238
Author(s):  
Andrada Serafim ◽  
Mihai Octavian Constantinescu ◽  
Florinel Tirdea Iordache ◽  
Eugeniu Vasile ◽  
Adriana Lungu ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Cellulose Fibers ◽  
Alkaline Treatment ◽  
Polymeric Matrix ◽  
Luffa Cylindrica ◽  
Inert Polymer ◽  
Water Affinity ◽  
Synthesized Materials

Luffa cylindrica fibers were purified through alkaline treatment and loaded with phosphate as mineral precursor. Their capacity of acting as bioactivator for an inert polymer was evaluated. In this respect, the PO43- - Luffa fibers were loaded in a polymeric matrix known not to promote biomineralization through immersion in mineralization media. The synthesized materials were subjected to alternative Ca/P baths and the formation of mineral was investigated through SEM. Also, the mechanical properties and the water affinity of the un-mineralized and mineralized materials were investigated.

Effect of alkaline treatment on physico-mechanical properties of black rice husk ash filled polypropylene biocomposites

2015 ◽  
Vol 57 (4) ◽  
pp. 370-376 ◽  
Author(s):  
Ahmad Adlie Shamsuri ◽  
Ahmad Khuzairi Sudari ◽  
Edi Syams Zainudin ◽  
Mazlina Ghazali
Keyword(s):  
Mechanical Properties ◽  
Rice Husk ◽  
Rice Husk Ash ◽  
Alkaline Treatment ◽  
Black Rice

scholarly journals Influence of Alkali Treatment on the Microstructure and Mechanical Properties of Coir and Abaca Fibers

Materials ◽  
2021 ◽  
Vol 14 (10) ◽  
pp. 2636
Author(s):  
Petr Valášek ◽  
Miroslav Müller ◽  
Vladimír Šleger ◽  
Viktor Kolář ◽  
Monika Hromasová ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Composite Materials ◽  
Alkali Treatment ◽  
Fiber Surface ◽  
Cellulose Fibers ◽  
Sem Analysis ◽  
Experimental Program ◽  
Time Interval ◽  
The European Union ◽  
Vegetable Fibers

Composite materials with natural fillers have been increasingly used as an alternative to synthetically produced materials. This trend is visible from a representation of polymeric composites with natural cellulose fibers in the automotive industry of the European Union. This trend is entirely logical, owing to a preference for renewable resources. The experimental program itself follows pronounced hypotheses and focuses on a description of the mechanical properties of untreated and alkali-treated natural vegetable fibers, coconut and abaca fibers. These fibers have great potential for use in composite materials. The results and discussion sections contribute to an introduction of an individual methodology for mechanical property assessment of cellulose fibers, and allows for a clear definition of an optimal process of alkalization dependent on the content of hemicellulose and lignin in vegetable fibers. The aim of this research was to investigate the influence of alkali treatment on the surface microstructure and tensile properties of coir and abaca fibers. These fibers were immersed into a 5% solution of NaOH at laboratory temperature for a time interval of 30 min, 1 h, 2 h, 3 h, 6 h, 12 h, 24 h, and 48 h, rinsed and dried. The fiber surface microstructures before and after the alkali treatment were evaluated by SEM (scanning electron microscopy). SEM analysis showed that the alkali treatment in the NaOH solution led to a gradual connective material removal from the fiber surface. The effect of the alkali is evident from the visible changes on the surface of the fibers.

Research on Mechanical Properties of Several New Regenerated Cellulose Fibers

2011 ◽  
Vol 332-334 ◽  
pp. 489-495 ◽  
Author(s):  
Rong Zhou ◽  
Ming Xia Yang
Keyword(s):  
Mechanical Properties ◽  
Phase Change Materials ◽  
Cellulose Fiber ◽  
Cellulose Fibers ◽  
Regenerated Cellulose ◽  
Pulp Fiber ◽  
Pulp Fibers ◽  
Bast Fiber ◽  
Bamboo Pulp ◽  
Lyocell Fiber

Regenerated cellulose fiber is the most widely-used and most variety of cellulose fiber. Five categories and ten kinds of fibers such as lyocell fiber, modal fiber, bamboo pulp fiber, sheng-bast fiber, Outlast viscose fiber were chosen as the research object. The strength property and elasticity of fibers in dry and wet state were tested and analysis. The comprehensive performances of fabrics were studied and mechanical properties of the fibers were listed in the order from good to bad by grey clustering analysis. The results show lyocell G100 and lyocell LF have better comprehensive mechanical properties ,while other new regenerated cellulose fibers’ comprehensive mechanical properties are general. Among these fibers modal fiber’s comprehensive mechanical properties are slightly better than sheng-bast fibers’ and bamboo pulp fibers’. Modal fiber, sheng-bast fiber and Bamboo pulp fiber have no significantly poor single parameter and all of them have better comprehensive mechanical properties than various viscose fibers. Outlast viscose in which has been added phase change materials sensitive to temperature by Microcapsule techniques fundamentally keeps similar comprehensive mechanical properties with other regenerated cellulose fibers,but its properties decline slightly .

A Review of Water-Resistant Cellulose-Based Materials in Pharmaceutical and Biomedical Application

2021 ◽  
Vol 28 ◽  
Author(s):  
Bei He ◽  
Xinxin Liu ◽  
Shi Qi ◽  
Run Zheng ◽  
Minmin Chang ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Biomedical Application ◽  
Drug Loading ◽  
Cellulose Fibers ◽  
Dip Coating ◽  
Wound Dressings ◽  
Attractive Alternative ◽  
Natural Polymers ◽  
Insoluble Drugs ◽  
Good Biocompatibility

Background: Cellulose, huge reserves of natural polymers, have been widely applied in pharmaceutical and biomedicine fields due to its good biocompatibility, biodegradability, non-toxicity and excellent mechanical properties. At present, water-resistant metal-based and petroleum-based materials applied in medical field exists obvious problems of poor biocompatibility and high cost. Therefore, water-resistant cellulose-based materials with good biocompatibility and low price will become an attractive alternative. This review aims to summarize the preparation of water-resistant cellulose-based materials and their potential application in pharmaceutical and biomedical in recent years. Methods: Common hydrophobic treatments of cellulose fibers or paper were overviewed. The preparation, properties and applications of water-resistant cellulose-based materials in the pharmaceutical and biomedical fields were summarized. Results: Common hydrophobic treatments of cellulose fibers or paper were divided into chemical modification (graft polymerization, crosslinking, solution casting or dip-coating), physico-chemical surface modifications (plasma treatments, surface patterning, electrostatic spraying and electrowetting) and physical processing (electrostatic spinning, SAS process and 3D EHD printing). These hydrophobically processed cellulose fibers or paper could be prepared into various water-resistant cellulose-based materials and applied in pharmaceutical excipients, drug-loaded amphiphilic micelles, drug-loaded composite fibers, hydrophobic biocomposite film/coatings and paper-based detectors. They presented excellent water resistance and biocompatibility, low cytotoxicity and high drug loading ability, and stable drug release rate, etc., which could be used for water-insoluble drugs carriers, wound dressings, and medical testing equipment. Conclusion: Currently, water-resistant cellulose-based materials were mainly applied in water-insoluble drugs delivery carriers, wound dressing and medical diagnosis and presented great application prospects. However, the contradiction between hydrophobicity and mechanical properties of these reported water-resistant cellulose-based materials limited their wider application in biomedicine such as tissue engineering. In the future, attention will be focused on the higher hydrophobicity of water-resistant cellulose-based materials with excellent mechanical properties. In addition, clinical medical research of water-resistant cellulose-based materials should be strengthened.

scholarly journals Enhancing Mechanical Response of Monolithic Magnesium Using Nano-NiTi (Nitinol) Particles

Metals ◽  
2018 ◽  
Vol 8 (12) ◽  
pp. 1014 ◽  
Author(s):  
Gururaj Parande ◽  
Vyasaraj Manakari ◽  
Saif Wakeel ◽  
Milli Kujur ◽  
Manoj Gupta
Keyword(s):  
Mechanical Properties ◽  
Mechanical Response ◽  
Hot Extrusion ◽  
Nickel Titanium ◽  
Structure Property ◽  
Microstructural Characteristics ◽  
Magnesium Matrix ◽  
Melt Deposition ◽  
Synthesized Materials ◽  
Minimal Adverse Effect

The present study focuses on investigating the effects of Nickel-Titanium (NiTi) nanoparticles on the microstructure and properties of pure Mg. Mg composites containing varying weight percentages (0.5, 1, 1.5, 3) of NiTi nanoparticles were fabricated using Disintegrated Melt Deposition (DMD), followed by hot extrusion. The synthesized materials were characterized in order to investigate their physical, microstructural and mechanical properties. Synthesized materials were characterized for their density and porosity levels, microstructural characteristics, and mechanical response. Superior grain refinement was realized by the presence of NiTi nanoparticles in the magnesium matrix. The addition of NiTi nanoparticles resulted in strength property enhancements of pure Mg with minimal adverse effect on the ductility. Structure-property evaluations are detailed in the current study.

scholarly journals Influence of kaolin filler on the mechanical properties of Luffa cylindrica/ polyester composite

2021 ◽  
Author(s):  
Aliyu Yaro ◽  
Laminu Kuburi ◽  
Musa Abiodun Moshood
Keyword(s):  
Mechanical Properties ◽  
Polyester Resin ◽  
Unsaturated Polyester ◽  
Low Cost ◽  
Microstructural Analysis ◽  
Polymeric Materials ◽  
Weight Fraction ◽  
Industrial Applications ◽  
Luffa Cylindrica ◽  
Polyester Composite

Abstract Polymeric materials are used in different industrial applications because they retain good environmental properties, low-cost, and easy to produce compared to conventional materials. This study investigated the effect of adding kaolin micro-filler (KF) on the mechanical properties of Luffa Fiber (LCF) reinforced polyester resin. Luffa cylindrica fiber treated with 5% NaOH, varied in weight fraction (5, 10, and 15%wt) was used to reinforce unsaturated polyester resin using hand lay-up method, whereas for the hybrid composite kaolin filler were kept constant at 6wt% fraction while the fibers varied as in the mono-reinforced composite. The samples were machined for mechanical and microstructural analysis. Analysis of the result revealed that the addition of kaolin has enhanced greatly the mechanical properties of Luffa-fibre based composites. The result reveal of the microstructure analysis, shows that there is an improvement in fiber-matrix adhesion.

Development of breathable Janus superhydrophobic polyester fabrics using alkaline hydrolysis and blade coating

2018 ◽  
Vol 89 (6) ◽  
pp. 959-974 ◽  
Author(s):  
Seonyoung Youn ◽  
Chung Hee Park
Keyword(s):  
Mechanical Properties ◽  
Alkaline Hydrolysis ◽  
Structural Changes ◽  
Treatment Time ◽  
Volume Ratio ◽  
Alkaline Treatment ◽  
The Other ◽  
Solution Temperature ◽  
Optimal Conditions ◽  
Wetting Properties

Alkaline hydrolysis is a common finishing method that is used to give polyester (polyethylene terephthalate, PET) a more natural touch and improved luster via chemical or physical changes in the fibers. However, its potential as a tool for surface modification in the development of single-sided superhydrophobic materials has not been studied yet. In this research, Janus superhydrophobic PET fabrics with asymmetric wetting properties (one side of the PET surface was rendered superhydrophobic while the other side was simply hydrophobic) were fabricated in two steps. Fine roughness was first achieved on the surface of PET fabrics by alkaline hydrolysis. Subsequently, optimized foam-coating emulsions were applied on only one surface of the alkaline-hydrolyzed PET. Alkaline treatment time, solution temperature, and viscosity of the foam-coating emulsions were varied to find optimal conditions in terms of structural changes, mechanical properties, superhydrophobicity, and absorption ability. The specimen treated with an aqueous solution of 8% sodium hydroxide at 70℃ for 60 min and coated with the mixture of the fluoro-emulsion and thickener in the volume ratio of 40:2 was determined to be the optimal conditions for the Janus superhydrophobic property. This sample showed a contact angle of 162.8° and a shedding angle of 5.6° on one side, whereas it completely permitted the percolation of water drops on the other side within 109 s. The mechanical properties of the developed Janus PET under the optimal conditions did not decrease significantly; its weight and tensile strength were found to have decreased by 3.3% and 19.2%, respectively. Furthermore, the single-sided superhydrophobic specimen demonstrated higher moisture transmissibility than the double-sided coated PET under the same alkaline treatment conditions. The method developed herein eliminates the requirement for an additional process to deliver nanoscale surface roughness and has the potential to produce waterproof–breathable PET fabrics for outdoor clothing.

Impact of Alkaline Treatment on Mechanical Properties and Thickness Swelling of Exterior Particleboard Made from Kelempayan (Neolamarckia cadamba) Wood

2018 ◽  
pp. 787-797
Author(s):  
Jamaludin Kasim ◽  
Nur Sakinah Mohamed Tamat ◽  
Nur Farahin Yusoff ◽  
Wan Mohd Nazri Wan Abdul Rahman ◽  
Nurrohana Ahmad ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Alkaline Treatment ◽  
Thickness Swelling

scholarly journals On the Use of Biobased Waxes to Tune Thermal and Mechanical Properties of Polyhydroxyalkanoates–Bran Biocomposites

Polymers ◽  
2020 ◽  
Vol 12 (11) ◽  
pp. 2615
Author(s):  
Vito Gigante ◽  
Patrizia Cinelli ◽  
Maria Cristina Righetti ◽  
Marco Sandroni ◽  
Giovanni Polacco ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Wheat Bran ◽  
Mechanical Performance ◽  
Low Cost ◽  
Impact Resistance ◽  
Mechanical Analysis ◽  
Polymeric Matrix ◽  
Flour Milling ◽  
Mechanical Performances ◽  
Analytic Models

In this work, processability and mechanical performances of bio-composites based on poly(3-hydroxybutyrate-co-3-hydroxyvalerate) (PHBV) containing 5, 10, and 15 wt % of bran fibers, untreated and treated with natural carnauba and bee waxes were evaluated. Wheat bran, the main byproduct of flour milling, was used as filler to reduce the final cost of the PHBV-based composites and, in the same time, to find a potential valorization to this agro-food by-product, widely available at low cost. The results showed that the wheat bran powder did not act as reinforcement, but as filler for PHBV, due to an unfavorable aspect ratio of the particles and poor adhesion with the polymeric matrix, with consequent moderate loss in mechanical properties (tensile strength and elongation at break). The surface treatment of the wheat bran particles with waxes, and in particular with beeswax, was found to improve the mechanical performance in terms of tensile properties and impact resistance of the composites, enhancing the adhesion between the PHBV-based polymeric matrix and the bran fibers, as confirmed by predictive analytic models and dynamic mechanical analysis results.

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