scholarly journals Evaluation of arsenic concentration in poultry and calf meat samples by hydride generation atomic fluorescence spectrometry

Author(s):  
Nusret ERTAŞ ◽  
Sema BURGAZ ◽  
Aysel BERKKAN ◽  
Orkun ALP
2013 ◽  
Vol 699 ◽  
pp. 3-6
Author(s):  
Qing Shan Pan ◽  
Wei Liu ◽  
He Ping Yan ◽  
Bo Zhou ◽  
Bao Sen Wang ◽  
...  

Using sulfhydryl cotton for preconcentration of arsenic in Radix aucklandiae and determination of the arsenic by hydride generation-atomic fluorescence spectrometry. The samples were pretreated by high pressure digest. The experimental conditions such as negative high-voltage of instrument, preconcentration conditions and separation conditions of arsenic were studied and optimized. There was a good linear relationship between the fluorescence intensity and arsenic concentration in the range of 0-10μg/L with a correlation coefficient of 0.9997, while the detection limits was 0.06μg/L, and the relative standard deviation was 1.7% .The content of arsenic in the samples was 68.9-252.3µg/kg and the recovery was 90.0-95.0%.


2012 ◽  
Vol 554-556 ◽  
pp. 1967-1970
Author(s):  
Wei Liu ◽  
Qing Shan Pan ◽  
Pei Zhang ◽  
Du Shu Huang ◽  
Ai Ping Fan ◽  
...  

To determine total arsenic in Chinese traditional herbs, a hydride generation atomic fluorescence spectrometry method was developed. The samples were pretreated by digesting system with HNO3-H2O2. The experimental conditions were studied and optimized. Under the optimum conditions, the samples was measured. There was a good linear relationship between the fluorescence intensity and arsenic concentration in the range of 0~80μg•L-1with a correlation coefficient of 0.9995,while the detection limit was 0.036μg•L-1,the relative standard deviation was 1.9% .Trace total arsenic in the samples was 0.145~0.376μg•g-1 and a recovery range of 83.9%~108.5% were obtained.


2016 ◽  
Vol 12 (2) ◽  
pp. 102-107 ◽  
Author(s):  
Walter N.L. dos Santos ◽  
Dannuza D. Cavalcante ◽  
Paula D.N. Gomes ◽  
Daniele C.M.B. Santos ◽  
Luciana B. Oliveira ◽  
...  

2015 ◽  
Vol 30 (5) ◽  
pp. 1133-1141 ◽  
Author(s):  
Lindomar A. Portugal ◽  
Laura Ferrer ◽  
Antonio M. Serra ◽  
Douglas Gonçalves da Silva ◽  
Sérgio Luis C. Ferreira ◽  
...  

A non-chromatographic automated system for antimony speciation.


2013 ◽  
Vol 25 (14) ◽  
pp. 8169-8172 ◽  
Author(s):  
Longfei Cai ◽  
Chunxiu Xu ◽  
Minghua Zhong ◽  
Yunying Wu ◽  
Shufen Zheng

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