Methods of testing plastics Effect of temperature. Methods 101 and 102. Crushing strength after heating (heat resistance), deformation at elevated temperatures

2015 ◽  
1967 ◽  
Vol 17 (01/02) ◽  
pp. 112-119 ◽  
Author(s):  
L Dintenfass ◽  
M. C Rozenberg

SummaryA study of blood coagulation was carried out by observing changes in the blood viscosity of blood coagulating in the cone-in-cone viscometer. The clots were investigated by microscopic techniques.Immediately after blood is obtained by venepuncture, viscosity of blood remains constant for a certain “latent” period. The duration of this period depends not only on the intrinsic properties of the blood sample, but also on temperature and rate of shear used during blood storage. An increase of temperature decreases the clotting time ; also, an increase in the rate of shear decreases the clotting time.It is confirmed that morphological changes take place in blood coagula as a function of the velocity gradient at which such coagulation takes place. There is a progressive change from the red clot to white thrombus as the rates of shear increase. Aggregation of platelets increases as the rate of shear increases.This pattern is maintained with changes of temperature, although aggregation of platelets appears to be increased at elevated temperatures.Intravenously added heparin affects the clotting time and the aggregation of platelets in in vitro coagulation.


2020 ◽  
pp. 511-515
Author(s):  
E.N. Eremin ◽  
A.S. Losev ◽  
I.A. Ponomarev ◽  
S.A. Borodikhin

The heat-resistance of coating from deposited steel 15N8G6M3FTB at temperature of 900 °С is studied. It is established that this dependence occurs in the first hours. The average mass gain of the metal scale of such coating at 900 °С is 0.0128 kg/(m2 •h). It is shown that the basis of metal scale of the composition 15N8G6M3FTB is hematite Fe2O3 and magnetite Fe3O4, as well as MnO, which have protective properties. The number of other phase compounds with high protective properties is negligible. The coating from steel 15N8G6M3FTB can be used for applying to the surface of parts operating at elevated temperatures.


2012 ◽  
Vol 531-532 ◽  
pp. 122-126
Author(s):  
Hai Bin Zhou ◽  
Chuan Shuang Hu ◽  
Jian Hui Zhou

Wood is being used extensively in timber construction in China. In fire-resistant design for timber construction, the main goal is to ensure that enough structural integrity is maintained during a fire to prevent structure collapse. It is important to understand its structural performance when exposed to elevated temperatures and loaded by stress levels. To study the interaction effect of Chinese larch wood, a total of 72 small clear wood samples were observed under constant stress levels when the wood temperature was elevated. The results indicated that Chinese larch wood was more susceptible to the coupling effect of temperature and stress. The interaction promoted a temporary stable flexural structure to collapse during a short exposure time.


1973 ◽  
Vol 46 (2) ◽  
pp. 483-503 ◽  
Author(s):  
T. C. P. Lee ◽  
S. H. Morrell

Abstract The network analysis of the aged sulfur vulcanizates of nitrile rubber serves to re-emphasize the complexity of the structural changes which can occur at elevated temperatures. Three factors control the rate and degree of crosslinking in these systems. First there is the crosslink structure. An essential feature for heat resistance in sulfur compounds is that they should contain, as near as possible, 100 per cent monosulfide crosslinks. Systems which contain polysulfide crosslinks, and probably to a lesser extent disulfide crosslinks, are prone to purely thermal crosslink shortening or cleavage reactions. The physical effect of these thermal changes would be superimposed on the effects brought about by thermooxidative changes. Despite their thermal stability monosulfide crosslinks can oxidize and cleave, a process which will result in stress relaxation if the sample is held in tension or compression. Hence for truly inert systems one will have to turn to non-sulfur cure in conjunction with a suitable stabilizer. Because the results indicate that scission associated with chemistry at the monosulfide crosslink is reversible, this cleavage does not contribute to the change in modulus or hardening during aging. This brings in the second controlling factor. The degree and rate of hardening depends on the nature of the products of vulcanization, and also possibly on those species intermediate between crosslink and accelerator, the pendent accelerator groups. In acting as an antioxidant ZDMC is apparently oxidized to a new source of sulfur. The more heat resistant cadmate system contains no such products and also a minimum of pendent accelerator groups. This leads to the third factor—the added antioxidant. For its heat resistance the cadmate system relies on an antioxidant. It is this which stops crosslinking reactions through autooxidation of the polymer backbone. The efficiency with which the antioxidant (dioctyldiphenylamine) works suggests that there is a synergistic effect in operation, which in some way involves cadmium. Thus the best heat resistance will be obtained where the compound yields monosulfide crosslinks, an uncomplicated network structure, unreactive vulcanization products, and contains a highly effective antioxidant system. Many facets of the aging of nitrile rubber are still open to explanation. Not the least of these is why crosslinks formed during the aging of the TMTD/S vulcanizate, which, by reason of their reactivity to methyl iodide, are thought to be sulfidic, are not themselves oxidized in a manner similar to the original monosulfide crosslinks. Model compound studies would answer this and other questions.


Author(s):  
Xianqin Yang ◽  
Frances Tran ◽  
Peipei Zhang ◽  
Hui Wang

The locus of heat resistance (LHR) can confer heat resistance to Escherichia coli to various extents. This study investigated the phylogenetic relationships, and genomic and phenotypic characteristics of E. coli with or without LHR recovered from beef by direct plating or from enrichment broth at 42°C. LHR-positive E. coli isolates (n=24) were whole genome-sequenced by short- and long-reads. LHR-negative isolates (n=18) from equivalent sources as LHR-positive isolates were short-read sequenced. All isolates were assessed for decimal reduction time at 60°C ( D 60°C ) and susceptibility to E-SAN and Perox-E. Selected isolates were evaluated for growth at 42°C. The LHR-positive and negative isolates were well separated on the core genome tree, with 22/24 of the positive isolates clustering into three clades. Isolates within clade 1 and 2, despite their different D 60°C values, were clonal, as determined by subtyping (MLST, core genome MLST, and serotyping). Isolates within each clade are of one serotype. The LHR-negative isolates were genetically diverse. The LHR-positive isolates had a larger (p<0.001) median genome size by 0.3 Mbp (5.0 vs 4.7 Mbp), and overrepresentation of genes in plasmid maintenance, stress response and cryptic prophages, but underrepresentation of genes involved in epithelial attachment and virulence. All LHR-positive isolates harbored a chromosomal copy of LHR, and all clade 2 isolates had an additional partial copy of LHR on conjugative plasmids. The growth rates at 42°C were 0.71±0.02 and 0.65±0.02 logOD h −1 for LHR-positive and negative isolates. No meaningful difference in sanitizer susceptibility was noted between LHR-positive and negative isolates. Importance Resistant bacteria are serious food safety and public health concerns. Heat resistance conferred by the LHR varies largely among different strains. The findings in this study show that genomic background and composition of LHR, in addition to the presence of LHR, play an important role in the degree of heat resistance in E. coli , and that strains with certain genetic background are more likely to acquire and maintain the LHR. Also, caution should be exercised when recovering E. coli at elevated temperatures as the presence of LHR may confer growth advantages to some strains. Interestingly, the LHR harboring strains seem to have evolved further from their primary animal host to adapt to their secondary habitat, as reflected by fewer genes in virulence and epithelial attachment. The phylogenetic relationships among the isolates point towards multiple mechanisms for acquiring LHR, likely prior to their deposition on meat.


2010 ◽  
Vol 2010 (HITEC) ◽  
pp. 000359-000366 ◽  
Author(s):  
Patrick McCluskey ◽  
Chandradip Patel ◽  
David Lemus

Elevated temperatures can significantly affect the performance and reliability of MEMS gyroscope sensors. A MEMS vibrating resonant gyroscope measures angular velocity via a displacement measurement which can be on the order on nanometers. High sensitivity to small changes in displacement causes the MEMS Gyroscope sensor to be strongly affected by changes in temperature which can affect the displacement of the sensor due to thermal expansion and thermomechanical stresses. Analyzing the effect of temperature on MEMS gyroscope sensor measurements is essential in mission critical high temperature applications, such as inertial tracking of the movement of a fire fighter in a smoke filled indoor environment where GPS tracking is not possible. In this paper, we will discuss the development of the high temperature package for the tracking application, including the characterization of the temperature effects on the performance of a MEMS gyroscope. Both stationary and rotary tests were performed at room and at elevated temperatures on 10 individual single axis MEMS gyroscope sensors.


2011 ◽  
Vol 2011 (HITEN) ◽  
pp. 000014-000020 ◽  
Author(s):  
James Galipeau ◽  
George Slama

As more electronics are used in down-hole energy exploration, under the hood automotive applications, and in other environments where temperatures exceed 200 °C; there is a need for compact passive magnetic components that operate reliably at elevated temperatures. Most ferrites used to make multi layer ceramic inductors have Curie temperatures in the 100–200 °C range. As temperatures rise above the Curie point ferrites lose their magnetic properties and become paramagnetic. This means that traditional multi-layer ceramic inductors suffer severe performance degradation when operated at elevated temperatures. Therefore, ferrite materials with higher Curie temperatures need to be developed to increase device performance and reliability at these high temperatures. In this work inductors were made from a low-temperature, co-fire compatible, ferrite with a Curie temperature of 350 °C. The inductors were first subjected to a 1000 hour life test at 300 °C during which the electrical parameters were found to change no more than 4 %. The inductance, resistance, core loss, and saturation flux density of the inductors were measured at various temperatures. Additional testing focused on the effect of temperature on the device's frequency profile and performance changes under thermal cycling and thermal shock.


2018 ◽  
Vol 7 (4.20) ◽  
pp. 205 ◽  
Author(s):  
Aqil M. ALmusawi ◽  
Thulfiqar S. Hussein ◽  
Muhaned A. Shallal

Recent developments in the production of ecologically friendly building composites have led to a renewed interest in the use of vegetable fibers as a reinforcement element. Traditional pure Plaster of Paris (POP) can suffer from the development of micro-cracks due to thermal expansion. Therefore, sisal fiber was studied for its potential as an ecological element to restrict and delay the development of micro-cracks in POP. Different sisal proportions of 0, 2, 4, 6, 8 and 10 wt. % of POP were used to characterize the physical and mechanical properties of POP at the ambient temperature. Then, the effects of temperatures of 25, 100, 200, 300, 400 and 500  were investigated. Results proved that the composite of 10% sisal fiber had the best mechanical properties. Also, when the fiber content was increased, the composite’s performance was enhanced, becoming better able to resist elevated temperatures. However, raising the temperature to 300 or above had a negative effect on the mechanical properties, which were significantly decreased due to the degradation of the sisal fiber. 


Author(s):  
J. Brnic ◽  
M. Canadija ◽  
G. Turkalj ◽  
D. Lanc

In this paper, some interesting, experimentally determined actualities referring to the 50CrMo4 steel are presented. That way, the mechanical properties of the material are derived from uniaxial tensile tests at lowered and elevated temperatures. Engineering stress versus strain diagrams for both mentioned temperatures, curves representing the effect of temperature on specimen elongation, and short-time creep curves are given. Notch impact energy test was also carried out. Taking into consideration the service life of the final product of the mentioned steel widely used in engine and machine technology, all of the mentioned data may be relevant during design and manufacturing procedure.


Sign in / Sign up

Export Citation Format

Share Document