Reference sources. Calibration of surface contamination monitors. Alpha-, beta- and photon emitters

2016 ◽  
Author(s):  
Pete Burgess

Normally, beta and alpha surface contamination monitors are used with a simple counting threshold, i.e. any pulse over a predetermined amplitude is counted. This is very different from gamma monitoring, where the use of counting windows is very popular and the use of full multi-channel analysis is common. Many current surface contamination ratemeters have the capacity to drive dual phosphor detectors and can be set up to provide beta and alpha channels. Effectively, the beta channel is a counting window, i.e. all pulses which are bigger than the threshold and smaller than the alpha threshold are counted. Larger pulses go into the alpha channel. This paper addresses how this can be used with beta only and alpha only detectors to provide information on the source. The detector is set up conventionally to a defined point for the lowest beta energy anticipated. The instrument is then switched to alpha + beta mode and the alpha threshold set to 3 times the beta threshold. With this set up, the alpha to beta channel count rate ratio varies smoothly by a factor of 14 between Y-90 (Emax 2.27 MeV) and C-14 (Emax 0.16 MeV). Hence the instrument can be used to estimate the energy of an unknown beta contaminant or to confirm that a mixed beta fingerprint has essentially the same mix. The same approach can be used with alpha probes to confirm the source quality. The main worry with alpha monitoring is the surface condition. A poor surface condition will lead to a low count rate. Using the channel ratio method will identify grubby sources. The resulting ratio can be used either as a go/no trigger, i.e. any surface with a low ratio will be treated as untrustworthy, or alternatively the ratio can be used to correct the reading to give a better estimate of surface activity.


2019 ◽  
Author(s):  
Florinda Cfarku ◽  
Manjola Shyti ◽  
Irma Berdufi ◽  
Polikron Dhoqina ◽  
Elida Bylyku

2016 ◽  
Vol 63 (2) ◽  
pp. 634-638 ◽  
Author(s):  
Y. Ifergan ◽  
S. Dadon ◽  
A. Ocherashvili ◽  
I. Israelashvili ◽  
Y. Yehuda-Zada ◽  
...  

Author(s):  
S. Fujishiro

The mechanical properties of three titanium alloys (Ti-7Mo-3Al, Ti-7Mo- 3Cu and Ti-7Mo-3Ta) were evaluated as function of: 1) Solutionizing in the beta field and aging, 2) Thermal Mechanical Processing in the beta field and aging, 3) Solutionizing in the alpha + beta field and aging. The samples were isothermally aged in the temperature range 300° to 700*C for 4 to 24 hours, followed by a water quench. Transmission electron microscopy and X-ray method were used to identify the phase formed. All three alloys solutionized at 1050°C (beta field) transformed to martensitic alpha (alpha prime) upon being water quenched. Despite this heavily strained alpha prime, which is characterized by microtwins the tensile strength of the as-quenched alloys is relatively low and the elongation is as high as 30%.


2020 ◽  
Vol 90 (5-6) ◽  
pp. 411-416 ◽  
Author(s):  
Carina Kolot ◽  
Ana Rodriguez-Mateos ◽  
Rodrigo Feliciano ◽  
Katharina Bottermann ◽  
Wilhelm Stahl

Abstract. Chalcones are a type of flavonoids characterized by an α-β unsaturated structural element which may react with thiol groups to activate pathways such as the Nrf2-Keap-1 system. Naringenin chalcone is abundant in the diet but little is known about its bioavailability. In this work, the bioavailability of naringenin chalcone from tomatoes was investigated in a group of healthy men (n=10). After ingestion of 600 grams of tomatoes providing a single dose of 17.3 mg naringenin chalcone, 0.2 mg of naringenin, and 195 mg naringin plasma levels of free and conjugated naringenin and naringenin chalcone (glucuronide and sulfate) were analyzed by UHPLC-QTOF-MS at 0.5, 1, 3, and 6 h post-consumption. Plasma levels of conjugated naringenin increased to about 12 nmol/L with a maximum at about 3 h. Concentrations of free naringenin hardly elevated above baseline. Plasma levels of free and conjugated naringenin chalcone significantly increased. A maximum of the conjugated chalcone was reached at about 3 h after ingestion with an average concentration of about 0.5 nmol/L. No free chalcone was detectable at baseline but low amounts of the unconjugated compound could be detected with an average maximum of 0.8 nmol/L at about 1 h after ingestion. The data demonstrate that naringenin chalcone is bioavailable in humans from cherry tomatoes as a dietary source. However, availability is poor and intramolecular cyclisation as well as extended metabolism likely contribute to the inactivation of the reactive alpha-beta unsaturated reactive center as well as the excretion of the biologically active molecule, respectively.


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